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ASTM D 5847 : 1999 : REV A : EDT 1

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

12-31-2010

1.1 This practice provides specific, mandatory requirements for incorporating quality control (QC) procedures into all test methods under the jurisdiction of committee D19.

1.2 Required QC sections in all applicable test methods are intended to achieve two goals. First, users of Committee D19 test methods will be able to demonstrate a minimum competency in the performance of these test methods by comparison with collaborative study data. Second, all users of test methods will be required to perform a minimum level of QC as part of proper implementation of these test methods to ensure ongoing competency.

1.3 This practice contains the primary requirements for QC of a specific test method. In many cases, it may be desirable to implement additional QC requirements to assure the desired quality of data.

1.4 The specific requirements in this practice may not be applicable to all test methods. These requirements may vary depending on the type of test method used as well as the analyte being determined and the sample matrix being analyzed. See Explanation 1 in Appendix X1.

1.5 This practice is for use with quantitative methods and may not be applicable to qualitative test methods.

1.6 Presently, this practice is applicable primarily to chemical test methods. It is intended that, in future revisions, the practice will be expanded to include other methods such as microbiological methods.

Committee
D 19
DocumentType
Standard Practice
Pages
11
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

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ASTM D 4517 : 2015 Standard Test Method for Low-Level Total Silica in High-Purity Water by Flameless Atomic Absorption Spectroscopy
ASTM D 5996 : 2016 Standard Test Method for Measuring Anionic Contaminants in High-Purity Water by On-Line Ion Chromatography
ASTM D 3645 : 2015 Standard Test Methods for Beryllium in Water
ASTM D 7575 : 2011 : R2017 Standard Test Method for Solvent-Free Membrane Recoverable Oil and Grease by Infrared Determination
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ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
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ASTM D 7168 : 2016 Standard Test Method for <sup>99</sup>Tc in Water by Solid Phase Extraction Disk
ASTM D 8001 : 2016 : EDT 1 Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography
ASTM D 3869 : 2015 Standard Test Methods for Iodide and Bromide Ions in Brackish Water, Seawater, and Brines
ASTM D 1253 : 2014 Standard Test Method for Residual Chlorine in Water
ASTM D 7979 : 2017 Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 8024 : 2016 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Water by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 3223 : 2017 Standard Test Method for Total Mercury in Water
ASTM D 3867 : 2016 Standard Test Methods for Nitrite-Nitrate in Water
ASTM D 3868 : 2015 Standard Test Method for Fluoride Ions in Brackish Water, Seawater, and Brines
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 4785 : 2008 : R2013 : EDT 1 Standard Test Method for Low-Level Analysis of Iodine Radioisotopes in Water
ASTM D 1691 : 2017 Standard Test Methods for Zinc in Water
ASTM D 1246 : 2016 Standard Test Method for Bromide Ion in Water
ASTM D 3590 : 2017 Standard Test Methods for Total Kjeldahl Nitrogen in Water
ASTM D 4012 : 2015 Standard Test Method for Adenosine Triphosphate (ATP) Content of Microorganisms in Water
ASTM D 7066 : 2004 : R2017 Standard Test Method for dimer/trimer of chlorotrifluoroethylene (S-316) Recoverable Oil and Grease and Nonpolar Material by Infrared Determination
