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ASTM D 4177 : 2016 : EDT 1

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
Available format(s)

Hardcopy , PDF

Superseded date

11-19-2020

Language(s)

English

Published date

03-31-2017

1.1This practice describes general procedures and equipment for automatically obtaining samples of liquid petroleum and petroleum products, crude oils, and intermediate products from the sample point into the primary container. This practice also provides additional specific information about sample container selection, preparation, and sample handling. If sampling is for the precise determination of volatility, use Practice D5842 (API MPMS Chapter 8.4) in conjunction with this practice. For sample mixing and handling, refer to Practice D5854 (API MPMS Chapter 8.3). This practice does not cover sampling of electrical insulating oils and hydraulic fluids.

1.2Table of Contents:

Section

INTRODUCTION

Scope

1

Referenced Documents

2

Terminology

3

Significance and Use

4

PART I–GENERAL

Representative Sampling Components

5

Design Criteria

6

Automatic Sampling Systems

7

Sampling Location

8

Mixing of the Flowing Stream

9

Proportionality

10

Sample Extractor Grab Volume

11

Containers

12

Sample Handling and Mixing

13

Control Systems

14

Sample System Security

15

System Proving (Performance Acceptance Tests)

16

Performance Monitoring

17

PART II–CRUDE OIL

Crude Oil

18

PART III–REFINED PRODUCTS

Refined Products

19

KEYWORDS

Keywords

20

ANNEXES

Calculations of the Margin of Error based on Number of Sample Grabs

Annex A1

Theoretical Calculations for Selecting the Sampler Probe Location

Annex A2

Performance Criteria for Portable Sampling Units

Annex A3

Profile Performance Test

Annex A4

Sampler Acceptance Test Data

Annex A5

APPENDIXES

Design Data Sheet for Automatic Sampling System

Appendix X1

Comparisons of Percent Sediment and Water versus Unloading Time Period

Appendix X2

1.3Units—The values stated in either SI units or US Customary (USC) units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Except where there is no direct SI equivalent, such as for National Pipe Threads/diameters, or tubing.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Standard Practice
Pages
45
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 7060 : 2012 : R2014 Standard Test Method for Determination of the Maximum Flocculation Ratio and Peptizing Power in Residual and Heavy Fuel Oils (Optical Detection Method)
ASTM D 7827 : 2012 : R2017 Standard Test Method for Measuring n-Heptane Induced Phase Separation of Asphaltene from Heavy Fuel Oils as Separability Number by an Optical Device
ASTM D 93 : 2018 Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester
ASTM D 3828 : 2016 : REV A Standard Test Methods for Flash Point by Small Scale Closed Cup Tester
ASTM D 7683 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Small Test Jar Method)
ASTM D 5863 : 2000 : REV A : R2016 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 7794 : 2018 : REV A Standard Practice for Blending Mid-Level Ethanol Fuel Blends for Flexible-Fuel Vehicles with Automotive Spark-Ignition Engines
ASTM D 7797 : 2018 Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method
ASTM D 2982 : 2007 : R2013 Standard Test Methods for Detecting Glycol-Base Antifreeze in Used Lubricating Oils
ASTM D 4377 : 2000 : R2011 Standard Test Method for Water in Crude Oils by Potentiometric Karl Fischer Titration (Withdrawn 2020)
ASTM D 7261 : 2017 Standard Test Method for Determining Water Separation Characteristics of Diesel Fuels by Portable Separometer
ASTM D 8009 : 2015 Standard Practice for Manual Piston Cylinder Sampling for Volatile Crude Oils, Condensates, and Liquid Petroleum Products
ASTM D 1018 : 2011 : R2016 Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021)
ASTM D 7689 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Mini Method)
ASTM D 8120 : 2017 Standard Test Method for Ferrous Debris Quantification
ASTM D 6079 : 2018 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR)
ASTM D 5708 : 2015 Standard Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry
ASTM D 189 : 2006 : R2014 Standard Test Method for Conradson Carbon Residue of Petroleum Products
ASTM D 5797 : 2018 Standard Specification for Methanol Fuel Blends (M51–M85) for Methanol-Capable Automotive Spark-Ignition Engines
ASTM D 7579 : 2009 : R2019 Standard Test Method for Pyrolysis Solids Content in Pyrolysis Liquids by Filtration of Solids in Methanol
