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BS EN 725-1:2007

Current

Current

The latest, up-to-date edition.

Advanced technical ceramics. Methods of test for ceramic powders Determination of impurities in alumina

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

10-31-2007

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
   4.1 General
   4.2 Reagents for fusion
   4.3 Sulphuric acid-phosphoric acid mixture for acid
       dissolution
   4.4 Reagents for calibration
5 Apparatus
6 Test sample
7 Decomposition of the test sample
   7.1 General
   7.2 Fusion
   7.3 Acid dissolution
8 Calibration graph
   8.1 General
   8.2 Fusion
   8.3 Acid dissolution
   8.4 Drawing the calibration curve
9 Adjustment of the apparatus
   9.1 Atomic absorption spectrometer
   9.2 Inductively coupled plasma spectrometer
10 Measurements
11 Expression of the results
12 Test report
Annex A (informative) Repeatability and reproducibility
Bibliography

Defines one fusion and one acid dissolution method for the determination of elements of sodium, potassium, iron, silicon, calcium and magnesium present as impurities in alumina using atomic absorption spectroscopy (AAS) or inductively coupled plasma (ICP) spectroscopy.

This Part of EN 725 specifies one fusion and one acid dissolution method for the determination of elements of sodium, potassium, iron, silicon, calcium and magnesium present as impurities in alumina using atomic absorption spectroscopy (AAS) or inductively coupled plasma (ICP) spectroscopy. For each element present as impurities, the methods are applicable to the following ranges, calculated as oxides : - Sodium oxide: 20 ppm to 6000 ppm - Potassium oxide: 20 ppm to 100 ppm - Ferric oxide: 20 ppm to 300 ppm - Silica: 50 ppm to 2000 ppm - Calcium oxide: 20 ppm to 700 ppm - Magnesium oxide: 5 ppm to 1000 ppm

Committee
RPI/13
DevelopmentNote
Supersedes 93/311578 DC. (08/2005) Supersedes 05/30117337 DC. (10/2007)
DocumentType
Standard
Pages
14
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
I.S. EN 725-1:2007 Identical
DIN EN 725-1:2008-06 Identical
NEN EN 725-1 : 2007 Identical
SN EN 725-1:2007 Identical
UNI EN 725-1 : 2008 Identical
NBN EN 725-1 : 2007 Identical
EN 725-1:2007 Identical
NS EN 725-1 : 2ED 2007 Identical
NF EN 725-1 : 2007 Identical

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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