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ASTM E 200 : 2016 : REDLINE

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis
Available format(s)

PDF

Superseded date

07-17-2023

Language(s)

English

Published date

07-27-2018

CONTAINED IN VOL. 15.05, 2017 Defines procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.

1.1This practice covers procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.

1.2The information in this practice is arranged as follows:

Sections

Referenced Documents

2

Terminology

3

Significance and Use

4

Apparatus

5

Temperature effects

6

Measurements

7

Reagents

8

Concentration of solutions

9

Mixing of solutions

10

Storage of solutions

11

Preparation and standardization of solutions

12

Precision and Bias

13

Sodium hydroxide solution, 0.02 to 1.0 meq/mL (N)

14 to 19

Hydrochloric acid, 0.02 to 1.0 meq/mL (N)

20 to 28

Sulfuric acid, 0.02 to 1.0 meq/mL (N)

29 to 33

Hydrochloric acid, special 1 meq/mL (N)

34 to 38

Sulfuric acid, special 1 meq/mL (N)

39 to 43

Silver nitrate solution, 0.1 meq/mL (N)

44 to 48

Ammonium thiocyanate solution, 0.1 meq/mL (N)

49 to 53

Iodine solution, 0.1 meq/mL (N)

54 to 58

Sodium thiosulfate solution, 0.1 meq/mL (N)

59 to 63

Potassium permanganate solution, 0.1 meq/mL (N)

64 to 68

Potassium dichromate solution, 0.1 meq/mL(N)

69 to 73

Methanolic sodium hydroxide solution, 0.5 meq/mL (N)

74 to 79

Ceric sulfate solution, 0.1 meq/mL (N)

80 to 84

Acetous perchloric acid, 0.1 meq/mL (N)

85 to 89

Disodium ethylenediaminetetraacetate solution, 0.05 mol/L(M)

90 to 94

Standard ion solutions

95

Nonstandardized reagent solutions and indicator solutions

96

1.3The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given throughout this practice.

Committee
D 16
DocumentType
Redline
Pages
16
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

Standards Relationship
UNE 55539-8:1994 Identical
UNE 55539-12:1995 Identical
UNE 55539-9:1994 Identical
UNE 55539-10:1994 Identical
UNE 55539-13:1995 Identical
UNE 55539-3:1994 Identical
UNE 55539-11:1994 Identical
UNE 55539-4:1994 Identical
UNE 55539-5:1994 Identical
UNE 55539-6:1994 Identical
UNE 55539-7:1994 Identical
UNE 55539-2:1994 Identical

