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  • ASTM D 7365 : 2009 : REV A : R2015

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    Standard Practice for Sampling, Preservation and Mitigating Interferences in Water Samples for Analysis of Cyanide

    Available format(s):  Hardcopy, PDF

    Superseded date:  06-18-2022

    Language(s):  English

    Published date:  08-05-2015

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 11.02, 2015 Specifies the collection and preservation of water samples for the analysis of cyanide.

    Scope - (Show below) - (Hide below)

    1.1This practice is applicable for the collection and preservation of water samples for the analysis of cyanide. This practice addresses the mitigation of known interferences prior to the analysis of cyanide. Responsibilities of field sampling personnel and the laboratory are indicated.

    1.2The sampling, preservation and mitigation of interference procedures described in this practice are recommended for the analysis of total cyanide, available cyanide, weak acid dissociable cyanide, and free cyanide by Test Methods D2036, D4282, D4374, D6888, D6994, D7237, D7284, and D7511. The information supplied in this practice can also be applied to other analytical methods for cyanide, for example, EPA Method 335.4.

    1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 19
    Document Type Standard Practice
    Product Note Reconfirmed 2015
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 4193 : 2008 : R2013 : EDT 1 Standard Test Method for Thiocyanate in Water
    ASTM E 800 : 2014 Standard Guide for Measurement of Gases Present or Generated During Fires
    ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
    ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 7572 : 2015 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
    ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 7728 : 2018 Standard Guide for Selection of ASTM Analytical Methods for Implementation of International Cyanide Management Code Guidance
    ASTM D 7295 : 2018 Standard Practice for Sampling Combustion Effluents and Other Stationary Sources for the Subsequent Determination of Hydrogen Cyanide
    ASTM D 2036 : 2009 : R2022 Standard Test Methods for Cyanides in Water
    ASTM D 7572 : 2015 : R2022 Standard Guide for Recovery of Aqueous Cyanides by Extraction from Mine Rock and Soil
    ASTM D 7284 : 2020 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 4193 : 2008 : R2020 : EDT 1 Standard Test Method for Thiocyanate in Water
    ASTM E 800 : 2020 Standard Guide for Measurement of Gases Present or Generated During Fires

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4840 : 1999 : R2018 : EDT 1 Standard Guide for Sample Chain-of-Custody Procedures
    ASTM D 6994 : 2010 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
    ASTM D 4282 : 2002 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 3694 : 1996 : R2011 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
    ASTM D 4841 : 1988 : R2008 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 3370 : 1995 : REV A : R2003 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
    ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
    ASTM D 4411 : 2003 : R2014 : EDT 1 Standard Guide for Sampling Fluvial Sediment in Motion
    ASTM D 1129 : 2013 : REDLINE Standard Terminology Relating to Water
    ASTM D 1129 : 2003 Standard Terminology Relating to Water
    ASTM D 4282 : 2002 : R2010 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 4841 : 1988 : R2018 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 1129 : 2013 Standard Terminology Relating to Water
    ASTM D 7511 : 2009 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 7237 : 2018 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
    ASTM D 2036 : 1991 Standard Test Methods for Cyanides in Water
    ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
    ASTM D 3694 : 1996 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
    ASTM D 6888 : 2003 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 6696 : 2016 : REDLINE Standard Guide for Understanding Cyanide Species
    ASTM D 7284 : 2013 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 6994 : 2004 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
    ASTM D 6696 : 2016 Standard Guide for Understanding Cyanide Species
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 4841 : 1988 : R1998 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
    ASTM D 4282 : 1995 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 6888 : 2016 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 6696 : 2010 Standard Guide for Understanding Cyanide Species
    ASTM D 1129 : 2006 Standard Terminology Relating to Water
    ASTM D 6696 : 2014 Standard Guide for Understanding Cyanide Species
    ASTM D 4841 : 1988 : R2003 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 3370 : 2010 Standard Practices for Sampling Water from Closed Conduits
    ASTM D 6994 : 2015 : REDLINE Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
    ASTM D 4282 : 2015 : REDLINE Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 4841 : 1988 : R2013 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 6696 : 2005 : EDT 1 Standard Guide for Understanding Cyanide Species
    ASTM D 4282 : 2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
    ASTM D 4374 : 2006 Standard Test Methods for Cyanides in Water-Automated Methods for Total Cyanide, Weak Acid Dissociable Cyanide, and Thiocyanate (Withdrawn 2013)
    ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
    ASTM D 2036 : 2009 : R2015 Standard Test Methods for Cyanides in Water
    ASTM D 3370 : 2008 Standard Practices for Sampling Water from Closed Conduits
    ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
    ASTM D 2036 : 1998 Standard Test Methods for Cyanides in Water
    ASTM D 6888 : 2009 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
    ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 6888 : 2004 Standard Test Method for Available Cyanide with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
    ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
    ASTM D 3694 : 1996 : R2004 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
    ASTM D 1129 : 2002 Standard Terminology Relating to Water
    ASTM D 6696 : 2005 Standard Guide for Understanding Cyanide Species
    ASTM D 7511 : 2009 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 7511 : 2012 : R2017 : EDT 1 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 7511 : 2012 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 4411 : 1998 Standard Guide for Sampling Fluvial Sediment in Motion
    ASTM D 2036 : 2009 Standard Test Methods for Cyanides in Water
    ASTM D 7284 : 2008 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 7284 : 2008 : EDT 1 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 7237 : 2010 Standard Test Method for Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 4411 : 2003 : R2019 Standard Guide for Sampling Fluvial Sediment in Motion
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 7237 : 2015 : REV A Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 7237 : 2006 Standard Test Method for Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
    ASTM D 1129 : 2004 Standard Terminology Relating to Water
    ASTM D 7284 : 2013 : R2017 Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
    ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
    ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
    ASTM D 3370 : 2018 Standard Practices for Sampling Water from Flowing Process Streams
    ASTM D 6696 : 2001 Standard Guide for Understanding Cyanide Species
    ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
    ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
    ASTM D 3370 : 1976 Standard Practices for Sampling Water
    ASTM D 4374 : 2000 Standard Test Methods for Cyanides in Water--Automated Methods for Total Cyanide, Acid dissociable Cyanide, and Thiocyanate
    ASTM D 4282 : 1995 : R2001 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 4841 : 1988 : R2013 : EDT 1 Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 3370 : 1995 : REV A : R1999 : EDT 1 Standard Practices for Sampling Water from Closed Conduits
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM D 1129 : 2010 Standard Terminology Relating to Water
    ASTM D 3370 : 2007 Standard Practices for Sampling Water from Closed Conduits
    ASTM D 2036 : 2006 Standard Test Methods for Cyanides in Water
    ASTM D 4411 : 2003 : R2008 Standard Guide for Sampling Fluvial Sediment in Motion
    ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
    ASTM D 7511 : 2009 : EDT 2 Standard Test Method for Total Cyanide by Segmented Flow Injection Analysis, In-Line Ultraviolet Digestion and Amperometric Detection
    ASTM D 1129 : 2001 Standard Terminology Relating to Water
    ASTM D 7237 : 2015 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 6994 : 2015 Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection
    ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 6888 : 2016 : REDLINE Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
    ASTM D 4282 : 2002 : R2015 Standard Test Method for Determination of Free Cyanide in Water and Wastewater by Microdiffusion
    ASTM D 4411 : 2003 : R2014 Standard Guide for Sampling Fluvial Sediment in Motion
    ASTM D 4411 : 2003 Standard Guide for Sampling Fluvial Sediment in Motion
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