IEC 60814 : 2.0

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INSULATING LIQUIDS - OIL-IMPREGNATED PAPER AND PRESSBOARD - DETERMINATION OF WATER BY AUTOMATIC COULOMETRIC KARL FISCHER TITRATION

Publisher: International Electrotechnical Committee

Published: 08-29-1997

Available Formats: PDF - English - French, Hardcopy - English - French
More Info on product formats

Table of Contents - (Show below) - (Hide below)

1 General
    1.1 Scope
    1.2 Normative references
2 Direct titration for low viscosity liquids
    2.1 Field of application
    2.2 Chemistry
    2.3 Apparatus
    2.4 Reagents and auxiliary materials
    2.5 Preparation of the apparatus
    2.6 Sampling methods
    2.7 Procedure
    2.8 Calculation of the result
    2.9 Report
    2.10 Precision
3 Evaporative stripping method for high viscosity liquids
    3.1 Field of application
    3.2 Outline of the method
    3.3 Apparatus and reagents
    3.4 Procedure
    3.5 Calculation of water content
    3.6 Report
4 Determination of water in oil-impregnated paper and
    pressboard
    4.1 Field of application
    4.2 Determination of water after previous extraction
          with methanol
    4.3 Determination by direct titration
    4.4 Evaporative stripping method
Figures
1 Block diagram of automatic titrator
2 Suitable titration vessel assembly
3 Block diagram of automatic titrator and evaporation
    stripping unit
4 Evaporator glass vessel with heater
5 Methanol container and extraction tube
Annexes
A Method for sampling of oil-impregnated paper and
    pressboard
ZA (normative) Normative references to international
    publications with their corresponding European
    publications

Abstract - (Show below) - (Hide below)

Covers procedures for determining water content of insulating liquids and in oil-impregnated cellulosic insulation with coulometrically generated Karl Fischer reagent.

General Product Information - (Show below) - (Hide below)

Published
Document Type	Standard
Status	Current
Publisher	International Electrotechnical Committee
Pages
ISBN
Committee	SC 10A

International Equivalents – Equivalent Standard(s) & Relationship - (Show below) - (Hide below)

Equivalent Standard(s)	Relationship
NF EN 60814 : 1998	Identical
DS EN 60814 : 1997	Identical
GOST R IEC 60814 : 2013	Identical
GOST IEC 60814 : 2014	Identical
NEN EN IEC 60814 : 1997	Identical
I.S. EN 60814:1998	Identical
PN EN 60814 : 2002	Identical
SN EN 60814 : 1997	Identical
DIN EN 60814 : 1999	Identical
VDE 0370-20 : 1999	Identical
IS 13567 : 2018	Identical
UNE EN 60814 : 1999	Identical
UNE 21384 : 1992	Identical
CEI 10-13 : 1ED 1997	Identical
CEI EN 60814 : 1998	Identical
EN 60814 : 1997	Identical
IS 13567 : 2018	Identical
UNE EN 60814 : 1999	Identical
NF EN 60814 : 1998	Identical
NEN EN IEC 60814 : 1997	Identical
I.S. EN 60814:1998	Identical
GOST R IEC 60814 : 2013	Identical
PN EN 60814 : 2002	Identical
DS EN 60814 : 1997	Identical
SN EN 60814 : 1997	Identical
GOST IEC 60814 : 2014	Identical
CEI EN 60814 : 1998	Identical
CEI 10-13 : 1ED 1997	Identical
UNE 21384 : 1992	Identical

Standards Referenced By This Book - (Show below) - (Hide below)

