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ASTM E 2838 : 2011 : R2016

Superseded
Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Determination of Thiodiglycol on Wipes by Solvent Extraction Followed by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
Available format(s)

Hardcopy , PDF

Superseded date

05-15-2021

Language(s)

English

Published date

09-25-2017

CONTAINED IN VOL. 15.08, 2017 Specifies the determination of thiodiglycol (TDG), also known as 2,2'-thiobis-ethanol, on wipes with 3,3'-thiodipropanol (TDP) as the surrogate.

1.1This procedure details the determination of thiodiglycol (TDG), also known as 2,2’-thiobis-ethanol, on wipes with 3,3’-thiodipropanol (TDP) as the surrogate. This method is based upon solvent extraction of wipes by either sonication or a pressurized fluid extraction (PFE) technique as an alternative option. The extract is filtered, concentrated and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). TDG is qualitatively and quantitatively determined.

1.2Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3The Method Detection Limit (MDL)2 and Reporting Range3 for TDG are listed in Table 1.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

(A)Chemical Abstract Service (CAS), A division of the American Chemical Society, 2540 Olentangy River Road, Columbus, OH, 43202, USA.

Committee
D 34
DocumentType
Test Method
Pages
10
ProductNote
Reconfirmed 2016
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

CFR 40(PTS100-149) : JUL 94 PROTECTION OF ENVIRONMENT - ENVIRONMENTAL PROTECTION AGENCY
ASTM D 653 : 2007 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 3740 : 2012-06 PRACTICE FOR MINIMUM REQUIREMENTS FOR AGENCIES ENGAGED IN TESTING AND/OR INSPECTION OF SOIL AND ROCK AS USED IN ENGINEERING DESIGN AND CONSTRUCTION
ASTM D 653 : 2020 : EDT 1 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 653 : 2021 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM E 2554 : 2013-05 PRACTICE FOR ESTIMATING AND MONITORING THE UNCERTAINTY OF TEST RESULTS OF A TEST METHOD USING CONTROL CHART TECHNIQUES
ASTM D 653 : 2014 : REDLINE Standard Terminology Relating to Soil, Rock, and Contained Fluids

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