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I.S. EN 13656:2002

I.S. EN 13656:2002

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

CHARACTERISATION OF WASTE - MICROWAVE ASSISTED DIGESTION WITH HYDROFLUORIC (HF), NITRIC (HNO[3]) AND HYDROCHLORIC (HCI) ACID MIXTURE FOR SUBSEQUENT DETERMINATION OF ELEMENTS

Available format(s)

Hardcopy , PDF

Superseded date

12-08-2020

Language(s)

English

Published date

01-01-2002

Publisher

National Standards Authority of Ireland

Preview

For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.

Only cited Standards give presumption of conformance to New Approach Directives/Regulations.

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Safety remarks
5 Sample
   5.1 Sample pre-treatment
   5.2 Mass of test portion
6 Equipment
   6.1 Closed vessel system
       6.1.1 Microwave unit
       6.1.2 Digestion vessels
   6.2 Semi-open vessel system
       6.2.1 Microwave unit
       6.2.2 Digestion vessels
   6.3 General equipment
7 Reagents
8 Interferences and sources of error
   8.1 General informations
   8.2 Closed vessel system
   8.3 Semi-open vessel system
9 Procedure
   9.1 Blank test
   9.2 Procedure for closed vessels
       9.2.1 Amount of samples and reagents
       9.2.2 Digestion
       9.2.3 Complexation of HF
       9.2.4 Preparation of the solution for analysis
   9.3 Procedure for semi-open vessels
       9.3.1 Amount of samples
       9.3.2 Digestion and complexation of HF
       9.3.3 Preparation of the solution for analysis
10 Test report
Annex A (normative) Calibration of the powder adjustment
Annex B (informative) Validation
Bibliography

Provides methods of microwave assisted digestion with hydrofluoric (HF), nitric (HNO[3]) and hydrochloric (HCI) acid mixture.

DocumentType
Standard
Pages
28
PublisherName
National Standards Authority of Ireland
Status
Superseded
SupersededBy

Standards Relationship
ONORM EN 13656 : 2002 Identical
NBN EN 13656 : 2002 Identical
NEN EN 13656 : 2002 Identical
NF EN 13656 : 2003 Identical
NS EN 13656 : 1ED 2002 Identical
DIN EN 13656:2003-01 Identical
SN EN 13656 : 2002 Identical
UNE-EN 13656:2003 Identical
EN 13656 : 2002 Identical
BS EN 13656:2002 Identical
UNI EN 13656 : 2004 Identical

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
EN 1483:2007 Water quality - Determination of mercury - Method using atomic absorption spectrometry
EN ISO 5961 : 1995 WATER QUALITY - DETERMINATION OF CADMIUM BY ATOMIC ABSORPTION SPECTROMETRY (ISO 5961:1994)
ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method
ENV 12506 : DRAFT 2000 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, CD, CR (6), CU, NI, PB, ZN, CL[-], NO[2][-], SO[4][2-]
ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
ISO 8288:1986 Water quality — Determination of cobalt, nickel, copper, zinc, cadmium and lead — Flame atomic absorption spectrometric methods
ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
EN 1233 : 1996 WATER QUALITY - DETERMINATION OF CHROMIUM - ATOMIC ABSORPTION SPECTROMETRIC METHODS
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 11969:1996 WATER QUALITY - DETERMINATION OF ARSENIC - ATOMIC ABSORPTION SPECTROMETRIC METHOD (HYDRIDE TECHNIQUE)
ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
EN 45001 : 1989 GENERAL CRITERIA FOR THE OPERATION OF TESTING LABORATORIES

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