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EN 16174:2012

Withdrawn
Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
Withdrawn date

02-28-2013

Published date

08-22-2012

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences and sources of errors
6 Reagents
7 Apparatus
8 Procedure
9 Test report
Annex A (informative) - Repeatability and
        reproducibility data
Bibliography

This European Standard specifies two methods for digestion of sludge, treated biowaste and soil by the use of aqua regia as digestion solution.This European Standard is applicable for the following elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).This European Standard may also be applicable for the digestion of other elements.Digestion with aqua regia will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.

Committee
CEN/TC 444
DevelopmentNote
Supersedes PREN 16174. (09/2012)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn

Standards Relationship
SN EN 16174 : 2012 Identical
PN EN 16174 : 2012 Identical
BS EN 16174:2012 Identical
NF EN 16174 : 2012 Identical
UNE-EN 16174:2012 Identical
NEN EN 16174 : 2012 Identical
UNI EN 16174 : 2012 Identical
I.S. EN 16174:2012 Identical
DIN EN 16174:2012-11 Identical
NS EN 16174 : 2012 Identical
NBN EN 16174 : 2012 Identical

S.R. CEN/TS 16171:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
S.R. CEN/TS 16170:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
PD ISO/TS 16965:2013 Soil quality. Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/CENELEC GUIDE 33 : 2016 GUIDE FOR ADDRESSING ENVIRONMENTAL ISSUES IN TESTING STANDARDS
ISO/TS 16965:2013 Soil quality Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/TS 16171:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/TS 16172:2013 Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)
EN 16175-2:2016 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
CEN/TS 16175-1:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS)
UNI CEN/TS 16170 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
BS EN 16175-2:2016 Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS)
UNI CEN/TS 16172 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
16/30330779 DC : 0 BS EN 16964 - FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS AND REMOVAL OF ORGANIC COMPOUNDS FROM FERTILIZER EXTRACTS
UNI CEN/TS 16188 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS IN AQUA REGIA AND NITRIC ACID DIGESTS - FLAME ATOMIC ABSORPTION SPECTROMETRY METHOD (FAAS)
I.S. EN 16175-1:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
UNI CEN/TS 16171 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
S.R. CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
S.R. CEN/TS 16175-2:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
I.S. EN 16171:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
I.S. EN 16170:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
I.S. EN 16175-2:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
S.R. CEN/TS 16175-1:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
CEN/TS 16175-2:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
CEN/TS 16170:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
ISO 11074:2015 Soil quality — Vocabulary
EN 1483:2007 Water quality - Determination of mercury - Method using atomic absorption spectrometry
EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
ISO 11969:1996 Water quality Determination of arsenic Atomic absorption spectrometric method (hydride technique)
EN ISO 5961 : 1995 WATER QUALITY - DETERMINATION OF CADMIUM BY ATOMIC ABSORPTION SPECTROMETRY (ISO 5961:1994)
ISO 5961:1994 Water quality Determination of cadmium by atomic absorption spectrometry
EN 15936:2012 Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion
ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
ISO 8288:1986 Water quality — Determination of cobalt, nickel, copper, zinc, cadmium and lead — Flame atomic absorption spectrometric methods
ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
EN 1233 : 1996 WATER QUALITY - DETERMINATION OF CHROMIUM - ATOMIC ABSORPTION SPECTROMETRIC METHODS
EN 13346 : 2000 CHARACTERIZATION OF SLUDGES - DETERMINATION OF TRACE ELEMENTS AND PHOSPHORUS - AQUA REGIA EXTRACTION METHODS
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 13650:2001 Soil improvers and growing media - Extraction of aqua regia soluble elements
EN 13657:2002 Characterization of waste - Digestion for subsequent determination of aqua regia soluble portion of elements
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
EN ISO 11969:1996 WATER QUALITY - DETERMINATION OF ARSENIC - ATOMIC ABSORPTION SPECTROMETRIC METHOD (HYDRIDE TECHNIQUE)
EN 45001 : 1989 GENERAL CRITERIA FOR THE OPERATION OF TESTING LABORATORIES

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