ANALYSIS OF AGRI-FOODSTUFFS - PROTOCOL OF CHARACTERIZATION FOR THE VALIDATION OF A QUANTITATIVE METHOD OF ANALYSIS BY CONSTRUCTION OF AN ACCURACY PROFILE

Published date

01-12-2013

Publisher

1 Domaine d'application
2 Références normatives
3 Définitions et symboles
  3.1 Vocabulaire général
  3.2 Vocabulaire propre au présent document
  3.3 symboles
4 Contenu du dossier de validation intra-laboratoire
  4.1 Texte ou référence précise de la méthode de
      référence
  4.2 Description détaillée de la méthode alternative
  4.3 Portée de la validation intra-laboratoire
  4.4 Organisation des protocoles de mesure
  4.5 Calculs et conclusions
5 Partie expérimentale
  5.1 Étalonnage de la méthode alternative (plan A)
  5.2 Spécificité de la méthode alternative (plan B)
  5.3 Évaluation de la fidélité (répétabilité) et de la
      justesse par rapport à la méthode de référence
      (plan C)
  5.4 Reproductibilité interne (plan D) (optionnel)
6 Résumé des expériences effectuées
Annexe A (informative) Exemples
Annexe B Tables statistiques
Annexe C Conduite des calculs avec un tableur
Bibliographie

Le présent document se propose de guider un laboratoire d'analyse agro-alimentaire dans la constitution d'un dossier de validation intralaboratoire d'une méthode d'analyse quantitative pratiquée en interne, par rapport à une méthode de référence. Cette validation doit permettre à tout analyste d'utiliser la méthode en connaissant ses performances.

DevelopmentNote	Indice de classement: V03-110. (02/2004) PR NFV 03 110 February 2009. (02/2009) PR NFV 03 110 November 2009. (11/2009)
DocumentType	Standard
PublisherName	Association Francaise de Normalisation
Status	Current

13/30278127 DC : 0	BS ISO 20752 - CORK STOPPERS - DETERMINATION OF RELEASABLE 2, 4, 6-TRICHLOROANISOL (TCA)
16/30294375 DC : DRAFT APR 2016	BS EN ISO 19343 - MICROBIOLOGY OF THE FOOD CHAIN - DETECTION AND QUANTIFICATION OF HISTAMINE IN FISH AND FISHERY PRODUCTS - HPLC METHOD
BS ISO 20752:2014	Cork stoppers. Determination of releasable 2, 4, 6-trichloroanisol (TCA)
DIN EN ISO 19343 E : 2017	MICROBIOLOGY OF THE FOOD CHAIN - DETECTION AND QUANTIFICATION OF HISTAMINE IN FISH AND FISHERY PRODUCTS - HPLC METHOD (ISO 19343:2017)
NFV 03 020-2 : 2005 XP	FOODSTUFFS - DETECTION AND QUANTIFICATION OF GENETICALLY MODIFIED VEGETAL ORGANISMS AND DERIVED PRODUCTS - PART 2: METHODS BASED ON POLYMERASE CHAIN REACTION
XP V03 044 : 2008 XP	INTRALABORATORY VALIDATION CRITERIA FOR THE METHODS OF DETECTION AND QUANTIFICATION OF SPECIFIC NUCLEIC ACID SEQUENCES
FD V03 115 : 96 FD	ANALYSIS OF AGRICULTURAL AND FOOD PRODUCTS - GUIDE FOR THE USE OF REFERENCE MATERIALS
BS EN ISO 19343:2017	Microbiology of the food chain. Detection and quantification of histamine in fish and fishery products. HPLC method
I.S. EN ISO 19343:2017	MICROBIOLOGY OF THE FOOD CHAIN - DETECTION AND QUANTIFICATION OF HISTAMINE IN FISH AND FISHERY PRODUCTS - HPLC METHOD (ISO 19343:2017)
UNE-EN ISO 19343:2018	Microbiology of the food chain - Detection and quantification of histamine in fish and fishery products - HPLC method (ISO 19343:2017)
ISO 19343:2017	Microbiology of the food chain — Detection and quantification of histamine in fish and fishery products — HPLC method
EN ISO 19343:2017	Microbiology of the food chain - Detection and quantification of histamine in fish and fishery products - HPLC method (ISO 19343:2017)
DIN EN ISO 19343:2016-05 (Draft)	MICROBIOLOGY OF THE FOOD CHAIN - DETECTION AND QUANTIFICATION OF HISTAMINE IN FISH AND FISHERY PRODUCTS - HPLC METHOD (ISO 19343:2017)
ISO 20752:2014	Cork stoppers — Determination of releasable 2, 4, 6-trichloroanisol (TCA)
FD X07 008 : 2008 FD	METROLOGY - ARBORESCENCE OF STANDARDS AND WORK ON METROLOGY ('ROAD MAP' OF STANDARDS)
NFX 07 008 : 2008 FD	METROLOGY - ARBORESCENCE OF STANDARDS AND WORK ON METROLOGY ("ROAD MAP" OF STANDARDS)

NF ISO 5725-2 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 2: BASIC METHOD FOR THE DETERMINATION OF REPEATABILITY AND REPRODUCIBILITY OF A STANDARD MEASUREMENT METHOD
NF ISO 5725-1 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 1: GENERAL PRINCIPLES AND DEFINITIONS
NF ISO 5725-3 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 3: INTERMEDIATE MEASURES OF THE PRECISION OF A STANDARD MEASUREMENT METHOD
NF ISO 5725-4 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 4: BASIC METHODS FOR THE DETERMINATION OF THE TRUENESS OF A STANDARD MEASUREMENT METHOD
ISO/IEC Guide 99:2007	International vocabulary of metrology Basic and general concepts and associated terms (VIM)