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ASTM D 4928 : 2012 : R2018

Current
Current

The latest, up-to-date edition.

Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

07-01-2018

1.1This test method covers the determination of water in the range from 0.02 to 5.00 mass or volume % in crude oils. Mercaptan (RSH) and sulfide (S or H2S) as sulfur are known to interfere with this test method, but at levels of less than 500 μg/g [ppm(m)], the interference from these compounds is insignificant (see Section 6).

1.2This test method can be used to determine water in the 0.005 to 0.02 mass % range, but the effects of the mercaptan and sulfide interference at these levels has not been determined. For the range 0.005 to 0.02 mass %, there is no precision or bias statement.

1.3This test method is intended for use with standard commercially available coulometric Karl Fischer reagent.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 8.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
6
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 6470 : 1999 : R2015 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 7059 : 2009 : R2017 Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography
ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 7829 : 2013 : R2018 Standard Guide for Sediment and Water Determination in Crude Oil
ASTM D 3230 : 2019 Standard Test Method for Salts in Crude Oil (Electrometric Method)
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM E 203 : 2016 Standard Test Method for Water Using Volumetric Karl Fischer Titration

ASTM E 203 : 2023 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM E 203 : 2024 Standard Test Method for Water Using Volumetric Karl Fischer Titration

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