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API 4635 : 1996

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

COMPILATION OF FIELD ANALYTICAL METHODS FOR ASSESSING PETROLEUM PRODUCT RELEASES

Withdrawn date

12-12-1996

Published date

12-01-1996

EXECUTIVE SUMMARY
1 INTRODUCTION
       BACKGROUND
       PURPOSE AND SCOPE
2 DATA QUALITY CLASSIFICATIONS
       DATA QUALITY LEVEL 1A
       DATA QUALITY LEVEL 1B
       DATA QUALITY LEVEL 2
       DATA QUALITY LEVEL 3
       DATA QUALITY LEVEL 4
3 TOTAL ORGANIC VAPOR DETECTORS AND HEADSPACE
    ANALYSIS SUMMARY
       METHOD OVERVIEW
            Applications and Advantages
       INTERFERENCES AND LIMITATIONS
       OPERATING PRINCIPLES/INSTRUMENTATION
            Flame Ionization Detectors
            Photoionization Detectors
       METHOD REQUIREMENTS
            Initial Setup
            Sampling and Analysis Procedures
       QUALITY ASSURANCE/QUALITY CONTROL REQUIREMENT
4 FIELD GAS CHROMATOGRAPHS
       SUMMARY
       METHOD OVERVIEW
            Application and Advantages
       INTERFERENCES AND LIMITATIONS
       OPERATING PRINCIPLES/INSTRUMENTATION
            Detectors
            Field Gas Chromatographs
       METHOD REQUIREMENTS
            Comparative Sample Preparation and Analysis
            Procedures
            Solvent Extraction
            Purge-and-Trap Method
            Static Headspace Method
            Headspace/GC and Soils
            Total Petroleum Hydrocarbon Analysis Using
            Field GCs
5 IMMUNOASSAY FIELD TEST KITS
       SUMMARY
       METHOD OVERVIEW
            Application and Advantages
       INTERFERENCES AND LIMITATIONS
            False Positives/False Negatives
            Temperature Ranges for Storage and Operation
            Calibration Standards
       OPERATING PRINCIPLES
       METHOD REQUIREMENTS
       QUALITY ASSURANCE/QUALITY CONTROL
            Calibration
            Method Blank
            Duplicate Field Analyses
            Confirmation by Reference Method
            Matrix Blanks
6 PORTABLE INFRARED DETECTORS
       SUMMARY
       METHOD OVERVIEW
            Application and Advantages
       INTERFERENCES AND LIMITATIONS
       OPERATING PRINCIPLES/INSTRUMENTATION
       METHOD REQUIREMENTS
            Initial Setup
            Sampling and Analysis Procedures
       QUALITY ASSURANCE/QUALITY CONTROL
    DO/REDOX ELECTRODES
       SUMMARY
       METHOD OVERVIEW
            Application and Advantages
       INTERFERENCES AND LIMITATIONS
            REDOX
            DO
       OPERATING PRINCIPLES
            Dissolved Oxygen
            REDOX
       INSTRUMENTATION
            Dissolved Oxygen
            REDOX
       METHOD REQUIREMENTS
            Initial Setup
            Sampling Procedures
       QUALITY ASSURANCE/QUALITY CONTROL
            Response Time
            Calibration
EMERGING FIELD ANALYTICAL METHODS
       FIBER OPTIC CHEMICAL SENSORS
       VISIBLE UV FLUORESCENCE AND UV FLUORESCENCE
       SPECTROSCOPY
       UV ABSORPTION SPECTROSCOPY
       GAS CHROMATOGRAPHY/MASS SPECTROMETRY
REFERENCES
GLOSSARY

Describes a compilation of the most widely used field analytical methods available to perform on-site analyses of organic compounds in soil and groundwater. Methods include total organic vapour analysers, field gas chromatography, immunoassay, infrared analysers, and dissolved oxygen/oxidation-reduction potential electrodes.

DocumentType
Standard
ProductNote
This product is unavailable in Cuba, Iran, North Korea, Syria
PublisherName
American Petroleum Institute
Status
Withdrawn

API 4670 : 1998 SELECTING FIELD ANALYTICAL METHODS - A DECISION-TREE APPROACH

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