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ASTM D 7039 : 2013

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

09-15-2013

1.1This test method covers the determination of total sulfur by monochromatic wavelength-dispersive X-ray fluorescence (MWDXRF) spectrometry in single-phase gasoline, diesel fuel, refinery process streams used to blend gasoline and diesel, jet fuel, kerosine, biodiesel, biodiesel blends, and gasoline-ethanol blends.

Note 1Volatile samples such as high-vapor-pressure gasolines or light hydrocarbons might not meet the stated precision because of the evaporation of light components during the analysis.

1.2The range of this test method is between the pooled limit of quantitation (PLOQ) value (calculated by procedures consistent with Practice D6259) of 3.2 mg/kg total sulfur and the highest level sample in the round robin, 2822 mg/kg total sulfur.

1.3Samples containing oxygenates can be analyzed with this test method provided the matrix of the calibration standards is either matched to the sample matrices or the matrix correction described in Section 5 or Annex A1 is applied to the results. The conditions for matrix matching and matrix correction are provided in the Interferences section (Section 5).

1.4Samples with sulfur content above 2822 mg/kg can be analyzed after dilution with appropriate solvent (see 5.4). The precision and bias of sulfur determinations on diluted samples has not been determined and may not be the same as shown for neat samples (Section 15).

1.5When the elemental composition of the samples differ significantly from the calibration standards used to prepare the calibration curve, the cautions and recommendation in Section 5 should be carefully observed.

1.6The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see 3.1.

Committee
D 02
DocumentType
Test Method
Pages
11
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 4814 : 2019 Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 8076 : 2018 Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
ASTM D 8048 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 4529 : 2017 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 396 : 2019 Standard Specification for Fuel Oils
ASTM D 4806 : 2019 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

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US$83.00
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