ASTM D 6247 : 2018
Current
The latest, up-to-date edition.
Standard Test Method for Determination of Elemental Content of Polyolefins by Wavelength Dispersive X-ray Fluorescence Spectrometry
Hardcopy , PDF
English
01-10-2018
This test method covers a general procedure for the determination of elemental content in polyolefins by wavelength-dispersive X-ray fluorescence (WDXRF) spectrometry, in mass fraction ranges typical of those contributed by additives, catalysts, and reactor processes.
1.1This test method covers a general procedure for the determination of elemental content in polyolefins by wavelength-dispersive X-ray fluorescence (WDXRF) spectrometry, in mass fraction ranges typical of those contributed by additives, catalysts, and reactor processes. The elements covered by this test method include fluorine, sodium, magnesium, aluminum, silicon, phosphorus, sulfur, calcium, titanium, chromium, and zinc in the composition ranges given in Table 1.
1.1.1This test method does not apply to polymers specifically formulated to contain flame retardants including brominated compounds and antimony trioxide.
1.1.2This test method does not apply to polymers formulated to contain high levels of compounds of vanadium, molybdenum, cadmium, tin, barium, lead, and mercury because the performance can be strongly influenced by spectral interferences or interelement effects due to these elements.
Note 1:Specific methods and capabilities of users may vary with differences in interelement effects and sensitivities, instrumentation and applications software, and practices between laboratories. Development and use of test procedures to measure particular elements, mass fraction ranges or matrices is the responsibility of individual users.
Note 2:One general method is outlined herein; alternative analytical practices can be followed, and are attached in notes, where appropriate.
1.2The values stated in SI units are to be regarded as the standard.
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 10.
Note 3:There is no known ISO equivalent to this standard.
1.4This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| Committee |
D 20
|
| DocumentType |
Test Method
|
| Pages |
12
|
| ProductNote |
THIS STANDARD ALSO REFERS TO JCGM 100 : 2008
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
| Supersedes |
| ASTM D 5929 : 2018 | Standard Test Method for Determining Biodegradability of Materials Exposed to Source-Separated Organic Municipal Solid Waste Mesophilic Composting Conditions by Respirometry |
| ASTM D 4703 : 2002 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM D 883 : 2023 | Standard Terminology Relating to Plastics |
| ASTM D 6247 : 1998 | Standard Test Method for Analysis of Elemental Content in Polyolefins By X-Ray Fluorescence Spectrometry |
| ASTM C 1118 : 2007 | Standard Guide for Selecting Components for Wavelength-Dispersive X-Ray Fluorescence (XRF) Systems (Withdrawn 2011) |
| ASTM E 29 : 2013 : R2019 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
| ASTM E 1621 : 2013 | Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry |
| ASTM D 883 : 2024 | Standard Terminology Relating to Plastics |
| ASTM E 135 : 2023 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1361 : 2002 : R2021 | Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis |
| ASTM E 29 : 2002 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
| ASTM E 135 : 2021 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 4703 : 2003 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM D 883 : 2022 | Standard Terminology Relating to Plastics |
| ASTM E 1621 : 2005 | Standard Guide for X-Ray Emission Spectrometric Analysis |
| ASTM D 883 : 2020 : REV B | Standard Terminology Relating to Plastics |
| ASTM D 4703 : 1993 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM E 1361 : 1990 : R1999 | Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis |
| ASTM E 1361 : 2002 : R2007 | Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis |
| ASTM E 135 : 2003 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 4703 : 2010 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM E 1601 : 2019 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1621 : 2022 | Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry |
| ASTM E 1361 : 2002 | Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis |
| ASTM E 135 : 2023 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1601 : 1998 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1601 : 2010 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1621 : 2021 | Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry |
| ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1361 : 2002 : R2014 : EDT 1 | Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis |
| ASTM E 135 : 2022 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1601 : 2012 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 135 : 2022 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM C 1118 : 1989 : R2000 | Standard Guide for Selecting Components for Wavelength-Dispersive X-Ray Fluorescence (XRF) Systems |
| ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 : REV C | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 4703 : 2000 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM D 4703 : 2010 : REV A | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM E 135 : 2022 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 4703 : 2016 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM E 1621 : 1994 : R1999 | Standard Guide for X-Ray Emission Spectrometric Analysis |
| ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM D 4703 : 2007 | Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets |
| ASTM E 29 : 2022 | Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications |
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