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ASTM D 4628 : 2016 : REDLINE

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
Available format(s)

PDF

Superseded date

06-13-2023

Language(s)

English

Published date

01-18-2017

Publisher

American Society for Testing and Materials

CONTAINED IN VOL. 05.02, 2017 Defines the determination of mass percent barium from 0.005 to 1.0%, calcium and magnesium from 0.002 to 0.3%, and zinc from 0.002 to 0.2% in lubricating oils.

1.1This test method is applicable for the determination of mass percent barium from 0.005 % to 1.0 %, calcium and magnesium from 0.002 % to 0.3 %, and zinc from 0.002 % to 0.2 % in lubricating oils.

1.2Higher concentrations can be determined by appropriate dilution. Lower concentrations of metals such as barium, calcium, magnesium, and zinc at about 10 ppm level can also be determined by this test method. Use of this test method for the determination at these lower concentrations should be by agreement between the buyer and the seller.

1.3Lubricating oils that contain viscosity index improvers may give low results when calibrations are performed using standards that do not contain viscosity index improvers.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 3.1, 6.3, and 8.1.

Committee
D 02
DocumentType
Redline
Pages
7
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

MIL-L-46152 Revision E:1990 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ADMINISTRATIVE SERVICE, METRIC
MIL L 21260 : D LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE AND BREAK IN
MIL L 2105 : D LUBRICATING OIL, GEAR, MULTI PURPOSE
MIL-PRF-46167 Revision D:2005 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ARCTIC
ASTM D 7578 : 2015-06 GUIDE FOR CALIBRATION REQUIREMENTS FOR ELEMENTAL ANALYSIS OF PETROLEUM PRODUCTS AND LUBRICANTS
ASTM D 7740 : 201 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
A-A-52306 Revision A:1995 LUBRICATING OIL, HEAVY-DUTY DIESEL ENGINE
ASTM D 4951 : 2014 : REDLINE Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7876 : 2013 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
ASTM D 6074 : 2015 : REDLINE Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 8110 : 2017 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
SAE J 2359 : 1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, MILITARY COMBAT/TACTICAL SERVICE
MIL PRF 009000 : K LUBRICATING OIL, SHIPBOARD INTERNAL COMBUSTION ENGINE, HIGH-OUTPUT DIESEL
MIL-PRF-9000 Revision L:2014 Lubricating Oil, Shipboard Internal Combustion Engine, High-Output Diesel
MIL-PRF-21260 Revision E:1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE BREAK-IN
SAE J 357 : 2016 PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS
ASTM D 6443 : 2014 : REDLINE TEST METHOD FOR DETERMINATION OF CALCIUM, CHLORINE, COPPER, MAGNESIUM, PHOSPHORUS, SULFUR, AND ZINC IN UNUSED LUBRICATING OILS AND ADDITIVES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (MATHEMATICAL CORRECTION PROCEDURE)
SAE J 2361 : 1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATION BREAK-IN
MIL L 9000 : H LUBRICATING OIL, SHIPBOARD INTERNAL COMBUSTION ENGINE, HIGH OUTPUT DIESEL
MIL L 2104 : F LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, COMBAT TACTICAL SERVICE
ASTM D 7740 : 2011 : R2016 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
ASTM D 4997 : 1989 Test Methods for Evaluation of Water Sensitivity of Multi-Purpose Power Transmission Fluids (Withdrawn 1995)

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