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PD CEN/TS 1948-5:2015

Current
Current

The latest, up-to-date edition.

Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Long-term sampling of PCDDs/PCDFs and PCBs
Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

04-30-2015

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle of long-term PCDD/PCDF/PCB sampling
6 Sampling device and materials
7 Minimum requirements for long-term PCDD/PCDF/PCB
   sampling methods
8 Quality assurance
9 Analytical procedure
10 Estimation of uncertainty of the method
11 Reporting
Annex A (normative) - Overview of minimum requirements
Annex B (informative) - Cleaning of the probe
Annex C (normative) - Performance criteria and test procedure
        for certification
Annex D (informative) - Examples of devices and operation for
        long-term sampling systems
Annex E (informative) - Fundamentals of isokinetic sampling
Annex F (informative) - Example for the determination of the
        representative sampling point
Annex G (informative) - Estimation of the uncertainty of
        measured PCDD/PCDF of the long-term sampling
        system
Annex H (informative) - Example for calculation of measurement
        results for standard conditions
Annex I (normative) - Adaption of the maximum deviation in
        relation to the PCDD/PCDF/PCB concentration
Bibliography

Describes the long-term sampling of PCDDs, PCDFs and PCBs.

This Technical Specification specifies the long-term sampling of PCDDs, PCDFs and PCBs. There are three different sampling methods, which use the three different principles described in EN1948‑1 modified for long-term sampling requirements: filter/condenser method; dilution method; cooled probe method. Each sampling method is illustrated in detail in AnnexD. The sampling methods described in this document are designed for a sampling duration of typically four weeks. Additionally this document specifies a framework of quality control requirements for any long-term sampling method to be applied (see AnnexC and AnnexF). With the methods described experiences were gained for a concentration range from typically 0,003ng I-TEQ/m 3 up to 4,0ng I-TEQ/m 3 and 0,003ng WHO-TEQ/m 3 up to 4,0ng WHO-TEQ/m 3 respectively at different stationary sources (e.g. waste incinerators, sinter plants, cement kilns). For the complete measurement method the use of EN1948‑2 and EN1948‑3 describing extraction and cleanup and identification and quantification, respectively, is necessary in order to determine PCDDs/PCDFs. Also EN1948‑4 is necessary for the analyses of dioxin-like PCBs.

Committee
EH/2/1
DocumentType
Standard
Pages
84
PublisherName
British Standards Institution
Status
Current

Standards Relationship
CEN/TS 1948-5:2015 Identical

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
EN 15267-3:2007 Air quality - Certification of automated measuring systems - Part 3: Performance criteria and test procedures for automated measuring systems for monitoring emissions from stationary sources
EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
ISO 14956:2002 Air quality Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty
EN ISO 16911-1:2013 Stationary source emissions - Manual and automatic determination of velocity and volume flow rate in ducts - Part 1: Manual reference method (ISO 16911-1:2013)
EN 15267-2:2009 Air quality - Certification of automated measuring systems - Part 2: Initial assessment of the AMS manufacturer’s quality management system and post certification surveillance for the manufacturing process
EN 15259:2007 Air quality - Measurement of stationary source emissions - Requirements for measurement sections and sites and for the measurement objective, plan and report
ISO/IEC Guide 99:2007 International vocabulary of metrology Basic and general concepts and associated terms (VIM)
EN 13284-1:2017 Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method
ISO 16911-1:2013 Stationary source emissions — Manual and automatic determination of velocity and volume flow rate in ducts — Part 1: Manual reference method
EN 14181:2014 Stationary source emissions - Quality assurance of automated measuring systems
EN 1948-1:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
EN ISO 14956 : 2002 AIR QUALITY - EVALUATION OF THE SUITABILITY OF A MEASUREMENT PROCEDURE BY COMPARISON WITH A REQUIRED MEASUREMENT UNCERTAINTY
ENV 13005 : DRAFT 1999 GUIDE TO THE EXPRESSION OF UNCERTAINTY IN MEASUREMENT
EN 1948-4:2010+A1:2013 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
EN 15267-1:2009 Air quality - Certification of automated measuring systems - Part 1: General principles

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