NF EN 50375 : 2002	TESTING METHODOLOGY FOR WIPERS USED IN ELECTRICAL INSULATING OIL
11/30235371 DC : 0	BS EN 62701 - FLUIDS FOR ELECTRO TECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
BS PD IEC TS 62332-3 : 2016	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 3: HERMETIC MOTOR-COMPRESSORS
I.S. EN 60422:2013	MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
BS PD IEC TR 62874 : 2015	GUIDANCE ON THE INTERPRETATION OF CARBON DIOXIDE AND 2-FURFURALDEHYDE AS MARKERS OF PAPER THERMAL DEGRADATION IN INSULATING MINERAL OIL
BS EN 61099 : 2010	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
UNE EN 62770 : 2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
03/100225 DC : DRAFT FEB 2003	IEC 60836 ED.2 - SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
BS EN 60422 : 2013	MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
17/30331680 DC : 0	BS ISO 18095 - CONDITION MONITORING AND DIAGNOSTICS OF POWER TRANSFORMERS
12/30257150 DC : 0	BS EN 62770 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS LIQUIDS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
BS EN 60450 : 2004	MEASUREMENT OF THE AVERAGE VISCOMETRIC DEGREE OF POLYMERIZATION OF NEW AND AGED CELLULOSIC ELECTRICALLY INSULATING MATERIALS
01/206865 DC : DRAFT SEP 2001	IEC 61221 ED.2 - PETROLEUM PRODUCTS AND LUBRICANTS - TRIARYL PHOSPHATE ESTER TURBINE CONTROL FLUIDS (CATEGORY ISO-L-TCD) - SPECIFICATIONS
BS EN 62770 : 2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
06/30159746 DC : 0	BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
08/30195180 DC : DRAFT DEC 2008	BS EN 61099 - SPECIFICATION FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
BS EN 50375 : 2002	TESTING METHODOLOGY FOR WIPERS USED IN ELECTRICAL INSULATING OIL
02/207269 DC : 0	IEC 60422 ED.3 - SUPERVISION AND MAINTENANCE GUIDE FOR MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT
BS EN 60296 : 2012	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
BS EN 60455-2 : 2015	RESIN BASED REACTIVE COMPOUNDS USED FOR ELECTRICAL INSULATION - PART 2: METHODS OF TEST
NBR IEC 60079-6 : 2017	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY OIL IMMERSION 'O'
03/100561 DC : DRAFT JULY 2003	IEC 60422 ED.3 - SUPERVISION AND MAINTENANCE GUIDE FOR MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT
SR CLC/TR 50503:2010	GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
BS EN 60836 : 2015	SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
BS EN 60867 : 1994	INSULATION LIQUIDS - SPECIFICATIONS FOR UNUSED LIQUIDS BASED ON SYNTHETIC AROMATIC HYDROCARBONS
13/30267448 DC : 0	BS EN 60079-6 ED 4.0 - EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
BIS IS 16081 : 2013	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
12/30268820 DC : 0	BS EN 60836 - SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
CEI EN 61099 : 2011	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
00/244591 DC : DRAFT OCT 2000	SPECIFICATION FOR UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
BS PD IEC TS 62332-2 : 2014	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 2: SIMPLIFIED TEST
10/30215366 DC : 0	BS EN 60422 - MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
DD IEC TS 62332-1 : 2011	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 1: GENERAL REQUIREMENTS
CEI EN 60079-6 : 2016	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
ASTM D 1533 : 2012 : REDLINE	Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
NBR IEC 60450 : 2009	MEASUREMENT OF THE AVERAGE VISCOMETRIC DEGREE OF POLYMERIZATION OF NEW AND AGED CELLULOSIC ELECTRICALLY INSULATING MATERIALS
BS 148(1998) : 1998	SPECIFICATION FOR UNUSED AND RECLAIMED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
BS EN 60079-6 : 2007	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY BY LIQUID IMMERSION 'O'
CLC/TR 50503 : 2010	GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
I.S. EN 62701:2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
IEC TS 62332-2 : 1ED 2014	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 2: SIMPLIFIED TEST
NF EN 60450 : 2004 AMD 1 2007	MEASUREMENT OF THE AVERAGE VISCOMETRIC DEGREE OF POLYMERIZATION OF NEW AND AGED CELLULOSIC ELECTRICALLY INSULATING MATERIALS
