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BS EN ISO 12010:2014

BS EN ISO 12010:2014

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Water quality. Determination of short-chain polychlorinated alkanes (SCCPs) in water. Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)

Available format(s)

Hardcopy , PDF

Superseded date

04-17-2019

Language(s)

English

Published date

06-30-2014

Publisher

British Standards Institution

Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pretreatment
8 Procedure
9 Expression of results
10 Test report
Annex A (informative) - Additional quality control check
        solutions
Annex B (informative) - Explanation of the calibration of the
        sum of SCCPs with multiple linear regression
Annex C (informative) - Typical GC-MS conditions
Annex D (informative) - Typical chromatograms of standard
        solutions 1 [mu]g/ml
Annex E (informative) - Presentation of goodness of fit
Annex F (informative) - Example for recoveries of quality
        assurance solutions
Annex G (informative) - Chromatogram of a real water sample
        with a sum of SCCPs concentration of 2,59 [mu]g/l
Annex H (informative) - Precision data
Bibliography

Describes a method for the quantitative determination of the sum of short-chain polychlorinated n-alkanes, also known as short-chain polychlorinated paraffins (SCCPs), in the carbon bond range n-C[10] to n-C[13] inclusive, in mixtures with chlorine mass fractions ('contents') between 49% and 67%, including approximately 6300 of approximately 8000 congeners.

ISO 12010:2012 specifies a method for the quantitative determination of the sum of short-chain polychlorinated n?alkanes, also known as short-chain polychlorinated paraffins (SCCPs), in the carbon bond range n-C10 to n-C13 inclusive, in mixtures with chlorine mass fractions (\'contents\') between 49 % and 67 %, including approximately 6 300 of approximately 8 000 congeners. This method is applicable to the determination of the sum of SCCPs in unfiltered surface water, ground water, drinking water and waste water using gas chromatography-mass spectrometry with electron capture negative ionization (GC-ECNI-MS). The method can be applied to samples containing 0,1 µg/l to 10 µg/l. Depending on the waste water matrix, the lowest detectable concentration is estimated to be >0,1 µg/l.

Committee
EH/3/2
DevelopmentNote
Renumbers and supersedes BS ISO 12010. 2014 Version incorporates corrigendum to BS ISO 12010. Supersedes 10/30156236 DC. (06/2014)
DocumentType
Standard
Pages
38
PublisherName
British Standards Institution
Status
Superseded
SupersededBy
Supersedes

Standards Relationship
ISO 12010:2012 Identical
EN ISO 12010:2014 Identical

ISO/TS 13530:2009 Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006 Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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Hardcopy - English
PDF - English
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