ASTM D 3120 : 2008 : R2019 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 2622 : 2016 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 6595 : 2017 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 5761 : 1996 : R2017 Standard Practice for Emulsification/Suspension of Multiphase Fluid Waste Materials
ASTM D 7524 : 2010 : R2015 Standard Test Method for Determination of Static Dissipater Additives (SDA) in Aviation Turbine Fuel and Middle Distillate Fuels—High Performance Liquid Chromatograph (HPLC) Method
ASTM D 7061 : 2017 Standard Test Method for Measuring n-Heptane Induced Phase Separation of Asphaltene-Containing Heavy Fuel Oils as Separability Number by an Optical Scanning Device
ASTM D 6378 : 2018 : REV A Standard Test Method for Determination of Vapor Pressure (VP<inf>X</inf>) of Petroleum Products, Hydrocarbons, and Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method)
ASTM D 613 : 2018 : REV A Standard Test Method for Cetane Number of Diesel Fuel Oil
ASTM D 91 : 2002 : R2019 Standard Test Method for Precipitation Number of Lubricating Oils
ASTM D 86 : 2018 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 5304 : 2015 Standard Test Method for Assessing Middle Distillate Fuel Storage Stability by Oxygen Overpressure
ASTM D 6890 : 2018 Standard Test Method for Determination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustion in a Constant Volume Chamber
ASTM D 808 : 2016 Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) (Withdrawn 2021)
ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants
ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 7806 : 2012 Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy
ASTM D 7094 : 2017 : REV A Standard Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester
ASTM D 7960 : 2018 Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Non-hydrocarbon Components
ASTM D 2709 : 2016 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
ASTM D 6078 : 2004 : R2016 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the Scuffing Load Ball-on-Cylinder Lubricity Evaluator (SLBOCLE) (Withdrawn 2021)
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM D 4539 : 2017 Standard Test Method for Filterability of Diesel Fuels by Low-Temperature Flow Test (LTFT)
ASTM D 7669 : 2015 Standard Guide for Practical Lubricant Condition Data Trend Analysis
ASTM D 3143/D3143M : 2019 Standard Test Method for Flash Point of Cutback Asphalt with Tag Open-Cup Apparatus
ASTM D 6074 : 2015 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 2068 : 2017 Standard Test Method for Determining Filter Blocking Tendency
ASTM D 6624 : 2019 Standard Practice for Determining a Flow-Proportioned Average Property Value (FPAPV) for a Collected Batch of Process Stream Material Using Stream Analyzer Data
ASTM D 7740 : 2011 : R2016 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
ASTM D 2700 : 2019 Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel
ASTM D 7591 : 2012 : R2017 Standard Test Method for Determination of Free and Total Glycerin in Biodiesel Blends by Anion Exchange Chromatography
ASTM D 5772 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)
ASTM D 6426 : 2018 Standard Test Method for Determining Filterability of Middle Distillate Fuel Oils
ASTM D 6730 : 2001 : R2016 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
ASTM D 5983 : 2018 Standard Specification for Methyl Tertiary-Butyl Ether (MTBE) for Blending With Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 7416 : 2009 : R2015 Standard Practice for Analysis of In-Service Lubricants Using a Particular Five-Part (Dielectric Permittivity, Time-Resolved Dielectric Permittivity with Switching Magnetic Fields, Laser Particle Counter, Microscopic Debris Analysis, and Orbital Viscometer) Integrated Tester
ASTM D 2892 : 2018 : REV A Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
ASTM D 7671 : 2010 : R2015 Standard Test Method for Corrosiveness to Silver by Automotive Spark–Ignition Engine Fuel–Silver Strip Method
ASTM D 6892 : 2003 : R2014 Standard Test Method for Pour Point of Petroleum Products (Robotic Tilt Method)
ASTM D 5773 : 2017 : EDT 1 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Constant Cooling Rate Method)
ASTM D 6824 : 2013 : R2018 Standard Test Method for Determining Filterability of Aviation Turbine Fuel
ASTM D 8254 : 2019 Standard Test Method for Flash and Fire Points of Asphalt by Cleveland Open Cup Tester
ASTM D 6560 : 2017 Standard Test Method for Determination of Asphaltenes (Heptane Insolubles) in Crude Petroleum and Petroleum Products
ASTM D 7547 : 2018 : REV A Standard Specification for Hydrocarbon Unleaded Aviation Gasoline
ASTM D 524 : 2015 Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products
