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ASTM C 1347 : 2008 : R2014 : EDT 1

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis
Available format(s)

Hardcopy , PDF

Superseded date

01-13-2023

Language(s)

English

Published date

06-14-2014

CONTAINED IN VOL. 12.01, 2015 Defines dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations.

1.1This practice covers dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations. Dissolution treatments for the major uranium materials assayed for uranium or analyzed for other components are listed.

1.2The treatments, in order of presentation, are as follows:

Procedure Title

Section

Dissolution of Uranium Metal and Oxide with Nitric Acid

8.1

Dissolution of Uranium Oxides with Nitric Acid and Residue
  Treatment

8.2

Dissolution of Uranium-Aluminum Alloys in Hydrochloric Acid
 with Residue Treatment

8.3

Dissolution of Uranium Scrap and Ash by Leaching with Nitric
 Acid and Treatment of Residue by Carbonate Fusion

8.4

Dissolution of Refractory Uranium-Containing Material by
 Carbonate Fusion

8.5

Dissolution of Uranium—Aluminum Alloys
Uranium Scrap and Ash, and Refractory
Uranium-Containing Materials by
Microwave Treatment

8.6


1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Committee
C 26
DocumentType
Standard Practice
Pages
9
ProductNote
Reconfirmed EDT 1
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM C 1411 : 2014 Standard Practice for The Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis
ASTM C 1672 : 2017 Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1647 : 2013 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials
ASTM C 1816 : 2016 Standard Practice for The Ion Exchange Separation of Small Volume Samples Containing Uranium, Americium, and Plutonium Prior to Isotopic Abundance and Content Analysis
ASTM C 968 : 2012 Standard Test Methods for Analysis of Sintered Gadolinium Oxide-Uranium Dioxide Pellets
ASTM C 1474 : 2019 Standard Test Method for Analysis of Isotopic Composition of Uranium in Nuclear-Grade Fuel Material by Quadrupole Inductively Coupled Plasma-Mass Spectrometry
ASTM C 1413 : 2018 Standard Test Method for Isotopic Analysis of Hydrolyzed Uranium Hexafluoride and Uranyl Nitrate Solutions by Thermal Ionization Mass Spectrometry
ASTM C 1625 : 2012 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C 1590 : 2004 : R2014 Standard Practice for Alternate Actinide Calibration for Inductively Coupled Plasma-Mass Spectrometry
ASTM C 1832 : 2016 Standard Test Method for Determination of Uranium Isotopic Composition by the Modified Total Evaporation (MTE) Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1845 : 2016 Standard Practice for The Separation of Lanthanide Elements from Uranium Matrices Using High Pressure Ion Chromatography (HPIC) for Isotopic Analyses by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM C 696 : 2011 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets
ASTM C 1517 : 2016 Standard Test Method for Determination of Metallic Impurities in Uranium Metal or Compounds by DC-Arc Emission Spectroscopy
ASTM C 1128 : 2018 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1287 : 2018 Standard Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry
ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
ASTM C 1267 : 2017 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
ASTM C 1462 : 2000 : R2013 Standard Specification for Uranium Metal Enriched to More than 15 % and Less Than 20 % 235U
ASTM C 1267 : 2017 : R2022 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
ASTM C 1411 : 2020 Standard Practice for The Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis
ASTM C 1625 : 2019 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM E 321 : 2020 Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method)
ASTM C 1871 : 2022 Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1832 : 2022 Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer
ASTM C 696 : 2019 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets
ASTM C 1590 : 2021 Standard Practice for Alternate Actinide Calibration for Inductively Coupled Plasma-Mass Spectrometry
ASTM C 1462 : 2021 Standard Specification for Uranium Metal Enriched to Less Than 20 % <sup> 235</sup >U
ASTM C 968 : 2019 Standard Test Methods for Analysis of Sintered Gadolinium Oxide-Uranium Dioxide Pellets
ASTM C 1647 : 2020 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials
ASTM C 1022 : 2017 : R2022 Standard Test Methods for Chemical and Atomic Absorption Analysis of Uranium-Ore Concentrate

ASTM C 776 : 2017 : R2022 Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM C 1168 : 2015 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM C 753 : 2016 : REV A Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM C 776 : 2017 Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors
ASTM C 1168 : 2001 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1168 : 2015 : REDLINE Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1168 : 1990 : R1995 : EDT 1 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM C 753 : 2016 : REV A : R2021 Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder
ASTM C 1168 : 2008 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis

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