ASTM D 3566 : 2003 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
ASTM D 5788 : 1995 : R2005 Standard Guide for Spiking Organics into Aqueous Samples
ASTM E 1910/E1910M : 2015 : REDLINE Standard Test Method for Agricultural pH Control Agents, Measurement of pH Change and Buffering Capacity
ASTM E 449:2008 Standard Test Methods for Analysis of Calcium Chloride
ASTM D 297 : 2015 : REDLINE Standard Test Methods for Rubber Products—Chemical Analysis
ASTM D 6363 : 1998 : R2003 : EDT 1 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
ASTM D 3546 : 2005 : R2011 Standard Test Method for Formic Acid in Glacial Acetic Acid
ASTM D 2790 : 1983 Methods of Analysis of Solvent Systems Used for Removal of Water-Formed Deposits (Withdrawn 1993)
ASTM D 4274 : 2016 : REDLINE Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
ASTM E 271 : 1998 Standard Test Methods for Analysis of Aqueous Hydrofluoric Acid (Withdrawn 2003)
ASTM D 2192 : 2006 : R2012 Standard Test Method for Purity of Aldehydes and Ketones (Withdrawn 2021)
ASTM D 3316 : 2006 Standard Test Method for Stability of Perchloroethylene with Copper
ASTM D 1614 : 2009 : R2017 Standard Test Method for Alkalinity in Acetone
ASTM D 4856 : 2011 Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis)
ASTM D 888 : 2012-05 TEST METHODS FOR DISSOLVED OXYGEN IN WATER
ASTM E 258 : 2007 : R2015 Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method (Withdrawn 2019)
ASTM D 3316 : 2006 : R2016 Standard Test Method for Stability of Perchloroethylene with Copper
ASTM E 1584 : 2017 : REDLINE Standard Test Method for Assay of Nitric Acid
ASTM C 574 : 1984 : R1988 Method for Chemical Analyisis of Magnesite and Dolomite Refractories
ASTM E 1147 : 1992 : R2005 Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography (Withdrawn 2013)
ASTM D 2106 : 2007 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
ASTM D 5810 : 1996 : R2011 Standard Guide for Spiking into Aqueous Samples
ASTM D 3249 : 1995 : R2000 Standard Practice for General Ambient Air Analyzer Procedures
ASTM D 4252 : 1989 : R2017 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 5788 : 1995 Standard Guide for Spiking Organics into Aqueous Samples
ASTM D 3089 : 1997 : R2008 Standard Practice for Determining the A-D Dimension of Aerosol Valve Dip Tubes
ASTM D 2086 : 2008 Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde
ASTM D 6363 : 1998 : R2013 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
ASTM D 1417 : 2016 : REDLINE Standard Test Methods for Rubber Latices—Synthetic
ASTM D 2086 : 2008 : R2012 Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde (Withdrawn 2021)
ASTM D 1942 : 1980 Method of Test for Morpholine in Water
ASTM D 5788 : 1995 : R2017 Standard Guide for Spiking Organics into Aqueous Samples
ASTM E 1547 : 2009 Standard Terminology Relating to Industrial and Specialty Chemicals
ASTM D 5916 : 1996 : R2002 Standard Test Method for Detection and Enumeration of <i>Clostridium perfringens</i> from Water and Extracted Sediments by Membrane Filtration (MF) (Withdrawn 2011)
ASTM D 6328 : 2012-11 GUIDE FOR QUALITY ASSURANCE PROTOCOLS FOR CHEMICAL ANALYSIS OF ATMOSPHERIC WET DEPOSITION
ASTM D 3316 : 2006 : R2011 Standard Test Method for Stability of Perchloroethylene with Copper
ASTM D 1141 : 1998 : R2013 Standard Practice for the Preparation of Substitute Ocean Water
ASTM D 2912 : 1976 : R1983 Test Method for Oxidant Content of the Atmosphere (Neutral KI) (Withdrawn 1990)
ASTM D 3228 : 2008 : R2014 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
MIL H 6083 : E HYDRAULIC FLUID, PETROLEUM BASE, FOR PRESERVATION AND OPERATION
ASTM D 4252 : 1989 : R1995 : EDT 1 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 5788 : 1995 : R2001 Standard Guide for Spiking Organics into Aqueous Samples
ASTM E 1788 : 2016 : REDLINE Standard Test Method for Acidity in Acrylonitrile
ASTM D 512 : 2012 Standard Test Methods for Chloride Ion In Water (Withdrawn 2021)
MIL-D-22346 Revision B:1973 DI-NORMAL-PROPYL ADIPATE (DNPA)
ASTM E 442 : 1991 Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997)
ASTM D 3566 : 2003 : R2009 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
ASTM D 5788 : 1995 : R2011 Standard Guide for Spiking Organics into Aqueous Samples
