WATER QUALITY - DETERMINATION OF SHORT-CHAIN POLYCHLORINATED ALKANES (SCCPS) IN SEDIMENT, SEWAGE SLUDGE AND SUSPENDED (PARTICULATE) MATTER - METHOD USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) AND ELECTRON CAPTURE NEGATIVE IONIZATION (ECNI) (ISO 18635:2016)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2016

Publisher

National Standards Authority of Ireland

Preview

For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.

Only cited Standards give presumption of conformance to New Approach Directives/Regulations.

National Foreword
European foreword
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample pretreatment
8 Procedure
9 Expression of results
10 Test report
Annex A (normative) - Programme for pressurized liquid
        extraction
Annex B (informative) - Explanation of the calibration of the
        sum of SCCPs with multiple linear regression
Annex C (informative) - Examples of typical GC-MS conditions
Annex D (normative) - Alternative clean-up with column
        chromatography
Annex E (informative) - Alternative clean-up with gel
        Chromatography
Annex F (informative) - Typical chromatograms of standard
         solutions 1 [mu]g/ml
Annex G (informative) - Presentation of goodness of fit of
        the calibration
Annex H (informative) - Example for recoveries of
        quality assurance solutions
Annex I (informative) - Chromatograms of real samples
Annex J (informative) - Performance data
Annex K (informative) - Quality control check solutions
Bibliography

Defines a method for the quantitative determination of the sum of short-chain polychlorinated n-alkanes also known as short-chain polychlorinated paraffins (SCCPs) in the carbon bond range n-C[10] to n-[C13] inclusive, in mixtures with chlorine mass fractions ('contents') between 50% and 67%, including approximately 6000 of approximately 8000 congeners.

DocumentType	Standard
Pages	50
PublisherName	National Standards Authority of Ireland
Status	Current

Standards	Relationship
ISO 18635:2016	Identical
EN ISO 18635:2016	Identical

ISO 5667-13:2011	Water quality Sampling Part 13: Guidance on sampling of sludges
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
ISO 5667-12:2017	Water quality — Sampling — Part 12: Guidance on sampling of bottom sediments from rivers, lakes and estuarine areas
ISO 5667-17:2008	Water quality — Sampling — Part 17: Guidance on sampling of bulk suspended solids
ISO 12010:2012	Water quality Determination of short-chain polychlorinated alkanes (SCCPs) in water Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)

View more information

US$70.16

Excluding Tax where applicable

Product format

I agree to the DRM document license rules apply against the PDF selection made.

Please confirm that you agree to the document license rules for this document.

I agree to the document license rules .

Please confirm that you agree to the document license rules for this document.

Access your standards online with a subscription

Features

Simple online access to standards, technical information and regulations.
Critical updates of standards and customisable alerts and notifications.
Multi-user online standards collection: secure, flexible and cost effective.

Learn more on subscription solutions

Get in touch with us

Log into your Account

I.S. EN ISO 18635:2016

Current

Table of Contents

Abstract

General Product Information

International Equivalents

Standards Referencing This Book

Category

Subcategory

Access your standards online with a subscription