EN 14582:2016
Current
Current
The latest, up-to-date edition.
Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods
Published date
08-03-2016
Publisher
European Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Hazards
7 Reagents and control mixtures
8 Sample conservation and pretreatment of test portion
9 Equipment
10 Procedure
11 Recommended methods of determination
12 Control measurements
13 Evaluation
14 Test report
Annex A (informative) - Performance characteristics
Annex B (informative) - Oxygen flask combustion by
Schoeniger
Annex C (informative) - Recovery yields obtained for
control mixtures with different absorption
solutions and analytical techniques
Annex D (informative) - Examples of possible control
substances
Annex E (informative) - Additional results of
inter-laboratory tests
Annex F (informative) - Summary of general
requirements and recommendations
Annex G (informative) - Additional validation data
Bibliography
This standard specifies a combustion method for the determination of halogen and sulfur contents in materials by combustion in a closed system containing oxygen (calorimetric bomb), and the subsequent analysis of the combustion product using different analytical techniques.This method is applicable to solid, pasty and liquid samples containing more than 0,025 g/kg of halogen and/or 0,025 g/kg of sulfur content. The limit of detection depends on the element, the matrix and the determination technique used.Insoluble halides and sulphate present in the sample or produced during the combustion step are not completely determined by these methods.
| Committee |
CEN/TC 444
|
| DevelopmentNote |
Supersedes PREN 14582. (08/2016)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| NBN EN 14582 : 2007 | Identical |
| SS-EN 14582:2016 | Identical |
| UNE-EN 14582:2016 | Identical |
| DIN EN 14582 E : 2016 | Identical |
| NS EN 14582 : 2007 | Identical |
| NF EN 14582 : 2016 | Identical |
| BS EN 14582:2007 | Identical |
| NEN EN 14582 : 2016 | Identical |
| PN EN 14582 : 2017 | Identical |
| I.S. EN 14582:2016 | Identical |
| DIN EN 14582:2015-04 (Draft) | Identical |
| SN EN 14582:2016 | Identical |
| UNI EN 14582 : 2007 | Identical |
| UNI EN 14582:2016 | Identical |
| DIN EN 14582:2016-12 | Identical |
| BS EN 14582:2016 | Identical |
| PD CEN/TR 16376:2012 | Characterization of waste. Overall guidance document for characterization of waste from the extractive industries |
| PD CLC/TS 50625-3-1:2015 | Collection, logistics & treatment requirements for WEEE Specification for de-pollution. General |
| IEC PAS 63015:2016 | Definition of "Low-Halogen" for electronic products |
| CEN/TR 16376:2012 | Characterization of waste - Overall guidance document for characterization of waste from the extractive industries |
| EN 15875:2011/AC:2012 | CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE |
| IPC J STD 004 RUSSIAN : B | REQUIREMENTS FOR SOLDERING FLUXES |
| IPC J STD 004 CHINESE : B | REQUIREMENTS FOR SOLDERING FLUXES |
| 10/30229134 DC : 0 | BS EN 62321-3-2 ED 1 - DETERMINATION OF CERTAIN SUBSTANCES IN ELECTROTECHNICAL PRODUCTS - PART 3-2: SCREENING OF TOTAL BROMINE IN ELECTRIC AND ELECTRONIC PRODUCTS BY COMBUSTION - ION CHROMATOGRAPHY (C-IC) |
| UNI EN 16457 : 2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| I.S. EN 50642:2018 | CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS |
| I.S. EN 16457:2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| EN 50642:2018 | Cable management systems - Test method for content of halogens |
| S.R. CEN/TR 16376:2012 | CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES |
| UNE-EN 15289:2011 | Solid biofuels - Determination of total content of sulfur and chlorine |
| 17/30348303 DC : 0 | BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT |
| UNE-EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| I.S. EN 15002:2015 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| BS EN 15289:2011 | Solid biofuels. Determination of total content of sulfur and chlorine |
| BS EN 62321-3-2:2014 | Determination of certain substances in electrotechnical products Screening. Total bromine in polymers and electronics by Combustion. Ion Chromatography |
| BS EN 15875:2011 | Characterisation of waste. Static test for determination of acid potential and neutralisation potential of sulfidic waste |
| PREN 50642 : DRAFT 2016 | CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS |
| I.S. EN ISO 16994:2016 | SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE (ISO 16994:2016) |
| UNE-EN 16457:2014 | Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report |
| UNI EN 15289 : 2011 | SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE |
| DIN EN 15875 E : 2012 | CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE |
