WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2015

Publisher

German Institute for Standardisation (Deutsches Institut für Normung)

National foreword
National Annex NA (informative) - Bibliography
European foreword
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Measurement of samples
11 Identification of individual compounds by
   means of GC-MS (SIM)
12 Calculation
13 Expression of results
14 Test report
Annex A (informative) - Suitable gas chromatographic
        conditions and example chromatograms -
        GC-conditions
Annex B (informative) - Repeatability and reproducibility
        data
Annex C (informative) - Dilution Schedules for standards
Annex D (informative) - Silica clean-up
Annex E (informative) - Examples of suitable solid-phase
        extraction disks (SPE-disks)
Bibliography

Defines a method for the determination of 7 polycyclic aromatic hydrocarbons (PAH) in whole water samples listed in Table 1.

DocumentType	Standard
Pages	35
PublisherName	German Institute for Standardisation (Deutsches Institut für Normung)
Status	Current

Standards	Relationship
EN 16691:2015	Identical

ISO 7981-1:2005	Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 1: Determination of six PAH by high-performance thin-layer chromatography with fluorescence detection after liquid-liquid extraction
EN ISO 17993 : 2003	WATER QUALITY - DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WATER BY HPLC WITH FLUORESCENCE DETECTION AFTER LIQUID-LIQUID EXTRACTION
NEN 7777 : 2011 + C1 2012	ENVIRONMENT AND FOOD - PERFORMANCE CHARACTERISTICS OF MEASUREMENT METHODS
DIN ISO 5725-2:2002-12	Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
ISO 1042:1998	Laboratory glassware One-mark volumetric flasks
ISO/TS 13530:2009	Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 7981-2:2005	Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 2: Determination of six PAH by high-performance liquid chromatography with fluorescence detection after liquid-liquid extraction
ISO 17993:2002	Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
DIN ISO 28540:2014-05	Water quality - Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water - Method using gas chromatography with mass spectrometric detection (GC-MS) (ISO 28540:2011)
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
EN ISO 1042 : 1999	LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 28540:2011	Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
ISO 6107-2:2006	Water quality Vocabulary Part 2:
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
EN 15527:2008	Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
ISO/TS 28581:2012	Water quality — Determination of selected non-polar substances — Method using gas chromatography with mass spectrometric detection (GC-MS)
EN ISO 5667-1 : 2006 COR 2007	WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES

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DIN EN 16691 E : 2015

Current

Table of Contents

Abstract

General Product Information

International Equivalents

Standards Referencing This Book

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