Soil quality Determination of some selected phenols and chlorophenols Gas chromatographic method with mass spectrometric detection

Available format(s)

Hardcopy , PDF , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

English, French

Published date

11-21-2014

Publisher

International Organization for Standardization

ISO/TS 17182:2014 describes the gas chromatographic determination of phenols, methyl phenols, di-methylphenols and tri-methylphenols (see Table 1) and selected chlorophenols (see Table 2) by using mass spectrometric detection in soil samples. This method can also be used for other solid samples, such as sediments and solid wastes. This International Standard describes an acidic liquid extraction of soil, followed by acetylation and then liquid/liquid extraction. Determination takes place by gas chromatography and mass spectrometric detection.

With this method, phenols and chlorophenols can be determined at the lowest of mass concentrations ranging from approximately 0,01 mg/kg to 0,1 mg/kg depending on the component sensitivity and the quantity of sample used. In some cases, complete separation of isomers cannot be achieved. Then the sum is reported.

NOTE With this method, other higher methylated phenols can also be analysed provided that the suitability and the validity of the method is proven.

DocumentType	Technical Specification
Pages	15
PublisherName	International Organization for Standardization
Status	Current

Standards	Relationship
PD ISO/TS 17182:2014	Identical

ISO 10381-1:2002	Soil quality Sampling Part 1: Guidance on the design of sampling programmes
EN 12673 : 1998	WATER QUALITY - GAS CHROMATOGRAPHIC DETERMINATION OF SOME SELECTED CHLOROPHENOLS IN WATER
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 11709:2011	Soil quality Determination of selected coal-tar-derived phenolic compounds using high performance liquid chromatography (HPLC)
ISO 14507:2003	Soil quality Pretreatment of samples for determination of organic contaminants
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 14154:2005	Soil quality — Determination of some selected chlorophenols — Gas-chromatographic method with electron-capture detection
ISO 18512:2007	Soil quality Guidance on long and short term storage of soil samples