| I.S. EN 15875:2011 | CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE |
| DIN EN 15875:2012-11 | Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste (includes Corrigendum :2012) |
| 13/30277477 DC : 0 | BS EN ISO 16994 - SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULPHUR AND CHLORINE |
| S.R. CLC/TS 50625-3-1:2015 | COLLECTION, LOGISTICS & TREATMENT REQUIREMENTS FOR WEEE - PART 3-1: SPECIFICATION FOR DE-POLLUTION - GENERAL |
| DIN EN 15289:2011-04 | SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE |
| 12/30263896 DC : 0 | BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| UNI EN 15875 : 2011 | CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE |
| DIN EN 16457:2014-07 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| I.S. EN 62321-3-2:2014 | DETERMINATION OF CERTAIN SUBSTANCES IN ELECTROTECHNICAL PRODUCTS - PART 3-2: SCREENING - TOTAL BROMINE IN POLYMERS AND ELECTRONICS BY COMBUSTION - ION CHROMATOGRAPHY |
| 13/30291099 DC : 0 | BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| 17/30350920 DC : 0 | BS EN 63031 - DEFINITION OF LOW HALOGEN MATERIALS USED IN ELECTRONIC AND ELECTRICAL PRODUCTS |
| ISO 16994:2016 | Solid biofuels — Determination of total content of sulfur and chlorine |
| PD IEC/PAS 63015:2016 | Definition of “Low-Halogen?? for electronic products |
| DIN EN 15002:2015-07 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| IPC J STD 004 : B | REQUIREMENTS FOR SOLDERING FLUXES |
| EN 16457:2014 | Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report |
| EN ISO 16994:2016 | Solid biofuels - Determination of total content of sulfur and chlorine (ISO 16994:2016) |
| CLC/TS 50625-3-1:2015 | Collection, logistics & treatment requirements for WEEE - Part 3-1: Specification for de-pollution - General |
| BS EN ISO 16994:2015 | Solid biofuels. Determination of total content of sulfur and chlorine |
| DIN EN 16457 E : 2014 | CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT |
| 10/30219387 DC : 0 | BS EN 15289 - SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULPHUR AND CHLORINE |
| NF EN 15875 : 2011 | CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL AND NEUTRALISATION POTENTIAL OF SULFIDIC WASTE |
| BS EN 16457:2014 | Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report |
| UNE-EN 15875:2012 | Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste |
| 08/30189276 DC : 0 | BS EN 15875 - CHARACTERIZATION OF WASTE - STATIC TEST FOR DETERMINATION OF ACID POTENTIAL OF SULFIDIC WASTE |
| 16/30331003 DC : 0 | BS EN 50642 - CABLE MANAGEMENT SYSTEMS - TEST METHOD FOR CONTENT OF HALOGENS |
| I.S. EN 15289:2011 | SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE |
| CSA ISO 16994 : 2015 | SOLID BIOFUELS - DETERMINATION OF TOTAL CONTENT OF SULFUR AND CHLORINE |
| DIN EN 15002 E : 2015 | CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE |
| BS EN 15002:2015 | Characterization of waste. Preparation of test portions from the laboratory sample |
| EN 62321-3-2:2014 | Determination of certain substances in electrotechnical products - Part 3-2: Screening - Total bromine in polymers and electronics by Combustion - Ion Chromatography |
| EN 15289:2011 | Solid biofuels - Determination of total content of sulfur and chlorine |
| EN ISO 11885:2009 | Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007) |
| EN ISO 10304-3 : 1997 | Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate (ISO 10304-3:1997) |
| ASTM D 808 : 2016 : REDLINE | Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) |
| ISO 10304-3:1997 | Water quality — Determination of dissolved anions by liquid chromatography of ions — Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate |
| EN 14346:2006 | CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE OR WATER CONTENT |
| ISO 9297:1989 | Water quality Determination of chloride Silver nitrate titration with chromate indicator (Mohr's method) |
| ISO 11885:2007 | Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) |
| ISO 10304-1:2007 | Water quality Determination of dissolved anions by liquid chromatography of ions Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate |
| ISO 10304-2:1995 | Water quality Determination of dissolved anions by liquid chromatography of ions Part 2: Determination of bromide, chloride, nitrate, nitrite, orthophosphate and sulfate in waste water |
| ISO 10359-1:1992 | Water quality — Determination of fluoride — Part 1: Electrochemical probe method for potable and lightly polluted water |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| ASTM E 442 : 1991 | Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997) |
| EN ISO 10304-1:2009 | Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007) |
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