ASTM D 3227 : 2016 Standard Test Method for (Thiol Mercaptan) Sulfur in Gasoline, Kerosine, Aviation Turbine, and Distillate Fuels (Potentiometric Method)
ASTM D 1093 : 2011 : R2017 Standard Test Method for Acidity of Hydrocarbon Liquids and Their Distillation Residues
ASTM D 7236 : 2016 : REV A Standard Test Method for Flash Point by Small Scale Closed Cup Tester (Ramp Method)
ASTM D 130 : 2019 Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test
ASTM D 8049 : 2019 Standard Test Method for Determining Concentration, Count, and Size Distribution of Solid Particles and Water in Light and Middle Distillate Fuels by Direct Imaging Analyzer
ASTM D 8166 : 2017 Standard Test Method for Sizing and Counting Particulates in Light and Middle Distillate Fuels and Biodiesel Blend (B6 to B20) Using Continuous Flow and Bottle Sampler Automatic Particle Counters
ASTM D 7946 : 2014 Standard Test Method for Initial pH (i-pH)-Value of Petroleum Products
ASTM D 3607 : 2008 : R2016 Standard Test Method for Removing Volatile Contaminants from Used Engine Oils by Stripping (Withdrawn 2022)
ASTM D 6793 : 2002 : R2012 Standard Test Method for Determination of Isothermal Secant and Tangent Bulk Modulus (Withdrawn 2021)
ASTM D 7622 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 7545 : 2014 Standard Test Method for Oxidation Stability of Middle Distillate Fuels—Rapid Small Scale Oxidation Test (RSSOT)
ASTM D 2386 : 2019 Standard Test Method for Freezing Point of Aviation Fuels
ASTM D 7662 : 2015 Standard Test Method for Carbon Content in Carbon Black Feedstock Oils
ASTM D 7170 : 2016 Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Fixed Range Injection Period, Constant Volume Combustion Chamber Method (Withdrawn 2019)
ASTM D 5985 : 2002 : R2014 Standard Test Method for Pour Point of Petroleum Products (Rotational Method)
ASTM D 4294 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 7666 : 2012 Standard Specification for Triglyceride Burner Fuel
ASTM D 322 : 1997 : R2016 Standard Test Method for Gasoline Diluent in Used Gasoline Engine Oils by Distillation (Withdrawn 2022)
ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
ASTM D 7346 : 2015 Standard Test Method for No Flow Point and Pour Point of Petroleum Products and Liquid Fuels
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
ASTM D 1160 : 2018 Standard Test Method for Distillation of Petroleum Products at Reduced Pressure
ASTM D 3605 : 2017 Standard Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy
ASTM D 6371 : 2017 : REV A Standard Test Method for Cold Filter Plugging Point of Diesel and Heating Fuels
ASTM D 3231 : 2018 Standard Test Method for Phosphorus in Gasoline
ASTM D 4929 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 4814 : 2019 Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D 6443 : 2014 : R2019 : EDT 1 Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
ASTM D 7483 : 2013 : REV A : R2017 Standard Test Method for Determination of Dynamic Viscosity and Derived Kinematic Viscosity of Liquids by Oscillating Piston Viscometer
ASTM D 4735 : 2019 Standard Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography
ASTM D 7153 : 2015 : EDT 1 Standard Test Method for Freezing Point of Aviation Fuels (Automatic Laser Method)
ASTM D 2885 : 2019 : REV A Standard Test Method for Determination of Octane Number of Spark-Ignition Engine Fuels by On-Line Direct Comparison Technique
ASTM D 7397 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Miniaturized Optical Method)
ASTM D 6470 : 1999 : R2015 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 7345 : 2017 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Micro Distillation Method)
ASTM D 2699 : 2019 Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 7551 : 2010 : R2015 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases and Natural Gas by Ultraviolet Fluorescence
ASTM D 4625 : 2016 : EDT 1 Standard Test Method for Middle Distillate Fuel Storage Stability at 43 °C (110 °F)
ASTM D 2274 : 2014 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
ASTM D 3831 : 2012 : R2017 Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
ASTM D 5853 : 2017 : REV A Standard Test Method for Pour Point of Crude Oils
ASTM D 4806 : 2019 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 483 : 2004 : R2018 Standard Test Method for Unsulfonated Residue of Petroleum Plant Spray Oils
ASTM D 8073 : 2016 Standard Test Method for Determination of Water Separation Characteristics of Aviation Turbine Fuel by Small Scale Water Separation Instrument
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 7923 : 2019 Standard Test Method for Water in Ethanol and Hydrocarbon Blends by Karl Fischer Titration
ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 7843 : 2018 Standard Test Method for Measurement of Lubricant Generated Insoluble Color Bodies in In-Service Turbine Oils using Membrane Patch Colorimetry
ASTM D 1318 : 2016 Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method)
ASTM D 1266 : 2018 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
ASTM D 4739 : 2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
ASTM D 7757 : 2017 Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 7679 : 2016 Standard Test Method for Sulfur Content in Carbon Black Feedstock Oils
ASTM D 4807 : 2005 : R2015 Standard Test Method for Sediment in Crude Oil by Membrane Filtration
ASTM D 6728 : 2016 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM E 1655 : 2017 Standard Practices for Infrared Multivariate Quantitative Analysis
ASTM D 1091 : 2011 : R2016 Standard Test Methods for Phosphorus in Lubricating Oils and Additives (Withdrawn 2021)
ASTM D 7235 : 2016 Standard Guide for Establishing a Linear Correlation Relationship Between Analyzer and Primary Test Method Results Using Relevant ASTM Standard Practices
ASTM D 7220 : 2012 : R2017 Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 7667 : 2010 : R2015 Standard Test Method for Determination of Corrosiveness to Silver by Automotive Spark-Ignition Engine Fuel—Thin Silver Strip Method
ASTM D 2273 : 2008 : R2016 Standard Test Method for Trace Sediment in Lubricating Oils (Withdrawn 2023)
ASTM D 3341 : 2016 Standard Test Method for Lead in Gasoline—Iodine Monochloride Method (Withdrawn 2022)
ASTM D 7620 : 2010 : R2015 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection
ASTM D 7451 : 2016 Standard Test Method for Water Separation Properties of Light and Middle Distillate, and Compression and Spark Ignition Fuels
ASTM D 3237 : 2017 Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 6756 : 2017 Standard Test Method for Determination of the Red Dye Concentration and Estimation of the ASTM Color of Diesel Fuel and Heating Oil Using a Portable Visible Spectrophotometer
ASTM D 4055 : 2004 : R2019 Standard Test Method for Pentane Insolubles by Membrane Filtration
ASTM D 4808 : 2017 Standard Test Methods for Hydrogen Content of Light Distillates, Middle Distillates, Gas Oils, and Residua by Low-Resolution Nuclear Magnetic Resonance Spectroscopy
ASTM E 3050 : 2016 Standard Specification for Denatured Ethanol for Use as Cooking and Appliance Fuel
ASTM D 8076 : 2018 Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
ASTM D 8148 : 2017 Standard Test Method for Spectroscopic Determination of Haze in Fuels
ASTM D 7525 : 2014 Standard Test Method for Oxidation Stability of Spark Ignition Fuel—Rapid Small Scale Oxidation Test (RSSOT)
ASTM D 7596 : 2014 Standard Test Method for Automatic Particle Counting and Particle Shape Classification of Oils Using a Direct Imaging Integrated Tester
ASTM D 396 : 2019 Standard Specification for Fuel Oils
ASTM D 5184 : 2012 : R2017 Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
ASTM D 7041 : 2016 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection
ASTM D 6448 : 2016 Standard Specification for Industrial Burner Fuels from Used Lubricating Oils
ASTM D 6377 : 2016 Standard Test Method for Determination of Vapor Pressure of Crude Oil: VPCR<inf>x</inf > (Expansion Method)
ASTM D 6898 : 2003 : R2016 Standard Test Method for Evaluating Diesel Fuel Lubricity by an Injection Pump Rig (Withdrawn 2021)
ASTM D 4530 : 2015 Standard Test Method for Determination of Carbon Residue (Micro Method)
ASTM D 6450 : 2016 : REV A Standard Test Method for Flash Point by Continuously Closed Cup (CCCFP) Tester
ASTM D 7317 : 2007 : R2019 Standard Test Method for Coagulated Pentane Insolubles in Used Lubricating Oils by Paper Filtration (LMOA Method)
ASTM D 5949 : 2016 Standard Test Method for Pour Point of Petroleum Products (Automatic Pressure Pulsing Method)
ASTM D 7318 : 2019 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 7039 : 2015 : REV A Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 5439 : 1995 : R2012 Standard Test Method for Determination of Sediment in Moellon
ASTM D 6823 : 2008 : R2013 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
ASTM D 6621 : 2000 : R2017 Standard Practice for Performance Testing of Process Analyzers for Aromatic Hydrocarbon Materials
ASTM D 7688 : 2018 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR) by Visual Observation
ASTM D 5291 : 2016 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants
ASTM D 7214 : 2007 : REV A : R2012 Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation
ASTM D 5771 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Optical Detection Stepped Cooling Method)
