Skip to content
Please enter a keyword to search

  • ASTM E 200 : 2016 : REDLINE

    Current The latest, up-to-date edition.
    Add to Watchlist
    This Standard has been added successfully to your Watchlist.
    Please visit My Watchlist to see all standards that you are watching.
    Please log in or to add this standard to your Watchlist.
    We could not add this standard to your Watchlist.
    Please retry or contact support for assistance.
    We could not add this standard to your Watchlist.
    Please retry or contact support for assistance.
    You have already added this standard to your Watchlist.
    Visit My Watchlist to view the full list.

    Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis

    Available format(s):  PDF

    Language(s):  English

    Published date:  04-01-2016

    Publisher:  American Society for Testing and Materials

    Add to Watchlist

    Add To Cart

    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 15.05, 2017 Defines procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.

    Scope - (Show below) - (Hide below)

    1.1This practice covers procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.

    1.2The information in this practice is arranged as follows:

    Sections

    Referenced Documents

    2

    Terminology

    3

    Significance and Use

    4

    Apparatus

    5

    Temperature effects

    6

    Measurements

    7

    Reagents

    8

    Concentration of solutions

    9

    Mixing of solutions

    10

    Storage of solutions

    11

    Preparation and standardization of solutions

    12

    Precision and Bias

    13

    Sodium hydroxide solution, 0.02 to 1.0 meq/mL (N)

    14 to 19

    Hydrochloric acid, 0.02 to 1.0 meq/mL (N)

    20 to 28

    Sulfuric acid, 0.02 to 1.0 meq/mL (N)

    29 to 33

    Hydrochloric acid, special 1 meq/mL (N)

    34 to 38

    Sulfuric acid, special 1 meq/mL (N)

    39 to 43

    Silver nitrate solution, 0.1 meq/mL (N)

    44 to 48

    Ammonium thiocyanate solution, 0.1 meq/mL (N)

    49 to 53

    Iodine solution, 0.1 meq/mL (N)

    54 to 58

    Sodium thiosulfate solution, 0.1 meq/mL (N)

    59 to 63

    Potassium permanganate solution, 0.1 meq/mL (N)

    64 to 68

    Potassium dichromate solution, 0.1 meq/mL(N)

    69 to 73

    Methanolic sodium hydroxide solution, 0.5 meq/mL (N)

    74 to 79

    Ceric sulfate solution, 0.1 meq/mL (N)

    80 to 84

    Acetous perchloric acid, 0.1 meq/mL (N)

    85 to 89

    Disodium ethylenediaminetetraacetate solution, 0.05 mol/L(M)

    90 to 94

    Standard ion solutions

    95

    Nonstandardized reagent solutions and indicator solutions

    96

    1.3The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given throughout this practice.

    General Product Information - (Show below) - (Hide below)