ASTM D 3986 : 2017 Standard Test Method for Barium in Brines, Seawater, and Brackish Water by Direct-Current Argon Plasma Atomic Emission Spectroscopy
ASTM D 1179 : 2016 Standard Test Methods for Fluoride Ion in Water
ASTM D 7572 : 2015 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
ASTM D 8243 : 2019 Standard Test Method for Determination of APS Reductase to Estimate Sulfate Reducing Bacterial Bioburdens in Water – Enzyme-Linked Immunosorbent Assay Method
ASTM D 2460 : 2007 : R2013 Standard Test Method for Alpha-Particle-Emitting Isotopes of Radium in Water (Withdrawn 2022)
ASTM D 3919 : 2015 Standard Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
ASTM D 1426 : 2015 Standard Test Methods for Ammonia Nitrogen In Water
ASTM D 3557 : 2017 Standard Test Methods for Cadmium in Water
ASTM D 7600 : 2016 : R2017 Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3558 : 2015 Standard Test Methods for Cobalt in Water
ASTM D 5542 : 2016 Standard Test Methods for Trace Anions in High Purity Water by Ion Chromatography
ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 4130 : 2015 Standard Test Method for Sulfate Ion in Brackish Water, Seawater, and Brines (Withdrawn 2024)
ASTM D 1429 : 2013 Standard Test Methods for Specific Gravity of Water and Brine (Withdrawn 2022)
ASTM D 6238 : 1998 : R2017 Standard Test Method for Total Oxygen Demand in Water
ASTM D 4192 : 2015 Standard Test Method for Potassium in Water by Atomic Absorption Spectrophotometry
ASTM D 8083 : 2016 Standard Test Method for Total Nitrogen, and Total Kjeldahl Nitrogen (TKN) by Calculation, in Water by High Temperature Catalytic Combustion and Chemiluminescence Detection
ASTM D 6239 : 2009 : R2015 Standard Test Method for Uranium in Drinking Water by High-Resolution Alpha-Liquid-Scintillation Spectrometry
ASTM D 858 : 2017 Standard Test Methods for Manganese in Water
ASTM D 6919 : 2017 Standard Test Method for Determination of Dissolved Alkali and Alkaline Earth Cations and Ammonium in Water and Wastewater by Ion Chromatography
ASTM D 1385 : 2007 : R2018 : EDT 1 Standard Test Method for Hydrazine in Water
ASTM D 7574 : 2016 Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3372 : 2017 Standard Test Method for Molybdenum in Water
ASTM D 511 : 2014 Standard Test Methods for Calcium and Magnesium In Water
ASTM D 3559 : 2015 Standard Test Methods for Lead in Water (Withdrawn 2024)
ASTM D 4839 : 2003 : R2017 Standard Test Method for Total Carbon and Organic Carbon in Water by Ultraviolet, or Persulfate Oxidation, or Both, and Infrared Detection
ASTM D 7939 : 2015 Standard Test Method for Rapid Radiochemical Determination of Americium-241 in Water (Withdrawn 2024)
ASTM D 3875 : 2015 Standard Test Method for Alkalinity in Brackish Water, Seawater, and Brines
ASTM D 6071 : 2014 Standard Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy
ASTM D 5811 : 2008 : R2013 Standard Test Method for Strontium-90 in Water
ASTM D 4191 : 2015 Standard Test Method for Sodium in Water by Atomic Absorption Spectrophotometry
ASTM D 8026 : 2016 Standard Practice for Determination of Tc-99 in Water by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM D 513 : 2016 Standard Test Methods for Total and Dissolved Carbon Dioxide in Water
ASTM D 7678 : 2017 Standard Test Method for Total Oil and Grease (TOG) and Total Petroleum Hydrocarbons (TPH) in Water and Wastewater with Solvent Extraction using Mid-IR Laser Spectroscopy
ASTM D 5673 : 2016 Standard Test Method for Elements in Water by Inductively Coupled Plasma—Mass Spectrometry
ASTM D 512 : 2012 Standard Test Methods for Chloride Ion In Water (Withdrawn 2021)
ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 516 : 2016 Standard Test Method for Sulfate Ion in Water
ASTM D 6855 : 2017 Standard Test Method for Determination of Turbidity Below 5 NTU in Static Mode
ASTM D 6501 : 2015 Standard Test Method for Phosphonate in Brines
