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CEN
EN 14538:2006

EN 14538:2006

Current

Current

The latest, up-to-date edition.

Fat and oil derivatives - Fatty acid methyl ester (FAME) - Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

Published date

06-07-2006

Publisher

Comite Europeen de Normalisation

Foreword
1 Scope
2 Normative references
3 Principle
4 Chemicals
5 Apparatus
6 Sampling
7 Preparation of the calibration solutions and the
   blank solution
   7.1 General
   7.2 Blank solution
   7.3 Calibration solution with a nominal element
       content of 0,5 mg/kg
   7.4 Calibration solution with a nominal element
       content of 1 mg/kg
   7.5 Calibration solution with a nominal element
       content of 5 mg/kg
   7.6 Calibration solution with a nominal element
       content of 10 mg/kg
8 Calibration
   8.1 General
   8.2 Calibration
   8.3 Check of calibration
9 Sample analysis
   9.1 Sample preparation
   9.2 Measurement
10 Calculation
11 Results
12 Precision
   12.1 Repeatability
   12.2 Reproducibility
13 Test report

This document specifies a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.

Committee
CEN/TC 19
DevelopmentNote
Supersedes PREN 14538. (12/2007)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

Standards Relationship
NS EN 14538 : 1ED 2006 Identical
SS-EN 14538:2006 Identical
DIN EN 14538 E : 2006 Identical
BS 2000-547(2006) : 2006 Identical
NF EN 14538 : 2007 Identical
SN EN 14538 : 2006 Identical
NBN EN 14538 : 2006 Identical
UNI EN 14538 : 2006 Identical
GOST R EN 14538 : 2009 Identical
PN EN 14538 : 2008 Identical
UNE-EN 14538:2006 Identical
BS EN 14538:2006 Identical
IP 547 : 2007 Identical
NEN EN 14538 : 2006 Identical
I.S. EN 14538:2006 Identical
DIN EN 14538:2006-09 Identical

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
15/30303049 DC : 0 BS ISO 21033 - ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
BS ISO 21033:2016 Animal and vegetable fats and oils. Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES)
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
CEN/TR 17144:2017 Resistance of metallic materials to liquid biogenic and alternative fuels and their blends
BS PD ISO/TS 21033 : 2011 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
S.R. CEN/TR 17144:2017 RESISTANCE OF METALLIC MATERIALS TO LIQUID BIOGENIC AND ALTERNATIVE FUELS AND THEIR BLENDS
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DD ISO/TS 21033 : 2011 ANIMAL AND VEGETABLE FATS AND OILS - DETERMINATION OF TRACE ELEMENTS BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROSCOPY (ICP-OES)
ISO 21033:2016 Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES)
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
ISO/TS 21033:2011 Animal and vegetable fats and oils Determination of trace elements by inductively coupled plasma optical emission spectroscopy (ICP-OES)
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
PD CEN/TR 17144:2017 Resistance of metallic materials to liquid biogenic and alternative fuels and their blends
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)

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