    Committee D 16
    Document Type Redline
    Publisher American Society for Testing and Materials
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 3566 : 2003 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
    ASTM D 5788 : 1995 : R2005 Standard Guide for Spiking Organics into Aqueous Samples
    ASTM E 1910/E1910M : 2015 : REDLINE Standard Test Method for Agricultural pH Control Agents, Measurement of pH Change and Buffering Capacity
    ASTM E 449:2008 Standard Test Methods for Analysis of Calcium Chloride
    ASTM D 297 : 2015 : REDLINE Standard Test Methods for Rubber Products—Chemical Analysis
    ASTM D 6363 : 1998 : R2003 : EDT 1 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
    ASTM D 3546 : 2005 : R2011 Standard Test Method for Formic Acid in Glacial Acetic Acid
    ASTM D 2790 : 1983 Methods of Analysis of Solvent Systems Used for Removal of Water-Formed Deposits (Withdrawn 1993)
    ASTM D 4274 : 2016 : REDLINE Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
    ASTM E 271 : 1998 Standard Test Methods for Analysis of Aqueous Hydrofluoric Acid (Withdrawn 2003)
    ASTM D 2192 : 2006 : R2012 Standard Test Method for Purity of Aldehydes and Ketones (Withdrawn 2021)
    ASTM D 3316 : 2006 Standard Test Method for Stability of Perchloroethylene with Copper
    ASTM D 1614 : 2009 : R2017 Standard Test Method for Alkalinity in Acetone
    ASTM D 4856 : 2011 Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis)
    ASTM D 888 : 2012-05 TEST METHODS FOR DISSOLVED OXYGEN IN WATER
    ASTM E 258 : 2007 : R2015 Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method (Withdrawn 2019)
    ASTM D 3316 : 2006 : R2016 Standard Test Method for Stability of Perchloroethylene with Copper
    ASTM E 1584 : 2017 : REDLINE Standard Test Method for Assay of Nitric Acid
    ASTM C 574 : 1984 : R1988 Method for Chemical Analyisis of Magnesite and Dolomite Refractories
    ASTM E 1147 : 1992 : R2005 Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography (Withdrawn 2013)
    ASTM D 2106 : 2007 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
    ASTM D 5810 : 1996 : R2011 Standard Guide for Spiking into Aqueous Samples
    ASTM D 3249 : 1995 : R2000 Standard Practice for General Ambient Air Analyzer Procedures
    ASTM D 4252 : 1989 : R2017 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
    ASTM D 5788 : 1995 Standard Guide for Spiking Organics into Aqueous Samples
    ASTM D 3089 : 1997 : R2008 Standard Practice for Determining the A-D Dimension of Aerosol Valve Dip Tubes
    ASTM D 2086 : 2008 Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde
    ASTM D 6363 : 1998 : R2013 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
    ASTM D 1417 : 2016 : REDLINE Standard Test Methods for Rubber Latices—Synthetic
    ASTM D 2086 : 2008 : R2012 Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde (Withdrawn 2021)
    ASTM D 1942 : 1980 Method of Test for Morpholine in Water
    ASTM D 5788 : 1995 : R2017 Standard Guide for Spiking Organics into Aqueous Samples
    ASTM E 1547 : 2009 Standard Terminology Relating to Industrial and Specialty Chemicals
    ASTM D 5916 : 1996 : R2002 Standard Test Method for Detection and Enumeration of Clostridium perfringens from Water and Extracted Sediments by Membrane Filtration (MF) (Withdrawn 2011)
    ASTM D 6328 : 2012-11 GUIDE FOR QUALITY ASSURANCE PROTOCOLS FOR CHEMICAL ANALYSIS OF ATMOSPHERIC WET DEPOSITION
    ASTM D 3316 : 2006 : R2011 Standard Test Method for Stability of Perchloroethylene with Copper
    ASTM D 1141 : 1998 : R2013 Standard Practice for the Preparation of Substitute Ocean Water
    ASTM D 2912 : 1976 : R1983 Test Method for Oxidant Content of the Atmosphere (Neutral KI) (Withdrawn 1990)
    ASTM D 3228 : 2008 : R2014 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
    MIL H 6083 : E HYDRAULIC FLUID, PETROLEUM BASE, FOR PRESERVATION AND OPERATION
    ASTM D 4252 : 1989 : R1995 : EDT 1 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
    ASTM D 5788 : 1995 : R2001 Standard Guide for Spiking Organics into Aqueous Samples
    ASTM E 1788 : 2016 : REDLINE Standard Test Method for Acidity in Acrylonitrile
    ASTM D 512 : 2012 Standard Test Methods for Chloride Ion In Water (Withdrawn 2021)
    MIL D 22346 : B DI-NORMAL-PROPYL ADIPATE (DNPA)
    ASTM E 442 : 1991 Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997)
    ASTM D 3566 : 2003 : R2009 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
    ASTM D 5788 : 1995 : R2011 Standard Guide for Spiking Organics into Aqueous Samples
