ASTM E 3061 : 2017
Current
The latest, up-to-date edition.
Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based Method)
Hardcopy , PDF
English
01-15-2017
CONTAINED IN VOL. 03.05, 2017 Specifies the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys.
1.1This test method describes the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys for the following elements:
| Elements | Application Range, % | |
| Minimum | Maximum | |
| Si | 0.02 | 16.8 |
| Fe | 0.02 | 3.06 |
| Cu | 0.005 | 7.0 |
| Mn | 0.003 | 1.41 |
| Mg | 0.006 | 8.2 |
| Cr | 0.004 | 0.52 |
| Ni | 0.004 | 2.71 |
| Zn | 0.02 | 9.65 |
| Ti | 0.009 | 0.20 |
| Ag | 0.003 | 0.4 |
| As | 0.005 | 0.012 |
| B | 0.009 | 0.027 |
| Ba | 0.002 | 0.03 |
| Be | 0.002 | 0.11 |
| Bi | 0.01 | 0.59 |
| Ca | 0.003 | 0.048 |
| Cd | 0.002 | 0.055 |
| Co | 0.002 | 0.034 |
| Ga | 0.01 | 0.019 |
| Li | 0.001 | 2.48 |
| Mo | 0.02 | 0.15 |
| Na | 0.008 | 0.026 |
| P | 0.01 | 0.025 |
| Pb | 0.009 | 0.51 |
| Sb | 0.01 | 0.28 |
| Sc | 0.01 | 0.065 |
| Sn | 0.008 | 6.28 |
| Sr | 0.0008 | 0.028 |
| Ti | 0.005 | 0.20 |
| Tl | 0.009 | 0.13 |
| V | 0.01 | 0.12 |
| Zr | 0.004 | 0.25 |
1.2This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different composition ranges if method validation, which includes evaluation of method sensitivity and precision and bias (as described in Section 14), is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user should carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.
1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Safety hazard statements are given in Section 10 and specific warning statements are given in Sections 15, 17, 18, 19, 20 and 21.
| Committee |
E 01
|
| DevelopmentNote |
Supersedes ASTM E 34. (09/2017)
|
| DocumentType |
Test Method
|
| Pages |
11
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
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| ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
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| ASTM E 177 : 2014 : REDLINE | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 1479 : 1999 : R2005 | Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers |
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| ASTM E 716 : 2016 : R2021 : EDT 2 | Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry |
| ASTM D 1193 : 1977 : R1983 : EDT 1 | Standard Specification for Reagent Water |
| ASTM E 50 : 2017 : REDLINE | Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials |
| ASTM E 135 : 2021 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 716 : 2016 : R2021 | Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry |
| ASTM E 1329 : 2000 : R2005 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 1479 : 2016 : REDLINE | Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers |
| ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 716 : 2016 | Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry |
| ASTM E 135 : 2003 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 691 : 2023 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM D 1193 : 2006 : R2011 | Standard Specification for Reagent Water |
| ASTM E 135 : 2023 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1452 : 1992 : R1996 | Standard Practice for Preparation of Calibration Solutions for Spectrophotometric and for Spectroscopic Atomic Analysis (Withdrawn 2005) |
| ASTM E 1329 : 2010 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019) |
| ASTM E 1479 : 1999 : R2011 | Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers |
| ASTM E 2857 : 2022 | Standard Guide for Validating Analytical Methods |
| ASTM E 691 : 2022 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 1329 : 2000 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 716 : 2016 : REDLINE | Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry |
| ASTM D 1193 : 1991 | Standard Specification for Reagent Water |
| ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2022 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 2857 : 2011 : R2021 : EDT 1 | Standard Guide for Validating Analytical Methods |
| ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 2857 : 2011 : R2016 | Standard Guide for Validating Analytical Methods |
| ASTM E 135 : 2022 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 : REV C | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 716 : 2016 : R2021 : EDT 1 | Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry |
| ASTM D 1193 : 1970 | Standard Specification For Reagent Water |
| ASTM E 2857 : 2011 | Standard Guide for Validating Analytical Methods |
| ASTM D 1193 : 2006 | Standard Specification for Reagent Water |
| ASTM E 135 : 2022 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 50 : 1982 : R1986 | Standard Practices for Apparatus, Reagents, and Safety Precautions for Chemical Analysis of Metals |
| ASTM D 1193 : 1999 | Standard Specification for Reagent Water |
| ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 1193 : 2006 : R2018 | Standard Specification for Reagent Water |
| ASTM E 1479 : 1999 | Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers |
| ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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