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ASTM D 5542 : 2016 : REDLINE

Current
Current

The latest, up-to-date edition.

Standard Test Methods for Trace Anions in High Purity Water by Ion Chromatography
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PDF

Language(s)

English

Published date

06-01-2016

CONTAINED IN VOL. 11.01, 2017 Defines the determination of trace ([mu]g/L) levels of fluoride, acetate, formate, chloride, phosphate, and sulfate in high purity water using ion chromatography in combination with sample preconcentration.

1.1These test methods cover the determination of trace (μg/L) levels of fluoride, acetate, formate, chloride, phosphate, and sulfate in high purity water using ion chromatography in combination with sample preconcentration. Other anions, such as bromide, nitrite, nitrate, sulfite, and iodide can be determined by this method. However, since they are rarely present in significant concentrations in high purity water, they are not included in this test method. Two test methods are presented and their ranges of application, as determined by a collaborative study, are as follows:

Range Tested
(μg/L Added)

Limit of DetectionA
(Single Operator)
(μg/L)

Sections

Test Method A:

716

 Chloride

0–24 

0.8

 Phosphate

0–39 

B

 Sulfate

0–55 

1.8

Test Method B:

1724

 Fluoride

0–14 

0.7

 Acetate

0–414

6.8

 Formate

0–346

5.6

(A)Limit of detection is lowest measurable concentration not reportable as zero at 99 % level of confidence as per EPRI study as cited in Sections 16 and 24.
(B)Insufficient data to calculate limit of detection.

1.2It is the user's responsibility to ensure the validity of these test methods for waters of untested matrices.

1.3The common practical range of Test Method A is as follows: chloride, 1 to 100 μg/L, phosphate, 3 to 100 μg/L, and sulfate, 2 to 100 μg/L.

1.4The common practical range of Test Method B is as follows: fluoride, 1 to 100 μg/L, acetate, 10 to 200 μg/L, and formate, 5 to 200 μg/L.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 19
DocumentType
Redline
Pages
16
PublisherName
American Society for Testing and Materials
Status
Current

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