    ASTM D 4415 : 2005 Standard Test Methods for Determination of Dimer in Acrylic Acid (Withdrawn 2011)
    ASTM D 6363 : 1998 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
    ASTM D 4224 : 1989 Test Method for Anionic Detergent by Para-Toluidine Hydrochloride (Withdrawn 1995)
    ASTM D 3566 : 2003 : R2014 Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion
    ASTM D 2379 : 2009 Standard Test Method for Acidity of Formaldehyde Solutions
    ASTM D 6303 : 1998 Standard Test Method for Formaldehyde in Water (Withdrawn 2007)
    ASTM D 1387 : 1989 : R2002 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
    ASTM D 6470 : 1999 : R2015 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
    ASTM D 3634 : 1999 : EDT 1 Standard Test Method for Trace Chloride Ion in Engine Coolants
    ASTM D 5810 : 1996 : R2006 Standard Guide for Spiking into Aqueous Samples
    ASTM D 3634 : 1999 : R2005 Standard Test Method for Trace Chloride Ion in Engine Coolants
    ASTM D 5810 : 1996 : R2015 Standard Guide for Spiking into Aqueous Samples
    ASTM E 257 : 1998 Standard Test Method for Sulfur in Organic Compounds by Sodium Peroxide Bomb Ignition
    ASTM D 345 : 2002 Side bearings of the freight wagon bogies. General specifications
    ASTM D 1387 : 1989 : R2007 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
    ASTM D 2942 : 2002 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
    ASTM E 1615 : 2016 : REDLINE Standard Test Method for Iron in Trace Quantities Using the FerroZine Method
    ASTM E 223 : 2016 : REDLINE Standard Test Methods for Analysis of Sulfuric Acid
    ASTM D 2382 : 1988 Test Method for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method) (Withdrawn 1994)
    ASTM D 4266 : 2017 : REDLINE Standard Test Methods for Precoat Capacity of Powdered Ion-Exchange Resins
    ASTM E 1910 : 2004 Test Method for Agricultural pH Control Agents
    ASTM D 240 : 2017 : REDLINE Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
    ASTM E 441 : 1990 Test Method for Vinyl Unsaturation in Organic Compounds with Mercuric Acetate (Withdrawn 1996)
    ASTM D 2106 : 2007 : R2017 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
    ASTM D 1067 : 2016 : REDLINE Standard Test Methods for Acidity or Alkalinity of Water
    ASTM D 1387 : 1989 : R2012 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
    ASTM D 2942 : 2002 : R2013 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
    ASTM E 567 : 1991 Test Method for Tertiary Hydroxyl Groups with Hydrogen Bromide (Withdrawn 1996)
    ASTM D 3249 : 1995 : R2005 Standard Practice for General Ambient Air Analyzer Procedures
    ASTM D 3634 : 1999 : R2015 Standard Test Method for Trace Chloride Ion in Engine Coolants
    ASTM D 7389 : 2007 Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes
    ASTM E 2677 : 2014 Standard Test Method for Determining Limits of Detection in Explosive Trace Detectors
    ASTM D 2195 : 2005 Standard Test Methods for Pentaerythritol (Withdrawn 2011)
    ASTM E 301 : 1994 Standard Test Method for Total Acidity of Organic Acids (Withdrawn 2001)
    ASTM D 5810 : 1996 Standard Guide for Spiking into Aqueous Samples
    ASTM D 7795 : 2015 : REDLINE Standard Test Method for Acidity in Ethanol and Ethanol Blends by Titration
    ASTM E 449 : 2008 : R2013 Standard Test Methods for Analysis of Calcium Chloride
    ASTM E 358 : 1995 Test Methods for Analysis of Phosphoric Acid (Withdrawn 2000)
    ASTM D 3634 : 1999 : R2009 Standard Test Method for Trace Chloride Ion in Engine Coolants
    AWWA B403 : 2016 ALUMINUM SULFATE - LIQUID, GROUND, OR LUMP
    ASTM D 2106 : 2007 : R2012 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
    ASTM E 819 : 1998 Standard Test Method for Trace Amounts of Arsenic in Organic Industrial Chemicals (Withdrawn 2003)
    ASTM E 234 : 1998 Standard Test Method for Total Bromine Number of Unsaturated Aliphatic Chemicals
    ASTM D 3546 : 2005 Standard Test Method for Formic Acid in Glacial Acetic Acid
    ASTM D 3546 : 2005 : R2019 Standard Test Method for Formic Acid in Glacial Acetic Acid
    ASTM D 1141 : 1998 : R2008 Standard Practice for the Preparation of Substitute Ocean Water
    ASTM D 3228 : 2008 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
    ASTM D 6470 : 1999 : R2010 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
    ASTM D 1141 : 1998 : EDT 1 Standard Practice for the Preparation of Substitute Ocean Water
    ASTM E 1228 : 2017 : REDLINE Standard Test Method for Assay of Peroxy Esters—Catalyzed Iodometric Procedure
