Determination of certain substances in electrotechnical products Screening. Total bromine in polymers and electronics by Combustion. Ion Chromatography

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Hardcopy , PDF

Language(s)

English

Published date

05-31-2014

Publisher

British Standards Institution

INTRODUCTION
1 Scope
2 Normative references
3 Terms, definitions and abbreviations
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Procedure
9 Calculation
10 Precision
11 Quality assurance and control
12 Test report
Annex A (informative) - Oxygen bomb
        combustion-ion chromatography
Annex B (informative) - Oxygen flask
        combustion-ion chromatography
Annex C (informative) - Example of a
        combustion device and IC system
Annex D (informative) - Results of international
        interlaboratory study #4A (IIS 4A)
Annex E (informative) - Additional results of
        TG 3-2 test
Annex F (informative) - Additional validation data
Annex G (informative) - Additional IC data
Bibliography
Annex ZA (normative) - Normative references to international
         Publications with their corresponding
         European publications

Defines the screening analysis of the total bromine (Br) in homogeneous materials found in polymers and electronics by using the analytical technique of combustion ion chromatography (C-IC).

Part 3-2 of IEC 62321 specifies the screening analysis of the total bromine (Br) in homogeneous materials found in polymers and electronics by using the analytical technique of combustion ion chromatography (C-IC). This test method has been evaluated for ABS (acrylonitrile butadiene styrene), EMC (epoxy molding compound), and PE (polyethylene) within the concentration ranges as specified in Table 1. The use of this method for other types of materials or concentration ranges outside those specified below has not been evaluated. Table 1 – Tested concentration ranges for bromine by C-IC in various materials Substance/element Bromine Parameter Unit of measure
mg/kg Medium/material tested ABS EMC PE Concentration or concentration range tested 124 to 890 195 to 976 96 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee	GEL/111
DevelopmentNote	Supersedes BS EN 62321, which remains current. Supersedes 10/30229134 DC. (05/2014)
DocumentType	Standard
Pages	36
PublisherName	British Standards Institution
Status	Current
Supersedes	10/30229134 DC : 0 BS EN 62321:2009

Standards	Relationship
EN 62321-3-2:2014	Identical

ISO 5725-1:1994	Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
EN 62321-1:2013	Determination of certain substances in electrotechnical products - Part 1: Introduction and overview
ASTM D 808 : 2016 : REDLINE	Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method)
IEC 60754-1:2011	Test on gases evolved during combustion of materials from cables - Part 1: Determination of the halogen acid gas content
EN 14582:2016	Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods
EN 14346:2006	CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT
EN 62321-3-1:2014	Determination of certain substances in electrotechnical products - Part 3-1: Screening - Lead, mercury, cadmium, total chromium and total bromine by X-ray fluorescence spectrometry
ISO 10304-1:2007	Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
EN 60754-1:2014	Test on gases evolved during combustion of materials from cables - Part 1: Determination of the halogen acid gas content
IEC 60754-2:2011	Test on gases evolved during combustion of materials from cables - Part 2: Determination of acidity (by pH measurement) and conductivity
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15002:2015	Characterization of waste - Preparation of test portions from the laboratory sample
ISO 6206:1979	Chemical products for industrial use — Sampling — Vocabulary
EN 62321-2:2014	Determination of certain substances in electrotechnical products - Part 2: Disassembly, disjointment and mechanical sample preparation
EN ISO 10304-1:2009	Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007)

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BS EN 62321-3-2:2014

Determination of certain substances in electrotechnical products Screening. Total bromine in polymers and electronics by Combustion. Ion Chromatography

Table of Contents

Abstract

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General Product Information

International Equivalents

Standards Referencing This Book

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