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ASTM E 415 : 2017

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Atomic Emission Spectrometry

Available format(s)

Hardcopy , PDF

Superseded date

11-11-2021

Language(s)

English

Published date

06-22-2017

1.1 This test method covers the simultaneous determination of 21 alloying and residual elements in carbon and low-alloy steels by spark atomic emission vacuum spectrometry in the mass fraction ranges shown Note 1.

1.1This test method covers the simultaneous determination of 21 alloying and residual elements in carbon and low-alloy steels by spark atomic emission vacuum spectrometry in the mass fraction ranges shown Note 1.

Element

Composition Range, %

Applicable Range,
Mass Fraction %A

Quantitative Range,
Mass Fraction %B

Aluminum

0 to 0.093

0.006 to 0.093

Antimony

0 to 0.027

0.006 to 0.027

Arsenic

0 to 0.1

0.003 to 0.1

Boron

0 to 0.007

0.0004 to 0.007

Calcium

0 to 0.003

0.002 to 0.003

Carbon

0 to 1.1

0.02 to 1.1

Chromium

0 to 8.2

0.007 to 8.14

Cobalt

0 to 0.20

0.006 to 0.20

Copper

0 to 0.5

0.006 to 0.5

Manganese

0 to 2.0

0.03 to 2.0

Molybdenum

0 to 1.3

0.007 to 1.3

Nickel

0 to 5.0

0.006 to 5.0

Niobium

0 to 0.12

0.003 to 0.12

Nitrogen

0 to 0.015

0.01 to 0.055

Phosphorous

0 to 0.085

0.006 to 0.085

Silicon

0 to 1.54

0.02 to 1.54

Sulfur

0 to 0.055

0.001 to 0.055

Tin

0 to 0.061

0.005 to 0.061

Titanium

0 to 0.2

0.001 to 0.2

Vanadium

0 to 0.3

0.003 to 0.3

Zirconium

0 to 0.05

0.01 to 0.05

(A)Applicable range in accordance with Guide E1763 for results reported in accordance with Practice E1950.
(B)Quantitative range in accordance with Practice E1601.

Note 1:The mass fraction ranges of the elements listed have been established through cooperative testing2 of reference materials.

1.2This test method covers analysis of specimens having a diameter adequate to overlap and seal the bore of the spark stand opening. The specimen thickness can vary significantly according to the design of the spectrometer stand, but a thickness between 10 mm and 38 mm has been found to be most practical.

1.3This test method covers the routine control analysis in iron and steelmaking operations and the analysis of processed material. It is designed for chill-cast, rolled, and forged specimens. Better performance is expected when reference materials and specimens are of similar metallurgical condition and composition. However, it is not required for all applications of this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
E 01
DocumentType
Test Method
Pages
11
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM B 848/B848M : 2021 Standard Specification for Powder Forged (PF) Ferrous Materials
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ASTM E 2093 : 2012 : R2016 Standard Guide for Optimizing, Controlling and Assessing Test Method Uncertainties from Multiple Workstations in the Same Laboratory Organization
ASTM D 6689 : 2001 : R2019 : EDT 1 Standard Guide for Optimizing, Controlling, and Reporting Test Method Uncertainties from Multiple Workstations in the Same Laboratory Organization
ASTM E 701 : 1980 : R2018 Standard Test Methods for Municipal Ferrous Scrap
ASTM B 883 : 2019 Standard Specification for Metal Injection Molded (MIM) Materials

ASTM E 1950 : 1998 Standard Practice for Reporting Results from Methods of Chemical Analysis
ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1329 : 2000 : R2005 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 1019 : 2018 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques
ASTM E 1019 : 2003 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys
ASTM E 1806 : 1996 : R2006 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1601 : 2019 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 1998 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1019 : 2008 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques
ASTM E 2972 : 2015 Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 1601 : 2010 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1329 : 2010 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM E 1806 : 2009 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 1806 : 2009 : R2016 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 1329 : 2000 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 1763 : 2006 Standard Guide for Interpretation and Use of Results from Interlaboratory Testing of Chemical Analysis Methods (Withdrawn 2015)
ASTM E 305 : 2013 Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves
ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1601 : 2012 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E2972 : 2015(2019) Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
ASTM E 1950 : 2017 Standard Practice for Reporting Results from Methods of Chemical Analysis (Withdrawn 2023)
ASTM E 135 : 2021 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1806 : 2018 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1763 : 1998 Standard Guide for Interpretation and Use of Results from Interlaboratory Testing of Chemical Analysis Methods
ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1806 : 1996 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 305 : 2021 Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves
ASTM E 135 : 2020 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1019 : 2000 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys
ASTM E 1806 : 1996 : R2001 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 1019 : 2002 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys
ASTM E 1950 : 2010 Standard Practice for Reporting Results from Methods of Chemical Analysis
ASTM E 1019 : 2011 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques
AS/NZS 4671:2019 Steel for the reinforcement of concrete

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