    ASTM D 513 : 2016 : REDLINE Standard Test Methods for Total and Dissolved Carbon Dioxide in Water
    ASTM D 1614 : 2009 Standard Test Method for Alkalinity in Acetone
    ASTM E 1547 : 2009 : R2017 Standard Terminology Relating to Industrial and Specialty Chemicals
    ASTM D 7389 : 2007 : R2012 Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes
    ASTM D 2942 : 2002 : R2008 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
    ASTM D 5318 : 1997 Standard Test Method for Hydrolyzable Chloride in Peroxy Esters and Peroxy Dicarbonates (Withdrawn 2004)
    ASTM D 3249 : 1995 : R2011 Standard Practice for General Ambient Air Analyzer Procedures
    ASTM E 394 : 2015 : REDLINE Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
    ASTM E 534 : 2013-11 TEST METHODS FOR CHEMICAL ANALYSIS OF SODIUM CHLORIDE
    ASTM D 4252 : 1989 : R2003 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
    ASTM D 4252 : 1989 : R2009 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
    ASTM E 224 : 2016 : REDLINE Standard Test Methods for Analysis of Hydrochloric Acid
    GOST 849:2018 Primary nickel. SpecificationsE
    ASTM D 2192 : 2006 Standard Test Method for Purity of Aldehydes and Ketones
    ASTM D 6363 : 1998 : R2009 : EDT 1 Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method
    ASTM D 4249 : 1983 : R1998 Standard Test Method for Enumeration of Candida albicans in Water
    ASTM E 222 : 2017 : REDLINE Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation
    ASTM E 326 : 1996 Test Method for Hydroxyl Groups by Phthalic Anhydride Esterification (Withdrawn 2001)
    ASTM D 4249 : 1983 : R2005 Standard Test Method for Enumeration of Candida albicans in Water (Withdrawn 2013)
    ASTM E 335 : 1996 Standard Test Method for Hydroxyl Groups by Pyromellitic Dianhydride Esterification (Withdrawn 2003)
    ASTM E 233 : 1990 Test Method for Assay of N-Butyllithium Solutions (Withdrawn 1996)
    ASTM D 5810 : 1996 : R2001 Standard Guide for Spiking into Aqueous Samples
    ASTM E 1147 : 1992 : R1997 Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography
    ASTM D 1613 : 2017 : REDLINE Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
    ASTM C 500/C500M : 2007 : R2011 : EDT 1 Standard Test Methods for Asbestos-Cement Pipe
    ASTM D 3634 : 1999 : R2005 : EDT 1 Standard Test Method for Trace Chloride Ion in Engine Coolants
    ASTM E 778 : 2015 : REDLINE Standard Test Methods for Nitrogen in Refuse-Derived Fuel Analysis Samples
    ASTM D 1141 : 1998 : R2003 Standard Practice for the Preparation of Substitute Ocean Water
    ASTM E 258 : 2007 Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method
    ASTM D 5058 : 2012 : REDLINE Standard Practices for Compatibility of Screening Analysis of Waste
    ASTM E 359 : 2017 : REDLINE Standard Test Methods for Analysis of Soda Ash (Sodium Carbonate)
    ASTM D 1387 : 1989 : R1995 : EDT 1 Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes
    ASTM D 1386 : 2015 : REDLINE Standard Test Method for Acid Number (Empirical) of Synthetic and Natural Waxes
    ASTM D 6511/D6511M : 2011-07 TEST METHODS FOR SOLVENT BEARING BITUMINOUS COMPOUNDS
    ASTM D 6470 : 1999 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
    ASTM D 5916 : 1996 Standard Test Method for Detection and Enumeration of Clostridium perfringens from Water and Extracted Sediments by Membrane Filtration (MF)
    ASTM C 25 : 2017 : REDLINE TEST METHODS FOR CHEMICAL ANALYSIS OF LIMESTONE, QUICKLIME, AND HYDRATED LIME
    ASTM D 2379 : 2009 : R2017 Standard Test Method for Acidity of Formaldehyde Solutions
    ASTM D 3875 : 2015 : REDLINE Standard Test Method for Alkalinity in Brackish Water, Seawater, and Brines
    ASTM D 2106 : 2007 : EDT 1 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents
    ASTM D 6470 : 1999 : R2004 Standard Test Method for Salt in Crude Oils (Potentiometric Method)
    ASTM D 4856 : 2011 : R2016 Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis)

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 50 : 2017 : REDLINE Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E 180 : 2003 Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009)
    ASTM E 203 : 2016 : REDLINE Standard Test Method for Water Using Volumetric Karl Fischer Titration
    View more information

    • Access your standards online with a subscription

      Features

      • Simple online access to standards, technical information and regulations
      • Critical updates of standards and customisable alerts and notifications
      • Multi - user online standards collection: secure, flexibile and cost effective