EN 14112:2016
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
Superseded date
12-07-2020
Published date
09-07-2016
Publisher
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Preparation of measurement
9 Measurement
10 Calculation and Evaluation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Background of the method
Annex B (informative) - Results of an Interlaboratory
Study
Bibliography
This European Standard specifies a method for the determination of the oxidation stability of fatty acid methyl esters (FAME) at 110 °C, by means of measuring the induction period up to 48 h.NOTE 1EN 15751 [1] describes a similar test method for oxidation stability determination of pure fatty acid methyl esters and of blends of FAME with petroleum-based diesel containing 2 % (V/V) of FAME at minimum.NOTE 2The precision statement of this test method was determined in a Round Robin exercise with induction periods up to 8,5 h, thus covering the limit value in EN 14214. Results from precision studies on EN 15751 indicate that the precision statement is valid for induction periods up to 48 h but not for higher values.NOTE 3Limited studies on EN 15751 with EHN (2-ethyl hexyl nitrate) on FAME blends indicated that the stability is reduced to an extent which is within the reproducibility of the test method. It is likely that the oxidation stability of pure FAMEs is also reduced in the presence of EHN when EN 14112 is used for testing.
| Committee |
CEN/TC 307
|
| DevelopmentNote |
Supersedes PREN 14112. (09/2016)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
| Standards | Relationship |
| I.S. EN 14112:2016 | Identical |
| SS-EN 14112 : 2016 | Identical |
| NS EN 14112 : 2003 | Identical |
| SANS 54112 : 1ED 2007(R2014) | Identical |
| NF EN 14112 : 2016 | Identical |
| NEN EN 14112 : 2016 | Identical |
| DIN EN 14112:2016-12 | Identical |
| DIN EN 14112:2014-07 (Draft) | Identical |
| NBN EN 14112 : 2016 | Identical |
| GOST R EN 14112 : 2010 | Identical |
| BS EN 14112:2003 | Identical |
| UNI EN 14112 : 2016 | Identical |
| UNE-EN 14112:2017 | Identical |
| SN EN 14112 : 2016 | Identical |
| PN EN 14112 : 2016 | Identical |
| UNI EN 14112 : 2003 | Identical |
| ONORM EN 14112 : 2016 | Identical |
| DIN EN 14112:2003-10 | Identical |
| SANS 54112:2020 | Identical |
| S.R. CEN/TR 16389:2017 | AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL AND BLENDS WITH FAME - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION |
| PD CEN/TR 16389:2017 | Automotive fuels. Paraffinic diesel fuel and blends with FAME. Background to the parameters required and their respective limits and determination |
| 09/30205523 DC : 0 | BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
| 13/30277078 DC : 0 | BS EN 16568 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C |
| BS 2000-574(2014) : 2014 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| I.S. EN 14213:2003 | HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS |
| DIN EN 15751 E : 2014 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| CEN/TR 16366:2012 | Liquid petroleum products - Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Round Robin report on applicability of Rapid Small Scale Oxidation Test method |
| DIN EN 16568 E : 2015 | AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C |
| S.R. CWA 16379:2011 | FUELS AND BIOFUELS - PURE PLANT OIL FUEL FOR DIESEL ENGINE CONCEPTS - REQUIREMENTS AND TEST METHODS |
| BS EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| DIN EN 14214:2014-06 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| UNI EN 15751 : 2014 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| BS EN 15751:2014 | Automotive fuels. Fatty acid methyl ester (FAME) fuel and blends with diesel fuel. Determination of oxidation stability by accelerated oxidation method |
| DIN EN 14214 E : 2003 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| DIN EN 15751:2014-06 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| I.S. EN 14214:2012 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| UNI EN 14214 : 2014 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| EN 14214:2012+A1:2014/AC:2014 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| UNE-EN 15751:2014 | Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method |
| BS 2000-620(2014) : 2014 | AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C |
| PREN 14214 : DRAFT 2009 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
| BS EN 16568:2014 | Automotive fuels. Blends of Fatty acid methyl ester (FAME) with diesel fuel. Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C |
| XP M15 032 : 2010 XP | AUTOMOTIVE FUELS - FATTY ACID METHYL AND ETHYL ESTERS (FAME AND FAEE) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS |
| DIN EN 16568:2015-03 | AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C |
| 18/30369065 DC : DRAFT FEB 2018 | BS EN 14214 AMD 2 - LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| 17/30365049 DC : 0 | BS EN 17181 - LUBRICANTS - DETERMINATION OF AEROBIC BIOLOGICAL DEGRADATION OF FULLY FORMULATED LUBRICANTS IN AN AQUEOUS SOLUTION - TEST METHOD BASED ON CO[2]-PRODUCTION |
| BS EN 14213:2003 | Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods |
| EN 14213:2003/AC:2003 | HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS |
| EN 15751:2014 | Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method |
| EN 16568:2014 | Automotive fuels - Blends of Fatty acid methyl ester (FAME) with diesel fuel - Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C |
| I.S. EN 16568:2014 | AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C |
| 08/30172824 DC : DRAFT JAN 2008 | BS EN 15751 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| PD CEN/TR 16366:2012 | Liquid petroleum products. Middle distillates and fatty acid methyl ester (FAME) fuels and blends. Round Robin report on applicability of Rapid Small Scale Oxidation Test method |
| 12/30268200 DC : 0 | BS EN 15751 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| S.R. CEN/TR 16366:2012 | LIQUID PETROLEUM PRODUCTS - MIDDLE DISTILLATES AND FATTY ACID METHYL ESTER (FAME) FUELS AND BLENDS - ROUND ROBIN REPORT ON APPLICABILITY OF RAPID SMALL SCALE OXIDATION TEST METHOD |
| BS 2000-574(2009) : 2009 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| UNE-EN 14214:2013 | Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods |
| ASTM D 7467 : 2017-03 | SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20) |
| I.S. EN 15751:2014 | AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY ACCELERATED OXIDATION METHOD |
| DIN EN 14213 E : 2003 | HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS |
| DIN EN 14214:2003-11 | LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS |
| DIN EN 14213:2003-11 | HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS |
| CEN/TR 16389:2017 | Automotive fuels - Paraffinic diesel fuel and blends with FAME - Background to the parameters required and their respective limits and determination |
| ISO 3171:1988 | Petroleum liquids — Automatic pipeline sampling |
| ISO 3170:2004 | Petroleum liquids — Manual sampling |
| ISO 6886:2016 | Animal and vegetable fats and oils Determination of oxidative stability (accelerated oxidation test) |
| EN ISO 6886:2016 | ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF OXIDATIVE STABILITY (ACCELERATED OXIDATION TEST) (ISO 6886:2016) |
| ISO 4259:2006 | Petroleum products Determination and application of precision data in relation to methods of test |
| EN 15751:2014 | Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
| EN ISO 3170:2004 | Petroleum liquids - Manual sampling (ISO 3170:2004) |
| EN ISO 3171:1999 | Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) |
| EN ISO 4259:2006 | Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) |
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