Name: ASTM D 7598 : 2016
Brand: ASTM
Price: 75.00 USD

ASTM D 7598 : 2016

Superseded

Standard Test Method for Determination of Thiodiglycol in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry

Available format(s)

Hardcopy , PDF

Superseded date

06-07-2016

Language(s)

English

Published date

02-01-2016

Publisher

American Society for Testing and Materials

CONTAINED IN VOL. 11.02, 2017 Defines the determination of thiodiglycol (TDG) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS).

1.1This procedure covers the determination of thiodiglycol (TDG) in surface water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). TDG is qualitatively and quantitatively determined by this test method. This test method adheres to single reaction monitoring (SRM) mass spectrometry.

1.2This test method has been developed by US EPA Region 5 Chicago Regional Laboratory (CRL).

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4The Detection Verification Level (DVL) and Reporting Range for TDG are listed in Table 1.

1.4.1The DVL is required to be at a concentration at least 3 times below the reporting limit (RL) and have a signal/noise ratio greater than 3:1. Fig. 1 displays the signal/noise ratio at the DVL.

1.4.2The RL is the concentration of the level 1 calibration standard as shown in Table 2. The reporting limit for this test method is 100 μg/L.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee	D 19
DocumentType	Test Method
Pages	9
ProductNote	Reconfirmed 2016
PublisherName	American Society for Testing and Materials
Status	Superseded
Supersedes	ASTM D 7598 : 2009 : EDT 2

ASTM D 1129 : 2013 : REDLINE	Standard Terminology Relating to Water
ASTM D 2777 : 2013 : REDLINE	Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM E 2554 : 2013-05	PRACTICE FOR ESTIMATING AND MONITORING THE UNCERTAINTY OF TEST RESULTS OF A TEST METHOD USING CONTROL CHART TECHNIQUES