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EN ISO 13032:2012

Current

Current

The latest, up-to-date edition.

Petroleum products - Determination of low concentration of sulfur in automotive fuels - Energy-dispersive X-ray fluorescence spectrometric method (ISO 13032:2012)

Published date

03-01-2012

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling and sample handling
7 Apparatus preparation
8 Calibration
9 Procedure
10 Calculation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Matrix effects
Annex B (normative) - Guidelines for measuring low
        sulfur concentrations
Bibliography

This European Standard specifies an energy dispersive X-ray fluorescence (EDXRF) test method for the determination of the sulfur content of automotive gasolines, including those containing up to 5 % (m/m) oxygen, and of automotive diesel fuels, including those containing up to 10 % (V/V) fatty acid methylester (FAME), having sulfur contents in the range 2 mg/kg to 50 mg/kg. Other products may be analysed and other sulfur contents may be determined according to this test method, however, no precision data for products other than automotive fuels and for results outside the specified range have been established for this standard. For reasons of spectral overlap, this standard is not applicable to leaded automotive gasolines, lead replacement gasolines containing greater than 8 mg/kg lead, or to products and feedstocks containing lead, silicon, phosphorus, calcium, potassium or halides at concentrations greater than one tenth of the concentration of sulfur measured or more than 10 mg/kg, whichever is the greater.

Committee
CEN/TC 19
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

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EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
BS EN 16709 : 2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
I.S. EN 228:2017 AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS
DIN EN 228:2004-03 AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS
I.S. EN 16709:2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214 E : 2003 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
BS EN 590 : 2013 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
DIN EN 16709 E : 2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 228:2017-08 AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS
EN 14214:2012+A1:2014/AC:2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
14/30294041 DC : 0 BS EN 16709 - AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 OR B30) - REQUIREMENTS AND TEST METHODS
EN 590:2013 Automotive fuels - Diesel - Requirements and test methods
EN 228:2012+A1:2017 Automotive fuels - Unleaded petrol - Requirements and test methods
BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
I.S. EN 590:2013+A1:2017&LC:2017 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
DIN EN 16709:2015-12 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
UNE-EN 16709:2016 Automotive fuels - High FAME diesel fuel (B20 and B30) - Requirements and test methods
UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
UNE-EN 228:2013 Automotive fuels - Unleaded petrol - Requirements and test methods

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 20847:2004 Petroleum products Determination of sulfur content of automotive fuels Energy-dispersive X-ray fluorescence spectrometry
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test

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