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ASTM C 1274 : 2012

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Advanced Ceramic Specific Surface Area by Physical Adsorption
Available format(s)

Hardcopy , PDF

Superseded date

05-15-2020

Language(s)

English

Published date

08-01-2012

1.1This test method covers the determination of the surface area of advanced ceramic materials (in a solid form) based on multilayer physisorption of gas in accordance with the method of Brunauer, Emmett, and Teller (BET) (1)2 and based on IUPAC Recommendations (1984 and 1994) (2) and (3). This test method specifies general procedures that are applicable to many commercial physical adsorption instruments. This test method provides specific sample outgassing procedures for selected common ceramic materials, including: amorphous and crystalline silicas, TiO2, kaolin, silicon nitride, silicon carbide, zirconium oxide, etc. The multipoint BET (1) equation along with the single point approximation of the BET equation are the basis for all calculations. This test method is appropriate for measuring surface areas of advanced ceramic powders down to at least 0.05 m2  (if in addition to nitrogen, krypton at 77.35 K is utilized as an adsorptive).

1.2This test method does not include all existing procedures appropriate for outgassing of advanced ceramic materials. However, it provides a comprehensive summary of procedures recommended in the literature for selected types of ceramic materials. The investigator shall determine the appropriateness of listed procedures.

1.3The values stated in SI units are to be regarded as standard. State all numerical values in terms of SI units unless specific instrumentation software reports surface area using alternate units. In this case, provide both reported and equivalent SI units in the final written report. It is commonly accepted and customary (in physical adsorption and related fields) to report the (specific) surface area of solids as m2/g, and, as a convention, many instruments (as well as certificates of reference materials) report surface area as m2 g-1, instead of using SI units (m2 kg-1).

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
C 28
DocumentType
Test Method
Pages
12
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM F 2883 : 2011 Standard Guide for Characterization of Ceramic and Mineral Based Scaffolds used for Tissue-Engineered Medical Products (TEMPs) and as Device for Surgical Implant Applications (Withdrawn 2020)
ASTM C 781 : 2018 Standard Practice for Testing Graphite Materials for Gas-Cooled Nuclear Reactor Components
ASTM C 1793 : 2015 Standard Guide for Development of Specifications for Fiber Reinforced Silicon Carbide-Silicon Carbide Composite Structures for Nuclear Applications
ASTM C 757 : 2016 : EDT 1 Standard Specification for Nuclear-Grade Plutonium Dioxide Powder for Light Water Reactors
ASTM C 1783 : 2015 Standard Guide for Development of Specifications for Fiber Reinforced Carbon-Carbon Composite Structures for Nuclear Applications

ASTM D 1993 : 1991 : R1997 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption
ASTM D 1993 : 2003 : R2013 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption
ASTM D 1993 : 2003 : R2008 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption
ASTM D 1993 : 2018 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption
ASTM D 1993 : 2003 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption
ASTM D 1993 : 2003 : R2013 : EDT 1 Standard Test Method for Precipitated Silica-Surface Area by Multipoint BET Nitrogen Adsorption

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