ASTM D 4415 : 2005 Standard Test Methods for Determination of Dimer in Acrylic Acid (Withdrawn 2011)
ASTM D 6363 : 1998 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
ASTM D 4224 : 1989 Test Method for Anionic Detergent by Para-Toluidine Hydrochloride (Withdrawn 1995)
ASTM D 3566 : 2003 : R2014 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
ASTM D 2379 : 2009 Standard Test Method for Acidity of Formaldehyde Solutions
ASTM D 6303 : 1998 Standard Test Method for Formaldehyde in Water (Withdrawn 2007)
ASTM D 1387 : 1989 : R2002 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
ASTM D 6470 : 1999 : R2015 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 3634 : 1999 : EDT 1 Standard Test Method for Trace Chloride Ion in Engine Coolants
ASTM D 5810 : 1996 : R2006 Standard Guide for Spiking into Aqueous Samples
ASTM D 3634 : 1999 : R2005 Standard Test Method for Trace Chloride Ion in Engine Coolants
ASTM D 5810 : 1996 : R2015 Standard Guide for Spiking into Aqueous Samples
ASTM E 257 : 1998 Standard Test Method for Sulfur in Organic Compounds by Sodium Peroxide Bomb Ignition
ASTM D 345 : 2002 Side bearings of the freight wagon bogies. General specifications
ASTM D 1387 : 1989 : R2007 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
ASTM D 2942 : 2002 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
ASTM E 1615 : 2016 : REDLINE Standard Test Method for Iron in Trace Quantities Using the FerroZine Method
ASTM E 223 : 2016 : REDLINE Standard Test Methods for Analysis of Sulfuric Acid
ASTM D 2382 : 1988 Test Method for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method) (Withdrawn 1994)
ASTM D 4266 : 2017 : REDLINE Standard Test Methods for Precoat Capacity of Powdered Ion-Exchange Resins
ASTM E 1910 : 2004 Test Method for Agricultural pH Control Agents
ASTM D 240 : 2017 : REDLINE Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
ASTM E 441 : 1990 Test Method for Vinyl Unsaturation in Organic Compounds with Mercuric Acetate (Withdrawn 1996)
ASTM D 2106 : 2007 : R2017 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
ASTM D 1067 : 2016 : REDLINE Standard Test Methods for Acidity or Alkalinity of Water
ASTM D 1387 : 1989 : R2012 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
ASTM D 2942 : 2002 : R2013 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
ASTM E 567 : 1991 Test Method for Tertiary Hydroxyl Groups with Hydrogen Bromide (Withdrawn 1996)
ASTM D 3249 : 1995 : R2005 Standard Practice for General Ambient Air Analyzer Procedures
ASTM D 3634 : 1999 : R2015 Standard Test Method for Trace Chloride Ion in Engine Coolants
ASTM D 7389 : 2007 Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes
ASTM E 2677 : 2014 Standard Test Method for Determining Limits of Detection in Explosive Trace Detectors
ASTM D 2195 : 2005 Standard Test Methods for Pentaerythritol (Withdrawn 2011)
ASTM E 301 : 1994 Standard Test Method for Total Acidity of Organic Acids (Withdrawn 2001)
ASTM D 5810 : 1996 Standard Guide for Spiking into Aqueous Samples
ASTM D 7795 : 2015 : REDLINE Standard Test Method for Acidity in Ethanol and Ethanol Blends by Titration
ASTM E 449 : 2008 : R2013 Standard Test Methods for Analysis of Calcium Chloride
ASTM E 358 : 1995 Test Methods for Analysis of Phosphoric Acid (Withdrawn 2000)
ASTM D 3634 : 1999 : R2009 Standard Test Method for Trace Chloride Ion in Engine Coolants
AWWA B403 : 2016 ALUMINUM SULFATE - LIQUID, GROUND, OR LUMP
ASTM D 2106 : 2007 : R2012 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
ASTM E 819 : 1998 Standard Test Method for Trace Amounts of Arsenic in Organic Industrial Chemicals (Withdrawn 2003)
ASTM E 234 : 1998 Standard Test Method for Total Bromine Number of Unsaturated Aliphatic Chemicals
ASTM D 3546 : 2005 Standard Test Method for Formic Acid in Glacial Acetic Acid
ASTM D 3546 : 2005 : R2019 Standard Test Method for Formic Acid in Glacial Acetic Acid
ASTM D 1141 : 1998 : R2008 Standard Practice for the Preparation of Substitute Ocean Water
ASTM D 3228 : 2008 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
ASTM D 6470 : 1999 : R2010 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 1141 : 1998 : EDT 1 Standard Practice for the Preparation of Substitute Ocean Water
