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ASTM D 7365 : 2009 : REV A : R2015

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide
Available format(s)

Hardcopy , PDF

Superseded date

06-18-2022

Language(s)

English

Published date

08-05-2015

CONTAINED IN VOL. 11.02, 2015 Specifies the collection and preservation of water samples for the analysis of cyanide.

1.1This practice is applicable for the collection and preservation of water samples for the analysis of cyanide. This practice addresses the mitigation of known interferences prior to the analysis of cyanide. Responsibilities of field sampling personnel and the laboratory are indicated.

1.2The sampling, preservation and mitigation of interference procedures described in this practice are recommended for the analysis of total cyanide, available cyanide, weak acid dissociable cyanide, and free cyanide by Test Methods D2036, D4282, D4374, D6888, D6994, D7237, D7284, and D7511. The information supplied in this practice can also be applied to other analytical methods for cyanide, for example, EPA Method 335.4.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
D 19
DocumentType
Standard Practice
Pages
11
ProductNote
Reconfirmed 2015
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 4193 : 2008 : R2013 : EDT 1 Standard Test Method for Thiocyanate in Water
ASTM E 800 : 2014 Standard Guide for Measurement of Gases Present or Generated During Fires
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 7572 : 2015 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 7728 : 2018 Standard Guide for Selection of ASTM Analytical Methods for Implementation of International Cyanide Management Code Guidance
ASTM D 7295 : 2018 Standard Practice for Sampling Combustion Effluents and Other Stationary Sources for the Subsequent Determination of Hydrogen Cyanide
ASTM D 2036 : 2009 : R2022 Standard Test Methods for Cyanides in Water
ASTM D 7572 : 2015 : R2022 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
ASTM D 7284 : 2020 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 4193 : 2008 : R2020 : EDT 1 Standard Test Method for Thiocyanate in Water
ASTM E 800 : 2020 Standard Guide for Measurement of Gases Present or Generated During Fires

ASTM D 4840 : 1999 : R2018 : EDT 1 Standard Guide for Sample Chain-of-Custody Procedures
ASTM D 6994 : 2010 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 4282 : 2002 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 3694 : 1996 : R2011 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 4841 : 1988 : R2008 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 3370 : 1995 : REV A : R2003 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
ASTM D 4411 : 2003 : R2014 : EDT 1 Standard Guide for Sampling Fluvial Sediment in Motion
ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 4282 : 2002 : R2010 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 4841 : 1988 : R2018 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 7511 : 2009 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 2036 : 1991 Standard Test Methods for Cyanides in Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3694 : 1996 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 6888 : 2003 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 6696 : 2016 : REDLINE Standard Guide for Understanding Cyanide Species
ASTM D 7284 : 2013 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 6994 : 2004 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 6696 : 2016 Standard Guide for Understanding Cyanide Species
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 4841 : 1988 : R1998 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 4282 : 1995 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 6696 : 2010 Standard Guide for Understanding Cyanide Species
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 6696 : 2014 Standard Guide for Understanding Cyanide Species
ASTM D 4841 : 1988 : R2003 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 3370 : 2010 Standard Practices for Sampling Water from Closed Conduits
ASTM D 6994 : 2015 : REDLINE Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 4282 : 2015 : REDLINE Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 4841 : 1988 : R2013 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 6696 : 2005 : EDT 1 Standard Guide for Understanding Cyanide Species
ASTM D 4282 : 2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 4374 : 2006 Standard Test Methods for Cyanides in Water-Automated Methods for Total Cyanide, Weak Acid Dissociable Cyanide, and Thiocyanate (Withdrawn 2013)
ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
ASTM D 3370 : 2008 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 2036 : 1998 Standard Test Methods for Cyanides in Water
ASTM D 6888 : 2009 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 6888 : 2004 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 3694 : 1996 : R2004 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 6696 : 2005 Standard Guide for Understanding Cyanide Species
ASTM D 7511 : 2009 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 7511 : 2012 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 4411 : 1998 Standard Guide for Sampling Fluvial Sediment in Motion
ASTM D 2036 : 2009 Standard Test Methods for Cyanides in Water
ASTM D 7284 : 2008 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 7284 : 2008 : EDT 1 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 7237 : 2010 Standard Test Method for Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 4411 : 2003 : R2019 Standard Guide for Sampling Fluvial Sediment in Motion
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 7237 : 2015 : REV A Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 7237 : 2006 Standard Test Method for Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 3370 : 2018 Standard Practices for Sampling Water from Flowing Process Streams
ASTM D 6696 : 2001 Standard Guide for Understanding Cyanide Species
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3370 : 1976 Standard Practices for Sampling Water
ASTM D 4374 : 2000 Standard Test Methods for Cyanides in Water--Automated Methods for Total Cyanide, Acid dissociable Cyanide, and Thiocyanate
ASTM D 4282 : 1995 : R2001 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 4841 : 1988 : R2013 : EDT 1 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 3370 : 1995 : REV A : R1999 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 3370 : 2007 Standard Practices for Sampling Water from Closed Conduits
ASTM D 2036 : 2006 Standard Test Methods for Cyanides in Water
ASTM D 4411 : 2003 : R2008 Standard Guide for Sampling Fluvial Sediment in Motion
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 7511 : 2009 : EDT 2 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 7237 : 2015 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 6994 : 2015 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 6888 : 2016 : REDLINE Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
ASTM D 4282 : 2002 : R2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
ASTM D 4411 : 2003 : R2014 Standard Guide for Sampling Fluvial Sediment in Motion
ASTM D 4411 : 2003 Standard Guide for Sampling Fluvial Sediment in Motion

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