BS ISO 17974:2002
Current
The latest, up-to-date edition.
Surface chemical analysis. High-resolution Auger electron spectrometers. Calibration of energy scales for elemental and chemical-state analysis
Hardcopy , PDF
English
11-29-2002
Foreword
Introduction
1 Scope
2 Normative reference
3 Terms and definitions
4 Symbols and abbreviated terms
5 Outline of method
6 Procedure for calibrating the energy scale
6.1 Obtaining reference samples
6.2 Mounting samples
6.3 Cleaning samples
6.4 Choosing spectrometer settings for energy calibration
6.5 Operating the instrument
6.6 Options for initial or subsequent
calibration measurements
6.7 Measurements for peak kinetic energy
repeatability standard deviation and scale linearity
6.8 Calculating peak kinetic energy repeatability
standard deviation
6.9 Determining relevant reference kinetic energies
6.10 Checking kinetic energy scale linearity
6.11 Procedure for regular calibration error
determination
6.12 Procedures for correction of the instrument
kinetic energy scale
6.13 Next calibration
6.14 Establishing calibration intervals
Annex A (normative) Maximum number of points for a
single application of Savitzky and Golaya smoothing
of peaks at 0,1 eV energy intervals
Annex B (normative) Least squares determination of peak
kinetic energy by a simple computational method
Annex C (informative) Derivation of uncertainties
Annex D (informative) Citation of uncertainties of
measured kinetic energy
smoothing of peaks at 0,1 eV energy intervals
Bibliography
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