ASTM E 1228 : 2017 : REDLINE Standard Test Method for Assay of Peroxy Esters—Catalyzed Iodometric Procedure
ASTM D 513 : 2016 : REDLINE Standard Test Methods for Total and Dissolved Carbon Dioxide in Water
ASTM D 1614 : 2009 Standard Test Method for Alkalinity in Acetone
ASTM E 1547 : 2009 : R2017 Standard Terminology Relating to Industrial and Specialty Chemicals
ASTM D 7389 : 2007 : R2012 Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes
ASTM D 2942 : 2002 : R2008 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
ASTM D 5318 : 1997 Standard Test Method for Hydrolyzable Chloride in Peroxy Esters and Peroxy Dicarbonates (Withdrawn 2004)
ASTM D 3249 : 1995 : R2011 Standard Practice for General Ambient Air Analyzer Procedures
ASTM E 394 : 2015 : REDLINE Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
ASTM E 534 : 2013-11 TEST METHODS FOR CHEMICAL ANALYSIS OF SODIUM CHLORIDE
ASTM D 4252 : 1989 : R2003 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM D 4252 : 1989 : R2009 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
ASTM E 224 : 2016 : REDLINE Standard Test Methods for Analysis of Hydrochloric Acid
GOST 849:2018 Primary nickel. SpecificationsE
ASTM D 2192 : 2006 Standard Test Method for Purity of Aldehydes and Ketones
ASTM D 6363 : 1998 : R2009 : EDT 1 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
ASTM D 4249 : 1983 : R1998 Standard Test Method for Enumeration of <I>Candida albicans</I> in Water
ASTM E 222 : 2017 : REDLINE Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation
ASTM E 326 : 1996 Test Method for Hydroxyl Groups by Phthalic Anhydride Esterification (Withdrawn 2001)
ASTM D 4249 : 1983 : R2005 Standard Test Method for Enumeration of <I>Candida albicans</I> in Water (Withdrawn 2013)
ASTM E 335 : 1996 Standard Test Method for Hydroxyl Groups by Pyromellitic Dianhydride Esterification (Withdrawn 2003)
ASTM E 233 : 1990 Test Method for Assay of N-Butyllithium Solutions (Withdrawn 1996)
ASTM D 5810 : 1996 : R2001 Standard Guide for Spiking into Aqueous Samples
ASTM E 1147 : 1992 : R1997 Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography
ASTM D 1613 : 2017 : REDLINE Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM C 500/C500M : 2007 : R2011 : EDT 1 Standard Test Methods for Asbestos-Cement Pipe
ASTM D 3634 : 1999 : R2005 : EDT 1 Standard Test Method for Trace Chloride Ion in Engine Coolants
ASTM E 778 : 2015 : REDLINE Standard Test Methods for Nitrogen in Refuse-Derived Fuel Analysis Samples
ASTM D 1141 : 1998 : R2003 Standard Practice for the Preparation of Substitute Ocean Water
ASTM E 258 : 2007 Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method
ASTM D 5058 : 2012 : REDLINE Standard Practices for Compatibility of Screening Analysis of Waste
ASTM E 359 : 2017 : REDLINE Standard Test Methods for Analysis of Soda Ash (Sodium Carbonate)
ASTM D 1387 : 1989 : R1995 : EDT 1 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
ASTM D 1386 : 2015 : REDLINE Standard Test Method for Acid Number (Empirical) of Synthetic and Natural Waxes
ASTM D 6511/D6511M : 2011-07 TEST METHODS FOR SOLVENT BEARING BITUMINOUS COMPOUNDS
ASTM D 6470 : 1999 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 5916 : 1996 Standard Test Method for Detection and Enumeration of <i>Clostridium perfringens</i> from Water and Extracted Sediments by Membrane Filtration (MF)
ASTM C 25 : 2017 : REDLINE TEST METHODS FOR CHEMICAL ANALYSIS OF LIMESTONE, QUICKLIME, AND HYDRATED LIME
ASTM D 2379 : 2009 : R2017 Standard Test Method for Acidity of Formaldehyde Solutions
ASTM D 3875 : 2015 : REDLINE Standard Test Method for Alkalinity in Brackish Water, Seawater, and Brines
ASTM D 2106 : 2007 : EDT 1 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
ASTM D 6470 : 1999 : R2004 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
ASTM D 4856 : 2011 : R2016 Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis)

ASTM E 50 : 2017 : REDLINE Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 180 : 2003 Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009)
ASTM E 203 : 2016 : REDLINE Standard Test Method for Water Using Volumetric Karl Fischer Titration

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