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ASTM D 6417 : 2015 : R2019

Current
Current

The latest, up-to-date edition.

Standard Test Method for Estimation of Engine Oil Volatility by Capillary Gas Chromatography
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

12-01-2019

1.1This test method covers an estimation of the amount of engine oil volatilized at 371 °C (700 °F).

1.1.1This test method can also be used to estimate the amount of oil volatilized at any temperature between 126 °C and 371 °C, if so desired.

1.2This test method is limited to samples having an initial boiling point (IBP) greater than 126 °C (259 °F) or the first calibration point and to samples containing lubricant base oils with end points less than 615 °C (1139 °F) or the last n-paraffins in the calibration mixture. By using some instruments and columns, it is possible to extend the useful range of the test method.

1.3This test method uses the principles of simulated distillation methodology.

1.4This test method may be applied to both lubricant oil base stocks and finished lubricants containing additive packages. These additive packages generally contain high molecular weight, nonvolatile components that do not elute from the chromatographic column under the test conditions. The calculation procedure used in this test method assumes that all of the sample elutes from the column and is detected with uniform response. This assumption is not true for samples with nonvolatile additives, and application of this test method under such conditions will yield results higher than expected. For this reason, results by this test method are reported as area percent of oil.

1.5The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are provided for information only.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
11
ProductNote
THIS STANDARD ALSO REFERES TO CEC L-40–93
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 4485 : 2019 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 6074 : 2015 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils

ASTM D 5800 : 2018 : REV A Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM E 1510 : 1995 : R2013 : EDT 1 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM D 6352 : 1998 Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700&#176C by Gas Chromatography
ASTM D 5800 : 2019 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 2887 : 2022 : EDT 1 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM D 6352 : 2019 : EDT 1 Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
ASTM D 2887 : 2022 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM D 2887 : 2019 : REV A : EDT 1 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM E 1510 : 1995 : R2021 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 2887 : 2023 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM D 4626 : 1995 : R2019 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 5800 : 2021 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 6352 : 2019 Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography
ASTM D 4626 : 2023 Standard Practice for Calculation of Gas Chromatographic Response Factors
ASTM D 2887 : 2019 : REV A Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM D 5800 : 2020 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 5800 : 2019 : REV A Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 2887 : 2019 : REV A : EDT 2 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
ASTM D 6352 : 2015 Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 °C to 700 °C by Gas Chromatography

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