Name: EN 16453:2014
Brand: CEN

Pulp, paper and paperboard - Determination of phthalates in extracts from paper and paperboard

Published date

01-29-2014

Publisher

Comite Europeen de Normalisation

Foreword
1 Scope
2 Normative references
3 Principle
4 Materials
5 Apparatus
6 Reagents
7 Sampling
8 Preparation of the test sample of water
   extract
9 Preparation of the test sample of the
   organic solvent extract
10 Preparation of the test sample of the
   MPPO Extract
11 Procedure
12 Expression of results
13 Test report
14 Precision data
Annex A (informative) - GC-MS total ion chromatogram
        of a standard calibration solution of
        2 mg/l of phthalates

This European Standard specifies a method for the determination of phthalates in water, solvent and modified polyphenylene oxide (MPPO) extracts of paper and board materials and articles intended for food contact using gas chromatography coupled to mass spectrometry (GC-MS).This method is applicable to the determination of phthalates in concentration ranging from 0,002 mg/L to 5 mg/L for water and solvent extracts and 0,0005 mg/dm² to 0,25 mg/dm² for MPPO migration depending on the individual substance and the value of the blank.

Committee	CEN/TC 172
DevelopmentNote	Supersedes PREN 16453. (02/2014)
DocumentType	Standard
PublisherName	Comite Europeen de Normalisation
Status	Current

Standards	Relationship
UNE-EN 16453:2014	Identical
NS EN 16453 : 2014	Identical
DIN EN 16453:2014-06	Identical
PN EN 16453 : 2014	Identical
NBN EN 16453 : 2014	Identical
I.S. EN 16453:2014	Identical
BS EN 16453:2014	Identical
DIN EN 16453 E : 2014	Identical
UNI EN 16453 : 2014	Identical
SS-EN 16453:2014	Identical
NEN EN 16453 : 2014	Identical
NF EN 16453 : 2014	Identical
SN EN 16453:2018	Identical

EN 645:1993	Paper and board intended to come into contact with foodstuffs - Preparation of a cold water extract
ISO 638:2008	Paper, board and pulps Determination of dry matter content Oven-drying method
ISO 18856:2004	Water quality — Determination of selected phthalates using gas chromatography/mass spectrometry
EN ISO 18856:2005	Water quality - Determination of selected phthalates using gas chromatography/mass spectrometry (ISO 18856:2004)
EN ISO 536:2012	Paper and board - Determination of grammage (ISO 536:2012)
ISO 186:2002	Paper and board — Sampling to determine average quality
ISO 536:2012	Paper and board Determination of grammage
EN 27213 : 1993	PULPS - SAMPLING FOR TESTING
EN ISO 186 : 2002	Paper and board - Sampling to determine average quality (ISO 186:2002)
EN 647:1993	Paper and board intended to come into contact with foodstuffs - Preparation of a hot water extract
EN 15519:2007	Paper and board intended to come into contact with foodstuffs - Preparation of an organic solvent extract
ISO 7213:1981	Pulps Sampling for testing
EN ISO 638:2008	Paper, board and pulps - Determination of dry matter content - Oven-drying method (ISO 638:2008)
EN 14338:2003	Paper and board intended to come into contact with foodstuffs - Conditions for determination of migration from paper and board using modified polyphenylene oxide (MPPO) as a simulant