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ASTM D 7521 : 2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of Asbestos in Soil
Available format(s)

Hardcopy , PDF

Superseded date

07-25-2022

Language(s)

English

Published date

06-02-2016

1.1This test method covers a procedure to: (1) identify asbestos in soil, (2) provide an estimate of the concentration of asbestos in the sampled soil (dried), and (3) optionally to provide a concentration of asbestos reported as the number of asbestos structures per gram of sample.

1.2In this test method, results are produced that may be used for evaluation of sites contaminated by construction, mine and manufacturing wastes, deposits of natural occurrences of asbestos (NOA), and other sources of interest to the investigator.

1.3This test method describes the gravimetric, sieve, and other laboratory procedures for preparing the soil for analysis as well as the identification and quantification of any asbestos detected. Pieces of collected soil and material embedded therein that pass through a 19-mm sieve will become part of the sample that is analyzed and for which results are reported.

1.3.1Asbestos is identified and quantified by polarized light microscopy (PLM) techniques including analysis of morphology and optical properties. Optional transmission electron microscopy (TEM) identification and quantification of asbestos is based on morphology, selected area electron diffraction (SAED), and energy dispersive X-ray analysis (EDXA). Some information about fiber size may also be determined. The PLM and TEM methods use different definitions and size criteria for fibers and structures. Separate data sets may be produced.

1.4This test method has an analytical sensitivity of 0.25 % by weight with optional procedures to allow for an analytical sensitivity of 0.1 % by weight.

1.5This test method does not purport to address sampling strategies or variables associated with soil environments. Such considerations are the responsibility of the investigator collecting and submitting the sample. Appendix X2 covering elements of soil sampling and good field practices is attached.

1.6Units—The values stated in SI units are to be regarded as the standard. Other units may be cited in the method for informational purposes only.

1.7Hazards—Asbestos fibers are acknowledged carcinogens. Breathing asbestos fibers can result in disease of the lungs including asbestosis, lung cancer, and mesothelioma. Precautions should be taken to avoid creating and breathing airborne asbestos particles when sampling and analyzing materials suspected of containing asbestos.

1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 22
DocumentType
Test Method
Pages
14
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM E 2356 : 2018 Standard Practice for Comprehensive Building Asbestos Surveys
ASTM E 1368 : 2014 Standard Practice for Visual Inspection of Asbestos Abatement Projects

ASTM E 11 : 2020 Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM D 3670 : 1991 : R1996 : EDT 1 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 6281 : 2004 Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)
ASTM D 6281 : 1998 Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 6281 : 2009 Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 11 : 2022 Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves
ASTM D 6620 : 2006 Standard Practice for Asbestos Detection Limit Based on Counts
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 6620 : 2006 : R2010 Standard Practice for Asbestos Detection Limit Based on Counts
ASTM D 3670 : 1991 : R2014 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 6620 : 2019 Standard Practice for Asbestos Detection Limit Based on Counts
ASTM D 3670 : 1991 : R2001 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 6281 : 2006 Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3670 : 1991 : R2007 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM C 136 : 1996 Standard Test Method for Sieve Analysis of Fine and Coarse Aggregates
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 6620 : 2000 Standard Practice for Asbestos Detection Limit Based on Counts
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 6281 : 2015 Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)

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