ASTM D 7719 : 2018 Standard Specification for High Aromatic Content Unleaded Hydrocarbon Aviation Gasoline
ASTM D 7344 : 2017 : REV A Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Mini Method)
ASTM D 8183 : 2018 Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method
ASTM D 5984 : 2011 : R2017 Standard Test Method for Semi-Quantitative Field Test Method for Base Number in New and Used Lubricants by Color-Indicator Titration
ASTM D 7112 : 2019 Standard Test Method for Determining Stability and Compatibility of Heavy Fuel Oils and Crude Oils by Heavy Fuel Oil Stability Analyzer (Optical Detection)
ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 8150 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 92 : 2018 Standard Test Method for Flash and Fire Points by Cleveland Open Cup Tester
ASTM D 5950 : 2014 Standard Test Method for Pour Point of Petroleum Products (Automatic Tilt Method)
ASTM D 7623 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion-Gold Amalgamation and Cold Vapor Atomic Absorption Method
ASTM D 1552 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 7619 : 2017 Standard Test Method for Sizing and Counting Particles in Light and Middle Distillate Fuels, by Automatic Particle Counter
ASTM D 8127 : 2017 : EDT 1 Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants
ASTM D 7154 : 2015 Standard Test Method for Freezing Point of Aviation Fuels (Automatic Fiber Optical Method)
ASTM D 7279 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer
ASTM D 7419 : 2018 Standard Test Method for Determination of Total Aromatics and Total Saturates in Lube Basestocks by High Performance Liquid Chromatography (HPLC) with Refractive Index Detection
ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 910 : 2017 : REV A Standard Specification for Leaded Aviation Gasolines
ASTM D 94 : 2007 : R2017 Standard Test Methods for Saponification Number of Petroleum Products
ASTM D 6304 : 2016 : EDT 1 Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration
ASTM D 5622 : 2017 Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis
ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 6822 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, and API Gravity of Crude Petroleum and Liquid Petroleum Products by Thermohydrometer Method
ASTM D 7095 : 2017 Standard Test Method for Rapid Determination of Corrosiveness to Copper from Petroleum Products Using a Disposable Copper Foil Strip

ASTM D 4840 : 1999 : R2018 : EDT 1 Standard Guide for Sample Chain-of-Custody Procedures
ASTM D 4007 : 1981 : R1995 : EDT 1 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 4007 : 2011 : R2016 : EDT 1 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 4928 : 2000 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
ASTM D 4007 : 2002 : R2006 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 5842 : 2014 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement
ASTM D 5854 : 1996 : R2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 5842 : 2004 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement
ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 5854 : 1996 : R2005 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 5842 : 1995 : R2000 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement
ASTM D 4928 : 2000 : EDT 1 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4928 : 2000 : R2010 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4928 : 2000 : R2005 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4007 : 2002 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 5842 : 2004 : R2009 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement
ASTM D 4007 : 2008 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 5854 : 1996 : R2000 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 4007 : 2011 : R2016 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 4928 : 2011 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4007 : 2011 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 4928 : 2012 : R2018 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 5842 : 2017 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement
ASTM D 4928 : 2012 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D 4007 : 2011 : EDT 1 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)
ASTM D 5854 : 1996 : R2015 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products

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  • Simple online access to standards, technical information and regulations.

  • Critical updates of standards and customisable alerts and notifications.

  • Multi-user online standards collection: secure, flexible and cost effective.