WATER QUALITY - DETERMINATION OF SHORT-CHAIN POLYCHLORINATED ALKANES (SCCPS) IN SEDIMENT, SEWAGE SLUDGE AND SUSPENDED (PARTICULATE) MATTER - METHOD USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) AND ELECTRON CAPTURE NEGATIVE IONIZATION (ECNI) (ISO 18635:2016)

Available format(s)

Hardcopy , PDF

Language(s)

German

Published date

01-01-2016

Publisher

German Institute for Standardisation (Deutsches Institut für Normung)

National foreword
National Annex NA (informative) - Bibliography
European foreword
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample pretreatment
8 Procedure
9 Expression of results
10 Test report
Annex A (normative) - Programme for pressurized liquid extraction
Annex B (informative) - Explanation of the calibration of the sum
        of SCCPs with multiple linear regression
Annex C (informative) - Examples of typical GC-MS conditions
Annex D (normative) - Alternative clean-up with column
        chromatography
Annex E (informative) - Alternative clean-up with gel
        chromatography
Annex F (informative) - Typical chromatograms of standard
        solutions 1 [mu]g/ml
Annex G (informative) - Presentation of goodness of fit of the
        calibration
Annex H (informative) - Example for recoveries of quality
        assurance solutions
Annex I (informative) - Chromatograms of real samples
Annex J (informative) - Performance data
Annex K (informative) - Quality control check solutions
Bibliography

Describes a method for the quantitative determination of the sum of shortchain polychlorinated n-alkanes also known as short-chain polychlorinated paraffins (SCCPs) in the carbon bond range, n-C[10] to n-C[13], inclusive in mixtures with chlorine mass fractions (contents) between 50% and 67%, including approximately 6000 of approximately 8000 congeners.

DocumentType	Standard
Pages	42
PublisherName	German Institute for Standardisation (Deutsches Institut für Normung)
Status	Current

Standards	Relationship
ISO 18635:2016	Identical
EN ISO 18635:2016	Identical

ISO 5667-13:2011	Water quality Sampling Part 13: Guidance on sampling of sludges
DIN 38402-51:2015-09	GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - GENERAL INFORMATION (GROUP A) - PART 51: CALIBRATION OF ANALYTICAL METHODS - LINEAR CALIBRATION (A 51)
DIN ISO 5725-2:2002-12	Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
DIN 38414-11:1987-08	GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE; SLUDGE AND SEDIMENTS (GROUP S); SAMPLING OF SEDIMENTS (S 11)
DIN EN ISO 5667-1:2007-04	Water quality - Sampling - Part 1: Guidance on the design of sampling programmes and sampling techniques (ISO 5667-1:2006)
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
ISO 5667-12:2017	Water quality — Sampling — Part 12: Guidance on sampling of bottom sediments from rivers, lakes and estuarine areas
ISO 12010:2012	Water quality Determination of short-chain polychlorinated alkanes (SCCPs) in water Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)

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DIN EN ISO 18635:2016-10

WATER QUALITY - DETERMINATION OF SHORT-CHAIN POLYCHLORINATED ALKANES (SCCPS) IN SEDIMENT, SEWAGE SLUDGE AND SUSPENDED (PARTICULATE) MATTER - METHOD USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) AND ELECTRON CAPTURE NEGATIVE IONIZATION (ECNI) (ISO 18635:2016)

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