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PD ISO/TS 16965:2013

Current
Current

The latest, up-to-date edition.

Soil quality. Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

10-31-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Procedure
8 Calculation
9 Expression of results
10 Performance characteristics
11 Test report
Annex A (informative) - Selected isotopes and spectral
        interferences for quadrupole ICP-MS instruments
Bibliography

Defines a method for the determination of the following elements in aqua regia or nitric acid digests or other extraction solutions of sludge, treated biowaste and soil: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc (Zn) and zirconium (Zr).

This Technical Specification specifies a method for the determination of the following elements in aqua regia or nitric acid digests or other extraction solutions of sludge, treated biowaste and soil:

Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium(Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium(Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium(Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel(Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver(Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc(Zn) and zirconium (Zr).

The working range depends on the matrix and the interferences encountered.

The limit of detection is between 0,1mg/kg dry matter and 2,0mg/kg dry matter for most elements.

The limit of detection will be higher in cases where the determination is likely to have interferences (see Clause4) or in the case of memory effects (see e.g. 8.2 of ISO17294-1:2004).

Committee
EH/4
DocumentType
Standard
Pages
22
PublisherName
British Standards Institution
Status
Current

Standards Relationship
ISO/TS 16965:2013 Identical

ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
EN 16174:2012 Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
ISO 17294-1:2004 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 1: General guidelines
EN 16173:2012 Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods

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