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ASTM D 4821 : 2020

Current
Current

The latest, up-to-date edition.

Standard Guide for Carbon Black—Validation of Test Method Precision and Bias
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

11-26-2020

1.1This guide covers procedures for using the ASTM Standard Reference Blacks2 (SRBs) and the HT and INR Iodine Number Standards to continuously monitor the precision of those carbon black test methods for which reference values have been established. It also offers guidelines for troubleshooting various test methods.

1.2This guide defines the environmental conditions that are required for laboratories that perform carbon black testing activities for those test methods under D24’s jurisdiction.

1.3This guide establishes procedures for the use of x-charts to continuously monitor those tests listed in Section 2 for within-lab precision (repeatability) and between-lab accuracy (reproducibility).

1.4This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the reference values of the ASTM reference blacks, within the ranges given in this guide.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 24
DocumentType
Guide
Pages
14
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 3324 : 2001 : REV A Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks (Withdrawn 2002)
ASTM D 2414 : 2022 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 3493 : 2020 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 3493 : 2021 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
ASTM D 1765 : 2023 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1510 : 2019 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 2414 : 2023 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1510 : 2024 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3265 : 2023 Standard Test Method for Carbon Black—Tint Strength
ASTM D 1765 : 2019 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 2414 : 2019 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM E 2282 : 2023 Standard Guide for Defining the Test Result of a Test Method
ASTM D 1765 : 2001 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 3265 : 2024 Standard Test Method for Carbon Black—Tint Strength
ASTM E 2282 : 2014 : R2019 Standard Guide for Defining the Test Result of a Test Method
ASTM D 3265 : 2019 : REV B Standard Test Method for Carbon Black—Tint Strength
ASTM D 7854 : 2018 : REV C : EDT 1 Standard Test Method for Carbon Black-Void Volume at Mean Pressure
ASTM E 2282 : 2014 : R2023 Standard Guide for Defining the Test Result of a Test Method
ASTM D 1510 : 2021 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 3265 : 2021 Standard Test Method for Carbon Black—Tint Strength
ASTM D 3265 : 2023 : REV A Standard Test Method for Carbon Black—Tint Strength
ASTM D 2414 : 2001 Standard Test Method for Carbon Black—Oil Absorption Number
ASTM D 6556 : 2019 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 1765 : 2021 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 6556 : 2021 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
ASTM D 2414 : 2023 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 1513 : 2005 : R2017 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 1765 : 2023 : REV B Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1765 : 2023 Standard Classification System for Carbon Blacks Used in Rubber Products
ASTM D 1513 : 2005 : R2023 Standard Test Method for Carbon Black, Pelleted—Pour Density
ASTM D 2414 : 2021 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM D 7854 : 2021 Standard Test Method for Carbon Black-Void Volume at Mean Pressure
ASTM D 1510 : 2023 Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1510 : 2023 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
ASTM D 1765 : 2022 Standard Classification System for Carbon Blacks Used in Rubber Products

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