Name: PREN 16190 : DRAFT 2017
Brand: CEN

SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)

Published date

11-28-2017

Publisher

Comite Europeen de Normalisation

European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Abbreviations
5 Principle
6 Reagents
7 Apparatus and materials
8 Sample storage and sample pretreatment
9 Extraction and clean-up
10 HRGC/HRMS analysis
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Toxic equivalency
        factor (TEF)
Annex B (informative) - Examples of extraction
        and clean-up methods
Annex C (informative) - Examples of operation of
        GC/HRMS determination - Example
Annex D (informative) - Repeatability and reproducibility
        data
Bibliography

Describes the method for quantitative determination of 17 2,3,7,8-chlorine substituted dibenzo-p-dioxins and dibenzofurans and dioxin-like polychlorinated biphenyls in sludge, treated biowaste and soil using liquid column chromatographic clean-up methods and GC/HRMS.

Committee	TC 444
DocumentType	Draft
PublisherName	Comite Europeen de Normalisation
Status	Current

Standards	Relationship
17/30363999 DC : DRAFT OCT 2017	Identical
NEN EN 16190 : DRAFT 2017	Identical
DIN EN 16190:2017-11 (Draft)	Identical
NF EN 16190 : 2017 PR	Identical
17/30363999 DC : 0	Identical

EN 1948-2:2006	Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
EN 1948-1:2006	Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006	Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
ISO 18073:2004	Water quality — Determination of tetra- to octa-chlorinated dioxins and furans — Method using isotope dilution HRGC/HRMS
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN 15934:2012	Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
EN 16179:2012	Sludge, treated biowaste and soil - Guidance for sample pretreatment