ASTM D 1783 : 2001 : R2012 : EDT 1 Standard Test Methods for Phenolic Compounds in Water
ASTM D 7644 : 2016 Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 1126 : 2017 Standard Test Method for Hardness in Water
ASTM D 4691 : 2017 Standard Practice for Measuring Elements in Water by Flame Atomic Absorption Spectrophotometry
ASTM D 8064 : 2016 Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams
ASTM D 1067 : 2016 Standard Test Methods for Acidity or Alkalinity of Water
ASTM D 7283 : 2017 Standard Test Method for Alpha and Beta Activity in Water By Liquid Scintillation Counting
ASTM D 4165 : 2006 : R2012 Standard Test Method for Cyanogen Chloride in Water
ASTM D 4922 : 2009 : R2016 : EDT 1 Standard Test Method for Determination of Radioactive Iron in Water
ASTM D 7597 : 2016 : R2017 Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Hydrogen Dimethylamidophosphate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Water by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 857 : 2017 Standard Test Method for Aluminum in Water
ASTM D 8025 : 2016 Standard Test Method for Determination of Select Pesticides in Water by Multiple Reaction Monitoring Liquid Chromatography Tandem Mass Spectrometry
ASTM D 3697 : 2017 Standard Test Method for Antimony in Water
ASTM D 7485 : 2016 Standard Test Method for Determination of Nonylphenol, p-<emph type="bdit">tert</emph >-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 5072 : 2009 : R2016 Standard Test Method for Radon in Drinking Water
ASTM D 3373 : 2017 Standard Test Method for Vanadium in Water
ASTM D 3082 : 2015 Standard Test Method for Boron in Water
ASTM D 7535 : 2009 : R2015 Standard Test Method for Lead-210 in Water (Withdrawn 2024)
ASTM D 7742 : 2017 Standard Practice for Determination of Nonylphenol Polyethoxylates (NPnEO, 3 ≤ n ≤ 18) and Octylphenol Polyethoxylates (OPnEO, 2 ≤ n ≤ 12) in Water by Single Reaction Monitoring (SRM) Liquid Chromatography/ Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 3651 : 2016 Standard Test Method for Barium in Brackish Water, Seawater, and Brines
ASTM D 1068 : 2015 Standard Test Methods for Iron in Water
ASTM D 859 : 2016 Standard Test Method for Silica in Water
ASTM D 4458 : 2015 Standard Test Method for Chloride Ions in Brackish Water, Seawater, and Brines
ASTM D 7599 : 2016 : R2017 Standard Test Method for Determination of Diethanolamine, Triethanolamine, <emph type="ital">N</emph>-Methyldiethanolamine and <emph type="ital">N</emph >-Ethyldiethanolamine in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 1688 : 2017 Standard Test Methods for Copper in Water
ASTM D 1886 : 2014 Standard Test Methods for Nickel in Water
ASTM D 5904 : 2002 : R2017 Standard Test Method for Total Carbon, Inorganic Carbon, and Organic Carbon in Water by Ultraviolet, Persulfate Oxidation, and Membrane Conductivity Detection
ASTM D 3865 : 2009 : R2015 Standard Test Method for Plutonium in Water (Withdrawn 2024)
ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 5463 : 2018 Standard Guide for Use of Test Kits to Measure Inorganic Constituents in Water
ASTM D 5907 : 2018 Standard Test Methods for Filterable Matter (Total Dissolved Solids) and Nonfilterable Matter (Total Suspended Solids) in Water
ASTM D 5811 : 2020 Standard Test Method for Strontium-90 in Water
ASTM D 888 : 2018 Standard Test Methods for Dissolved Oxygen in Water
ASTM D 5176 : 2020 Standard Test Method for Total Chemically Bound Nitrogen in Water by Pyrolysis and Chemiluminescence Detection
ASTM D 3866 : 2018 Standard Test Methods for Silver in Water
ASTM D 7284 : 2020 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 1252 : 2006 : R2020 Standard Test Methods for Chemical Oxygen Demand (Dichromate Oxygen Demand) of Water
