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EN 1948-4:2010+A1:2013

Current
Current

The latest, up-to-date edition.

STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
Published date

12-04-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle of the measurement procedure
6 Device, materials and [13]C[12]-labelled
   standards
7 Safety measures
8 Measurement procedure
9 Method validation
10 Quality control requirements for the
   measurement
11 Quality assurance criteria for
   extraction/clean-up/quantification procedure
   blanks
12 Performance characteristics
13 Interferences (informative)
Annex A (informative) - Toxicity and toxic equivalency
Annex B (informative) - Examples of extraction and
        clean-up procedures
Annex C (informative) - Evaluation of the performance
        characteristics
Annex D (informative) - Recommendations for measuring
        high concentrations of dioxin-like PCBs
Annex E (informative) - Possible interferences in
        dioxin-like PCB analysis
Annex F (informative) - Measurement of the marker
        PCBs 28, 52, 101, 138, 153, and 180 in addition
        to the 12 dioxin-like PCBs
Annex G (informative) - Measurement of hexachlorobenzene
        (HCB)
Annex H (informative) - Significant technical changes
Annex ZA (informative) - Relationship between this
         European Standard and the essential requirements
         of EU Directives
Bibliography

This European Standard specifies sampling from stationary sources, extraction, clean-up, identification and quantification procedures of the dioxin-like PCBs. The procedure described lays down requirements to measure the PCB congeners given in Annex A (see Table A.1).

Committee
TC 264
DevelopmentNote
Supersedes CEN/TS 1948-4. (10/2010) Supersedes PREN 1948-4. (04/2011) 2010 Edition Re-Issued in December 2013 & incorporates AMD 1 2013. (01/2014)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

PD CEN/TS 1948-5:2015 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Long-term sampling of PCDDs/PCDFs and PCBs
CEN/TS 1948-5:2015 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 5: Long-term sampling of PCDDs/PCDFs and PCBs
VDI 3890:2016-03 Emission control - Pet cremation facilities
VDI 3476 Blatt 1:2015-06 Waste gas cleaning - Methods of catalytic waste gas cleaning - Fundamentals
VDI 2578:2017-05 Emission control - Glassworks
VDI 2102 Blatt 2:2013-04 Emission control - Copper and copper alloy melting plants
07/30146333 DC : 0 BS ISO 16000-14 - INDOOR AIR - PART 14: DETERMINATION OF TOTAL (GAS AND PARTICLE-PHASE) POLYCHLORINATED DIOXIN-LIKE BIPHENYLS (PCBS) AND POLYCHLORINATED DIBENZO-P-DIOXINS/DIBENZOFURANS (PCDDS/PCDFS) - EXTRACTION, CLEAN-UP AND ANALYSIS BY HIGH-RESOLUTION GAS CHROMATOGRAPHY/MASS SPECTROMETRY
S.R. CEN/TS 1948-5:2015 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 5: LONG-TERM SAMPLING OF PCDDS/PCDFS AND PCBS

ISO 4793:1980 Laboratory sintered (fritted) filters — Porosity grading, classification and designation
EN 12766-1:2000 Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD)
VDI 2310 Blatt 32:1995-11 Maximum immission values - Maximum immission values for PCBs to protect farm animals
EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
EN ISO 9169:2006 Air quality - Definition and determination of performance characteristics of an automatic measuring system (ISO 9169:2006)
EN ISO 16000-12:2008 Indoor air - Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) (ISO 16000-12:2008)
EN 13284-1:2017 Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method
EN 1948-1:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 16000-12:2008 Indoor air Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs)
ISO 9169:2006 Air quality Definition and determination of performance characteristics of an automatic measuring system

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