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ASTM D 5384 : 1995 : R2000 : EDT 1

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

04-10-2000

1.1 These test methods cover the determination of chlorine in used oils, fuels, and related materials, including: crankcase, hydraulic, diesel, lubricating and fuel oils, and kerosene, all containing <25% (mass/mass) water.

1.1.1 Bromide and iodide are also titrated and reported on a molar basis as chlorine.

1.2 The entire analytical sequence, including sampling, sample pretreatment, chemical reactions, extraction, and quantification, is available in kit form using predispensed and encapsulated reagents. The overall objective is to provide a simple, easy to use procedure, permitting nontechnical personnel to perform a test in or outside of the laboratory environment in under 10 min. The test method also gives information to run the test without a kit.

1.2.1 Method A is preset to provide a greater than or less than result at 1000 mg/kg (ppm) total chlorine to meet regulatory requirements for used oils.

1.2.2 Method B provides results over a range from 200 to 4000 mg/kg total chlorine.

1.3 For both methods, positive bias will result from samples that contain greater than 3% (mass/mass) total sulfur. While a false negative result will not occur, other analytical methods should be used on high sulfur oils.

1.4 Method B Lower Limit of Quantitation -In the round- robin study to develop statistics for this method, participants were asked to report results to the nearest 100 mg/kg. The lower limit of quantification could therefore only be determined to be in the range from 870 to 1180 mg/kg .

1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety statements are given in Section 3.

Committee
D 02
DocumentType
Test Method
Pages
4
ProductNote
Reconfirmed EDT 1
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 6823 : 2008 : R2013 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants

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US$66.00
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