Animal feeding stuffs. Methods of sampling and analysis. Determination of T-2 and HT-2 toxins, Deoxynivalenol and Zearalenone, in feed materials and compound feed by LCMS

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

12-31-2016

Publisher

British Standards Institution

This method of analysis is applicable to the determination of HT-2 toxin (HT2) in the tested range of 22 µg/kg to 178 µg/kg, T-2 toxin (T2) in the tested range of 7 µg/kg to 50 µg/kg, Deoxynivalenol (DON) in the tested range of 88 µg/kg to 559 µg/kg, and Zearalenone (ZON) in the tested range of 14 µg/kg to 430 µg/kg in cereals and cereal-based compound animal feed. The actual working ranges may extend beyond the tested ranges. It is the responsibility of the laboratory to prove that the limit of quantitation (LOQ) for HT-2 and T-2 toxin is ? 10 µg/kg, for DON ? 100 µg/kg, and for ZON ? 20µg/kg.

Committee	AW/10
DevelopmentNote	Supersedes 15/30321302 DC. (12/2016)
DocumentType	Standard
Pages	36
PublisherName	British Standards Institution
Status	Current
Supersedes	15/30321302 DC : 0

Standards	Relationship
EN 16877:2016	Identical

EN ISO 6498:2012	Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 6498:2012	Animal feeding stuffs — Guidelines for sample preparation
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
ISO 5725-5:1998	Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method