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MATERIALS AND ARTICLES IN CONTACT WITH FOODSTUFFS - PLASTICS SUBSTANCES SUBJECT TO LIMITATION - PART 7: DETERMINATION OF MONOETHYLENE GLYCOL AND DIETHYLENE GLYCOL IN FOOD SIMULANTS
Publisher: National Standards Authority of Ireland
Published:
Available Formats: PDF - English, Hardcopy - English More Info on product formats
For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.Only cited Standards give presumption of conformance to New Approach Directives/Regulations.
Foreword1 Scope2 Normative references3 Principle4 Reagents5 Apparatus6 Samples7 Procedure 7.1 Preparation of standards 7.1.1 Intermediate standards 7.1.2 Internal standard, 800 mg/l butan-1,4-diol 7.1.3 Working standards for aqueous simulants 7.1.4 Working standards for olive oil 7.2 Preparation of calibration graphs 7.2.1 Injection of standards 7.2.2 Validation of stock monoethylene glycol/diethylene glycol solution 7.3 Extraction of olive oil simulant migration test samples 7.4 Preparation of aqueous simulant migration test samples 7.5 Injection of samples8 Expression of results 8.1 Method of calculation 8.1.1 As milligrams of monoethylene glycol and diethylene glycol per kilogram of food simulant 8.1.2 As milligrams of monoethylene glycol and diethylene glycol per square decimetre of surface area of plastic material or article 8.1.3 Calculation of the specific migration 8.2 Precision 8.2.1 Validation 8.2.2 Repeatability and reproducibility 8.2.3 Detection limit9 Confirmation of monoethylene glycol and diethylene glycol 9.1 Requirement for confirmation 9.2 Confirmation by re-analysis using confirmed by gas chromatography - mass spectrometry10 Test reportAnnex A (informative)Annex B (informative)Bibliography
Specifies methods for the determination of monoethylene glycol and diethylene glycol in the food simulants; water, 3% (w/v) acetic acid, 15% (v/v)ethanol and olive oil and other fatty food simulants, simulants D.
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