ASTM C 1068 : 2015
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
Available format(s)
Hardcopy , PDF
Superseded date
11-10-2021
Language(s)
English
Published date
06-30-2015
1.1This guide provides guidance for selecting, validating, and qualifying measurement methods when qualification is required for a specific program. The recommended practices presented in this guide provide a major part of a quality assurance program for the laboratory data (see Fig. 1). Qualification helps to assure that the data produced will meet established requirements.
1.2The activities intended to assure the quality of analytical laboratory measurement data are diagrammed in Fig. 1. Discussion and guidance related to some of these activities appear in the following sections:
| Section | |
| Selection of Measurement Methods | 5 |
| Validation of Measurement Methods | 6 |
| Qualification of Measurement Methods | 7 |
| Control | 8 |
| Personnel Qualification | 9 |
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| Committee |
C 26
|
| DocumentType |
Guide
|
| Pages |
7
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
| ASTM C 1316 : 2008 : R2017 | Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using <sup>252</sup>Cf Shuffler |
| ASTM C 1187 : 2015 | Standard Guide for Establishing Surveillance Test Program for Boron-Based Neutron Absorbing Material Systems for Use in Nuclear Fuel Storage Racks In a Pool Environment |
| ASTM C 1672 : 2017 | Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 697 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets |
| ASTM C 1625 : 2019 | Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry |
| ASTM C 1832 : 2021 | Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer |
| ASTM C 1907 : 2021 | Standard Practice for Preparation of Plutonium Materials by Pyrohydrolysis for Determination of Fluoride, Chloride, or Both |
| ASTM C 1187 : 2020 : REV A | Standard Guide for Establishing Surveillance Test Program for Boron-based Neutron Absorbing Material Systems for Use in Nuclear Fuel Storage Racks in Pool Environment |
| ASTM C 759 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions |
| ASTM C 1853 : 2017 | Standard Test Method for The Determination of Carbon (Total) Content in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by Direct Combustion-Infrared Detection Method |
| ASTM C 1156 : 2018 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM C 1625 : 2012 | Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry |
| ASTM C 1854 : 2017 | Standard Test Method for Determination of Hydrogen (total from all sources) in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by the Inert Gas Fusion Technique Followed by Thermal Conductivity Measurement |
| ASTM C 1855 : 2018 | Standard Test Method for Determination of Uranium and Plutonium Concentration in Aqueous Solutions Using Hybrid K-Edge Densitometry and X-Ray Fluorescence |
| ASTM C 1009 : 2013 : REV A | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
| ASTM C 698 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O<inf>2</inf>) |
| ASTM C 1832 : 2016 | Standard Test Method for Determination of Uranium Isotopic Composition by the Modified Total Evaporation (MTE) Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 1742 : 2017 | Standard Test Method for Isotopic Analysis of Uranium Hexafluoride by Double Standard Single-Collector Gas Mass Spectrometer Method (Withdrawn 2023) |
| ASTM C 1865 : 2018 | Standard Test Method for The Determination of Carbon and Sulfur Content in Plutonium Oxide Powder by the Direct Combustion-Infrared Spectrophotometer |
| ASTM C 1210 : 2018 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM C 1128 : 2018 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1267 : 2017 | Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium |
| ASTM C 758 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal |
| ASTM C 1817 : 2016 | Standard Test Method for The Determination of the Oxygen to Metal (O/M) Ratio in Sintered Mixed Oxide ((U, Pu)O<inf>2</inf>) Pellets by Gravimetry |
| ASTM C 1871 : 2018 : REV A | Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 1108 : 2017 | Standard Test Method for Plutonium by Controlled-Potential Coulometry |
| ASTM C 1207 : 2010 : R2018 | Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting |
| ASTM C 1165 : 2017 | Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode |
| ASTM C 1009 : 2013 : REV A | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
| ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 2655 : 2008 | Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods |
| ASTM C 1210 : 2018 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM C 1128 : 2018 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1009 : 1996 : EDT 1 | Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005) |
| ASTM C 1210 : 1996 : EDT 1 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005) |
| ASTM C 1210 : 2021 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry |
| ASTM C 1128 : 1995 : EDT 1 | Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials |
| ASTM E 2554 : 2013 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques |
| ASTM C 1156 : 2003 : R2011 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM C 1210 : 2012 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM E 2655 : 2014 : R2020 | Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods |
| ASTM C 1128 : 2015 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1210 : 2006 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM E 2554 : 2018 : EDT 1 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques |
| ASTM C 1297 : 2003 : R2011 | Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1297 : 2003 | Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1297 : 1995 : EDT 1 | Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1156 : 2018 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM E 2655 : 2014 | Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods |
| ASTM C 1128 : 2001 | Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials |
| ASTM E 2554 : 2007 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method in a Single Laboratory Using a Control Sample Program |
| ASTM C 1156 : 1995 : EDT 1 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM E 2554 : 2018 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques |
| ASTM C 1009 : 2021 | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
| ASTM C 1128 : 2001 : R2008 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1009 : 2013 | Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry |
| ASTM C 1156 : 2003 | Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials |
| ASTM C 1009 : 2006 | Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
| ASTM C 1297 : 2018 | Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials |
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