ASTM D 7979 : 2020 Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent, and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 7573 : 2018 : REV A : EDT 1 Standard Test Method for Total Carbon and Organic Carbon in Water by High Temperature Catalytic Combustion and Infrared Detection
ASTM D 6800 : 2018 Standard Practice for Preparation of Water Samples Using Reductive Precipitation Preconcentration Technique for ICP-MS Analysis of Trace Metals
ASTM D 3920 : 2018 Standard Test Method for Strontium in Water
ASTM D 6850 : 2018 Standard Guide for QC of Screening Methods in Water
ASTM D 1783 : 2001 : R2020 Standard Test Methods for Phenolic Compounds in Water
ASTM D 6581 : 2018 Standard Test Methods for Bromate, Bromide, Chlorate, and Chlorite in Drinking Water by Suppressed Ion Chromatography
ASTM D 8018 : 2015 : R2020 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 1976 : 2020 Standard Test Method for Elements in Water by Inductively-Coupled Plasma Atomic Emission Spectroscopy
ASTM D 4785 : 2020 Standard Test Method for Low-Level Analysis of Iodine Radioisotopes in Water
ASTM D 6508 : 2015 Standard Test Method for Determination of Dissolved Inorganic Anions in Aqueous Matrices Using Capillary Ion Electrophoresis and Chromate Electrolyte
ASTM D 2330 : 2020 Standard Test Method for Methylene Blue Active Substances
ASTM D 4193 : 2008 : R2020 : EDT 1 Standard Test Method for Thiocyanate in Water
ASTM D 8361 : 2020 Standard Test Method for Total Organic Carbon in Water by Two Stage Wet Chemical Catalyzed Hydroxyl Radical Oxidation with Infra-Red Detection of Resulting Carbon Dioxide
ASTM D 3859 : 2015 Standard Test Methods for Selenium in Water
ASTM D 4382 : 2018 Standard Test Method for Barium in Water, Atomic Absorption Spectrophotometry, Graphite Furnace
ASTM D 4165 : 2006 : R2020 : EDT 1 Standard Test Method for Cyanogen Chloride in Water
ASTM D 2972 : 2015 Standard Test Methods for Arsenic in Water
ASTM D 7645 : 2016 Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 7598 : 2016 : R2017 Standard Test Method for Determination of Thiodiglycol in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry
ASTM D 3454 : 2018 Standard Test Method for Radium-226 in Water
ASTM D 7065 : 2017 Standard Test Method for Determination of Nonylphenol, Bisphenol A, <emph type="bdit" >p-tert</emph>-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry
ASTM D 3561 : 2016 Standard Test Method for Lithium, Potassium, and Sodium Ions in Brackish Water, Seawater, and Brines by Atomic Absorption Spectrophotometry
ASTM D 5257 : 2017 Standard Test Method for Dissolved Hexavalent Chromium in Water by Ion Chromatography
ASTM D 8018 : 2015 Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS)
ASTM D 4282 : 2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 5174 : 2007 : R2013 Standard Test Method for Trace Uranium in Water by Pulsed-Laser Phosphorimetry (Withdrawn 2022)
ASTM D 4658 : 2015 Standard Test Method for Sulfide Ion in Water (Withdrawn 2024)
ASTM D 4193 : 2008 : R2013 : EDT 1 Standard Test Method for Thiocyanate in Water
ASTM D 6994 : 2015 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 4190 : 2015 Standard Test Method for Elements in Water by Direct-Current Plasma Atomic Emission Spectroscopy
ASTM D 7365 : 2009 : REV A : R2015 Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
ASTM D 7315 : 2017 Standard Test Method for Determination of Turbidity Above 1 Turbidity Unit (TU) in Static Mode
ASTM D 3972 : 2009 : R2015 Standard Test Method for Isotopic Uranium in Water by Radiochemistry (Withdrawn 2024)
ASTM D 7968 : 2017 : REV A Standard Test Method for Determination of Polyfluorinated Compounds in Soil by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 4327 : 2017 Standard Test Method for Anions in Water by Suppressed Ion Chromatography

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