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ASTM D 3859 : 2015

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods for Selenium in Water
Available format(s)

Hardcopy , PDF

Superseded date

01-09-2024

Language(s)

English

Published date

02-16-2016

These test methods cover the determination of dissolved and total recoverable selenium in most waters and wastewaters.

1.1These test methods cover the determination of dissolved and total recoverable selenium in most waters and wastewaters. Both test methods utilize atomic absorption procedures, as follows:

Sections

Test Method A—Gaseous Hydride AAS2, 3

7 – 16

Test Method B—Graphite Furnace AAS

17 – 26

1.2These test methods are applicable to both inorganic and organic forms of dissolved selenium. They are applicable also to particulate forms of the element, provided that they are solubilized in the appropriate acid digestion step. However, certain selenium-containing heavy metallic sediments may not undergo digestion.

1.3These test methods are most applicable within the following ranges:

Test Method A—Gaseous Hydride AAS2, 3

1 to 20 μg/L

Test Method B—Graphite Furnace AAS

2 to 100 μg/L

These ranges may be extended (with a corresponding loss in precision) by decreasing the sample size or diluting the original sample, but concentrations much greater than the upper limits are more conveniently determined by flame atomic absorption spectrometry.

1.4The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 11.12 and 13.14.

Committee
D 19
DocumentType
Test Method
Pages
12
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 4691 : 2017 Standard Practice for Measuring Elements in Water by Flame Atomic Absorption Spectrophotometry
ASTM D 1971 : 2016 Standard Practices for Digestion of Water Samples for Determination of Metals by Flame Atomic Absorption, Graphite Furnace Atomic Absorption, Plasma Emission Spectroscopy, or Plasma Mass Spectrometry
ASTM D 8006 : 2016 Standard Guide for Sampling and Analysis of Residential and Commercial Water Supply Wells in Areas of Exploration and Production (E&P) Operations
ASTM D 4382 : 2018 Standard Test Method for Barium in Water, Atomic Absorption Spectrophotometry, Graphite Furnace
ASTM D 1971 : 2016 : R2021 : EDT 1 Standard Practices for Digestion of Water Samples for Determination of Metals by Flame Atomic Absorption, Graphite Furnace Atomic Absorption, Plasma Emission Spectroscopy, or Plasma Mass Spectrometry

ASTM D 5810 : 1996 : R2021 Standard Guide for Spiking into Aqueous Samples
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 4841 : 1988 : R1998 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 2777 : 2021 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5847 : 2022 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5810 : 1996 Standard Guide for Spiking into Aqueous Samples
ASTM D 5810 : 1996 : R2015 Standard Guide for Spiking into Aqueous Samples

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