IEC TR 62874 : 1ED 2015	GUIDANCE ON THE INTERPRETATION OF CARBON DIOXIDE AND 2-FURFURALDEHYDE AS MARKERS OF PAPER THERMAL DEGRADATION IN INSULATING MINERAL OIL
I.S. EN 60867:1996	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED LIQUIDS BASED ON SYNTHETIC AROMATIC HYDROCARBONS
UNE EN 61099 : 2011	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
I.S. EN 60455-2:2015	RESIN BASED REACTIVE COMPOUNDS USED FOR ELECTRICAL INSULATION - PART 2: METHODS OF TEST
I.S. EN 60296:2012	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
I.S. EN 60836:2015	SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
I.S. EN 62770:2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
CEI EN 50375 : 2003	TESTING METHODOLOGY FOR WIPERS USED IN ELECTRICAL INSULATING OIL
DIN EN 60465 : 1994	SPECIFICATION FOR UNUSED INSULATING MINERAL OILS FOR CABLES WITH OIL DUCTS
VDE 0372-2 : 1996	UNUSED MINERAL INSULATING OILS - SPECIFICATION FOR UNUSED POLYBUTENES
I.S. EN 61099:2010	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
IEC 60296 REDLINE : 4.0	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
DIN IEC 60963 : 1996	SPECIFICATION FOR UNUSED POLYBUTENES
NF EN 61099 : 2011	INSULATING LIQUIDS - SPECIFICATION FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
I.S. EN 60079-6:2015	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
09/30213528 DC : 0	BS EN 60296 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OIL FOR TRANSFORMERS AND SWITCHGEAR
ISO 18095 : 2018	CONDITION MONITORING AND DIAGNOSTICS OF POWER TRANSFORMERS
VDE 0370-12 : 1994	SPECIFICATION FOR UNUSED INSULATING MINERAL OILS FOR CABLES WITH OIL DUCTS
UNE EN 60836 : 2015	SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
CEI EN 62770 : 2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
I.S. EN 60450:2004	MEASUREMENT OF THE AVERAGE VISCOMETRIC DEGREE OF POLYMERIZATION OF NEW AND AGED CELLULOSIC ELECTRICALLY INSULATING MATERIALS
IEC TS 62332-3 : 1.0	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 3: HERMETIC MOTOR-COMPRESSORS
IEC TS 62332-1 : 2.0	ELECTRICAL INSULATION SYSTEMS (EIS) - THERMAL EVALUATION OF COMBINED LIQUID AND SOLID COMPONENTS - PART 1: GENERAL REQUIREMENTS
IEC 60079-6 : 2015	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
IEC 60836 : 3.0	SPECIFICATIONS FOR UNUSED SILICONE INSULATING LIQUIDS FOR ELECTROTECHNICAL PURPOSES
IEC 62770 : 1ED 2013	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
IEC 60450 : 2.1	MEASUREMENT OF THE AVERAGE VISCOMETRIC DEGREE OF POLYMERIZATION OF NEW AND AGED CELLULOSIC ELECTRICALLY INSULATING MATERIALS
IEC 60296 : 4.0EN+(REDLINE+VERSION)	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
UNE EN 60079-6 : 2016	EXPLOSIVE ATMOSPHERES - PART 6: EQUIPMENT PROTECTION BY LIQUID IMMERSION 'O'
IEC 60455-2 : 3.0	RESIN BASED REACTIVE COMPOUNDS USED FOR ELECTRICAL INSULATION - PART 2: METHODS OF TEST
IEC 61099 : 2.0	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
UNE EN 60296 : 2012	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
IEC 62701 : 1ED 2014	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
IEC 60867 : 2.0	INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED LIQUIDS BASED ON SYNTHETIC AROMATIC HYDROCARBONS
UNE EN 60422 : 2013	MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
IEC 60422 : 4.0	MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE
EN 60296 : 2012	FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012)

Standards Referencing This Book - (Show below) - (Hide below)

ISO 595-2 : 1987	REUSABLE ALL GLASS OR METAL AND GLASS SYRINGES FOR MEDICAL USE - PART 2: DESIGN, PERFORMANCE REQUIREMENTS AND TESTS
IEC 60475 : 2.0	METHOD OF SAMPLING INSULATING LIQUIDS
IEC 60567 : 4.0	OIL-FILLED ELECTRICAL EQUIPMENT - SAMPLING OF GASES AND ANALYSIS OF FREE AND DISSOLVED GASES - GUIDANCE
ISO 595-1 : 1986	REUSABLE ALL GLASS OR METAL AND GLASS SYRINGES FOR MEDICAL USE - PART 1: DIMENSIONS

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IEC 60814 : 2.0

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Abstract - (Show below) - (Hide below)

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International Equivalents – Equivalent Standard(s) & Relationship - (Show below) - (Hide below)

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