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BS EN 1071-4:2006

Current

Current

The latest, up-to-date edition.

Advanced technical ceramics. Methods of test for ceramic coatings Determination of chemical composition by electron probe microanalysis (EPMA)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

06-30-2006

Foreword
1 Scope
2 Normative references
3 Terms and definitions
  3.1 General
  3.2 Terms used in electron probe microanalysis
4 Principle
5 Apparatus and materials
  5.1 General
  5.2 Scanning electron microscope
  5.3 Electron probe microanalyser
  5.4 Energy dispersive spectrometer
  5.5 Wavelength dispersive spectrometer
6 Preparation of test piece
  6.1 General
  6.2 Surface roughness
  6.3 Surface conduction
7 Test procedure
  7.1 General
  7.2 Instrument
  7.3 Analysis of thin coatings
  7.4 Analysis of thick coatings
  7.5 Analysis of multilayer coatings
8 Accuracy and interferences
9 Test report
Bibliography

Specifies methods for chemical analysis of ceramic coatings by means of electron probe microanalysis (EPMA) using a scanning electron microscope (SEM) or an electron probe microanalyser.

This European Standard describes methods for chemical analysis of ceramic coatings by means of electron probe microanalysis (EPMA) using a scanning electron microscope (SEM) or an electron probe microanalyser. The methods described are limited to the examination of single layer coatings when the analysis is carried out normal to the sample surface, but graded and multilayer coatings may also be analysed in cross-section if the thickness of the individual layers or gradations are greater than the maximum width of the volume of material within which characteristic or fluorescent X-rays are generated. NOTE This method can also be used for the analysis of bulk materials.

Committee
RPI/13
DevelopmentNote
Supersedes DD ENV 1071-4 and 04/30078581 DC. (06/2006)
DocumentType
Standard
Pages
18
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
NS EN 1071-4 : 1ED 2006 Identical
I.S. EN 1071-4:2006 Identical
EN 1071-4:2006 Identical
NF EN 1071-4 : 2006 Identical
NBN EN 1071-4 : 2006 Identical
SN EN 1071-4 : 2006 Identical
NEN EN 1071-4 : 2006 Identical
UNI EN 1071-4 : 2006 Identical
DIN EN 1071-4:2006-05 Identical

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
EN 623-4:2004 Advanced technical ceramics - Monolithic ceramics - General and textural properties - Part 4: Determination of surface roughness
ISO 14594:2014 Microbeam analysis Electron probe microanalysis Guidelines for the determination of experimental parameters for wavelength dispersive spectroscopy
ISO 15632:2012 Microbeam analysis Selected instrumental performance parameters for the specification and checking of energy-dispersive X-ray spectrometers for use in electron probe microanalysis

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