ISO 3793:1976
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Essential oils — Estimation of primary and secondary free alcohols content by acetylation in pyridine
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04-05-2019
English, French
08-01-1976
The method consists in acetylating the hydroxyl groups containing compounds with a mixture of acetic anhydride and pyridine. The excess of acetic anhydride is hydrolized and the acetic acid formed is titrated with a potassium hydroxide solution. Primary and secondary alcoholes are acetylated completely by this method. Phenols, anthranilates and aldehydes are acetylated either completely or partially. Tertiary alcohols are acetylated only in a negligible extent.
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