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EN 16995:2017

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Foodstuffs - Vegetable oils and foodstuff on basis of vegetable oils - Determination of mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbons (MOAH) with on-line HPLC-GC-FID analysis
Withdrawn date

12-31-2017

Published date

06-14-2017

European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sample storage
8 Preparation of the test sample
9 Preparation of the analytical sample
10 Liquid chromatography and gas chromatography
11 Precision
12 Test report
Annex A (informative) - Examples of chromatograms
Annex B (informative) - Precision data
Bibliography

This European Standard specifies a highly efficient method for the determination of saturated and aromatic hydrocarbons (from C10 to C50) in vegetable fats and oils and foodstuff on basis of vegetable oils for which it has been interlaboratory validated, with online-HPLC-GC-FID [1], [2] and [3]. This standard is not intended to be applied to other matrices.The method can be used for the analysis of mineral oil saturated hydrocarbons (MOSH) and/or mineral oil aromatic hydrocarbons (MOAH).The method has been tested in an interlaboratory study via the analysis of both naturally contaminated and spiked vegetable oil samples and mayonnaise and margarine samples, ranging from 4 mg/kg to 197 mg/kg for MOSH, and from 2 mg/kg to 51 mg/kg for MOAH.According to the results of the interlaboratory studies, the method has been proven suitable for MOSH- and MOAH mass concentrations each above 10 mg/kg.In case of suspected interferences from natural sources, the mineral origin of the MOSH and MOAH fraction can be verified by examination of the pattern by GC-MS.

Committee
CEN/TC 275
DevelopmentNote
Supersedes PREN 16995. (06/2017)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn

Standards Relationship
PN EN 16995 : 2017 Identical
BS EN 16995:2017 Identical
NF EN 16995 : 2017 Identical
DIN EN 16995:2016-05 (Draft) Identical
NS EN 16995 : 2017 Identical
I.S. EN 16995:2017 Identical
UNE-EN 16995:2018 Identical
SN EN 16995 : 2017 Identical
DIN EN 16995 E : 2017 Identical
UNI EN 16995 : 2017 Identical
NEN EN 16995 : 2017 Identical
DIN EN 16995:2017-08 Identical

ISO 5555:2001 Animal and vegetable fats and oils — Sampling
EN ISO 661:2005/AC:2006 ANIMAL AND VEGETABLE FATS AND OILS - PREPARATION OF TEST SAMPLE
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 661:2003 Animal and vegetable fats and oils Preparation of test sample

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