Name: UNI EN ISO 22032 : 2009
Brand: UNI

WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHERS IN SEDIMENT AND SEWAGE SLUDGE - METHOD USING EXTRACTION AND GAS CHROMOTOGRAPHY/MASS SPECTROMETRY

Published date

06-25-2009

Publisher

Ente Nazionale Italiano di Unificazione (UNI)

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) Clean-up procedures
Annex B (informative) Examples for separation conditions in
gas chromatography and mass spectrometry
Annex C (informative) Typical ions and time windows for
electron impact ionization detection
Annex D (informative) Examples of chromatograms and spectra
Annex E (informative) Precision data
Bibliography

Describes a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode.

DocumentType	Standard
PublisherName	Ente Nazionale Italiano di Unificazione (UNI)
Status	Current

Standards	Relationship
EN ISO 22032:2009	Identical
ISO 22032:2006	Identical

ISO 5667-13:2011	Water quality Sampling Part 13: Guidance on sampling of sludges
ISO/TR 13530:1997	Water quality Guide to analytical quality control for water analysis
EN 12880:2000	Characterization of sludges - Determination of dry residue and water content
DIN 32645:2008-11	CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function